2-Bromo-4′-Nitroacetophenone CAS 99-81-0 Purity >98.5% (HPLC)

Short Description:

Chemical Name: 2-Bromo-4′-Nitroacetophenone

Synonyms: 4-Nitrophenacyl Bromide 

CAS: 99-81-0

Purity: >98.5% (HPLC)  

Appearance: Light Yellow to Yellow Crystalline Powder 

Contact: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com


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Description:

Shanghai Ruifu Chemical Co., Ltd. is the leading manufacturer and supplier of 2-Bromo-4'-Nitroacetophenone (CAS: 99-81-0) with high quality. We can provide COA, worldwide delivery, small and bulk quantities available. If you are interested in this product, please send detailed information includes CAS number, product name, quantity to us. Please contact: alvin@ruifuchem.com

Chemical Properties:

Chemical Name 2-Bromo-4'-Nitroacetophenone 
Synonyms α-Bromo-4-Nitroacetophenone; 4-Nitrophenacyl Bromide; p-Nitrophenacyl Bromide; ω-Bromo-4-Nitroacetophenone; alpha-Bromo-4-Nitroacetophenone; 2-Bromo-1-(4-Nitrophenyl)ethanone; 2-Bromo-1-(4-Nitrophenyl)ethan-1-one 
CAS Number 99-81-0 
CAT Number RF2928
Stock Status In Stock, Production Capacity 15 Tons per Month  
Molecular Formula C8H6BrNO3 
Molecular Weight 244.04  
Melting Point 97.0 to 101.0℃
Boiling Point 325.2±17.0℃ at 760 mmHg
Flash Point 150.5℃
Density 1.671g/cm3
Sensitive Air Sensitive 
Hazard Note  Irritant
TSCA Yes
Hazard Class  8
Packing Group  III
HS Code  29147000
Brand Ruifu Chemical

Specifications:

Item Specifications
Appearance Light Yellow to Yellow Crystalline Powder
Purity / Analysis Method >98.5% (HPLC) 
Melting Point 97.0 to 101.0℃
Loss on Drying <1.00%
4-Nitroacetophenone <0.50% (HPLC)
Total Impurities <1.50%
Infrared Spectrum Conforms to Structure
Solubility in Hot Methanol Very Faint Turbidity Pass
Test Standard Enterprise Standard
Usage Organic Synthesis; Pharmaceutical Intermediates

Package & Storage:

Package: Bottle, Aluminum foil bag, 25kg/Cardboard Drum, or according to customer's requirement

Storage Condition: Store in sealed containers at cool and dry place; Protect from light and moisture

Advantages:

Sufficient Capacity: Sufficient facilities and technicians

Professional Service: One stop purchasing service

OEM Package: Custom package and label available

Fast Delivery: If within stock, three days delivery guaranteed

Stable Supply: Maintain reasonable stock    

Technical Support: Technology solution available

Custom Synthesis Service: Ranged from grams to kilos

High Quality: Established a complete quality assurance system

FAQ:

How to Purchase? Please contact Dr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com 

15 Years Experience? We have more than 15 years of experience in the manufacture and export of a wide range of high quality pharmaceutical intermediates or fine chemicals.

Main Markets? Sell to domestic market, North America, Europe, India, Korea, Japanese, Australia, etc.

Advantages? Superior quality, affordable price, professional services and technical support, fast delivery.

Quality AssuranceStrict quality control system. Professional equipment for analysis include NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, K.F, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.

SamplesMost products provide free samples for quality evaluation, shipping cost should be paid by customers.

Factory AuditFactory audit welcome. Please make an appointment in advance.

MOQ? No MOQ. Small order is acceptable.

Delivery Time? If within stock, three days delivery guaranteed.

TransportationBy Express (FedEx, DHL), by Air, by Sea.

Documents? After sales service: COA, MOA, ROS, MSDS, etc. can be provided.

Custom SynthesisCan provide custom synthesis services to best fit your research needs.

Payment TermsProforma invoice will be sent first after confirmation of order, enclosed our bank information. Payment by T/T (Telex Transfer), PayPal, Western Union, etc. 

Application:

2-Bromo-4'-Nitroacetophenone (CAS: 99-81-0) is used as raw materials for organic synthesis and pharmaceutical intermediates, etc. A pharmaceutical intermediate for the synthesis of chloramphenicol and the like. Preparation Method It is prepared by bromination of p-nitroacetophenone. The solvent chlorobenzene and p-nitroacetophenone are added into the reaction vessel, and a small amount of bromine is added dropwise at 18℃, the temperature is controlled at 26~28℃, and bromine is added dropwise. After dropping, the reaction is carried out for 1 hour, and the temperature is raised to drive out HBr, and the post-treatment is obtained.
99-81-0 - Risk and Safety
Hazard Symbols: C - Corrosive
Risk Codes: R34 - Causes burns
Safety Description: S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible)

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