6-Aminohexanoic Acid CAS 60-32-2 (ε-aminocaproic Acid) Assay 98.5 ~ 100.5% Factory

6-Aminohexanoic Acid (ε-Aminocaproic Acid) (CAS: 60-32-2) AJI97 Hanyar Gwaji
ε-Aminocaproic Acid, idan aka lissafta bisa tushen anhydrous, ya ƙunshi bai wuce kashi 98.5 ba kuma bai wuce kashi 100.5 na ε-Aminocaproic Acid (C6H13NO2).
Bayani: Farin lu'ulu'u ko lu'ulu'u masu launin fari, ɗanɗano mai ɗaci.
Mai narkewa cikin ruwa da glacial acetic acid, dan kadan mai narkewa a cikin methanol, a zahiri maras narkewa a cikin ethanol.
Solubility (H2O, g/100g): Yana iya narkewa cikin ruwa
Ganewa: Kwatanta nau'in infrared na samfurin tare da ma'auni ta hanyar fayafai bromide.
Ƙayyadaddun bayanai:
Halin Magani (Mai watsawa): 0.5g a cikin 10ml na H2O, spectrophotometer, 430nm, 10mm kauri.
Chloride (Cl): 0.7g, A-1, ref: 0.40ml na 0.01mol/L HCl
Ammonium (NH4): B-1
Sulfate (SO4): 1.2g, (1), ref: 0.50ml na 0.005mol/L H2SO4
Iron (Fe): 0.5g, Ref: 1.5ml na Iron Std.(0.01mg/ml)
Karfe masu nauyi (Pb): 2.0g, (1), pH=7, ref: 2.0ml na Pb Std.(0.01mg/ml)
Arsenic (As2O3): 2.0g, (1), ref: 2.0ml na As2O3 Std.
Sauran Amino Acids: Gwajin gwaji: 100μg, B-1-a, sarrafawa;ε-Acp 0.6μg
Ruwa: 500mg, methanol: ethyleneglycol (1:2) don Hanyar Karl Fischer, A, na mintina 15.
Residue on Ignition (Sulfated): AJI Test 13
Assay: Samfurin ƙididdiga akan tushen anhydrous, 130mg, (1), 3ml na formic acid, 50ml na glacial acetic acid, 0.1mol/L HCLO4 1ml=13.117mg C6H13NO2
pH: 1.0g a cikin 10ml na H2O
Ƙayyadaddun ma'auni da yanayin da aka ba da shawarar: Tsayayyen kwantena a zafin dakin da aka sarrafa (shekaru 2).

6-Aminohexanoic Acid (ε-Aminocaproic Acid) (CAS: 60-32-2) Hanyar Gwajin USP35
Aminocaproic acid ya ƙunshi bai wuce kashi 98.5 ba kuma bai wuce kashi 101.5 na C6H13NO2 ba, ana ƙididdige shi bisa tushen anhydrous.
Marufi da ajiya-Ajiye a cikin matsuguni.Ajiye a zafin jiki.
Matsayin Magana na USP <11>-
USP Aminocaproic acid RS
Ganewa, Ciwon Infrared <197K>.
Ruwa, Hanyar I <921>: bai wuce 0.5% ba.
Ragowa akan kunnawa <281>: bai wuce 0.1% ba.
Karfe masu nauyi, Hanyar II <231>: 0.002%.
Assay-
Magani A- Canja wurin 0.55 g na sodium 1-heptanesulfonate zuwa 1000-mL volumetric flask, narke a cikin kuma tsarma da ruwa zuwa girma, da kuma haɗuwa.
Wayar hannu lokaci- Canja wurin 10 g na monobasic potassium phosphate zuwa 1000-mL beaker, narke a cikin 300 ml na Magani A, ƙara 250 ml na methanol, bi da wani 300 ml na Magani A, da kuma Mix.Daidaita cakuda tare da phosphoric acid zuwa pH na 2.2.Canja wurin duka cakuda zuwa 1000-mL flask volumetric, tsoma tare da Magani A zuwa girma, da haɗuwa.Tace da dagaske.Yi gyare-gyare idan ya cancanta (duba Dacewar Tsarin ƙarƙashin Chromatography <621>).
Maganin daidaitaccen ciki-Shirya maganin methionine a cikin ruwa mai ɗauke da 1.25 MG kowace ml.
Daidaitaccen shiri-Narke daidai adadin USP Aminocaproic Acid RS a cikin ruwa don samun maganin Hannun jari mai sananniya na 12.5 MG kowace ml.Canja wurin 5.0 ml na Maganin Hannun Jari zuwa 100-mL flask volumetric, ƙara 2.0 ml na daidaitaccen bayani na ciki, tsarma da ruwa zuwa ƙarar, da haɗuwa.
Shirye-shiryen Assay-Canja wurin daidaitaccen adadin 1.25 g na Aminocaproic Acid zuwa faifan volumetric 100-mL, narke ciki kuma a tsoma shi da ruwa zuwa ƙara, da haɗuwa.Canja wurin 5.0 ml na wannan maganin zuwa 100-mL flask volumetric, ƙara 2.0mL na daidaitaccen bayani na ciki, tsarma da ruwa zuwa ƙara, da haɗuwa.
Tsarin Chromatographic (duba Chromatography <621>) -Chromatograph na ruwa an sanye shi da na'urar ganowa na 210-nm da ginshiƙi na 4.6-mm × 15-cm wanda ya ƙunshi tattara L1 kuma ana kiyaye shi a 30°.Matsakaicin kwarara shine kusan 0.7 ml a minti daya.Chromatograph da Daidaitaccen shiri, da yin rikodin martanin kololuwa kamar yadda aka umurce su don Tsari: lokutan riƙewar dangi kusan 0.76 na aminocaproic acid da 1.0 na methionine;ƙuduri, R, tsakanin aminocaproic acid da methionine bai zama ƙasa da 2.0 ba;kuma madaidaicin ma'auni na dangi don kwafin injections bai wuce 2.0%.
Tsari-Na dabam allura daidai juzu'i (kimanin 20 µL) na daidaitaccen shiri da shirye-shiryen Assay a cikin chromatograph, kuma ba da damar shirye-shiryen Assay ya ɓace don bai gaza sau biyu lokacin riƙe aminocaproic acid ba.Yi rikodin chromatograms, kuma auna duk mafi girman martani.Yi ƙididdige adadin, a g, na C6H13NO2 a cikin ɓangaren Aminocaproic Acid da aka ɗauka ta dabara:
2C (RU / RS)
wanda C shine maida hankali, a cikin MG da ml, na USP Aminocaproic Acid RS a cikin Shirye-shiryen Daidaitawa;da RU da RS sune ma'auni na amsawar aminocaproic acid ga mafi girman martani na ciki da aka samu daga shirye-shiryen Assay da Daidaitaccen shiri, bi da bi.