(Boc) 2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Tsarkake>99.0% (HPLC) Reagent Kariyar Factory

Takaitaccen Bayani:

Sunan Sinadari: Di-tert-Butyl Iminodicarboxylate

Ma’ana: (Boc)2NH;N-Boc-tert-Butylcarbamate

Saukewa: 51779-32-9

Tsafta:> 99.0% (HPLC)

Bayyanar: Farin Crystalline Foda

Kare Reagent, Babban inganci

Tuntuɓi: Dr. Alvin Huang

Wayar hannu/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com


Cikakken Bayani

Samfura masu dangantaka

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Bayani:

Shanghai Ruifu Chemical Co., Ltd. shine babban kamfani na Di-tert-Butyl Iminodicarboxylate ((Boc) 2NH) (CAS: 51779-32-9) tare da babban inganci.Ruifu Chemical yana ba da jerin abubuwan kariya da reagents masu haɗawa.Za mu iya samar da isarwa a duniya, farashi mai gasa, ƙanana da yawa da ake samu.Sayi Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com

Abubuwan Sinadarai:

Sunan Sinadari Di-tert-Butyl Iminodicarboxylate
Makamantu (Boc) 2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic acid Di-tert-Butyl Ester;Bis (tert-Butoxycarbonyl) ammonia
Matsayin Hannun jari A Stock
Lambar CAS 51779-32-9
Tsarin kwayoyin halitta Saukewa: C10H19NO4
Nauyin Kwayoyin Halitta 217.27 g/mol
Matsayin narkewa 114.0 ~ 120.0 ℃
Yawan yawa 1.037± 0.06 g/cm3
M Mai Sauraron Iska, Mai Haske
Ruwan Solubility Mara narkewa a cikin Ruwa
Solubility Chloroform, methanol
Adana Yanayin. Wuri Mai sanyi & Busassun wuri (2 ~ 8 ℃)
COA & MSDS Akwai
Kashi Kare Reagent
Alamar Ruifu Chemical

Ƙayyadaddun bayanai:

Abubuwa Ka'idojin dubawa Sakamako
Bayyanar Farin Crystalline Foda Ya bi
Matsayin narkewa 114.0 ~ 120.0 ℃ 118.8 ~ 119.3 ℃
Asara akan bushewa <0.50% 0.10%
Tsarkake / Hanyar Bincike > 99.0% (HPLC) 99.6%
Infrared Spectrum Yayi daidai da Tsarin Ya bi
Farashin NMR Spectrum Yayi daidai da Tsarin Ya bi
Kammalawa An gwada samfurin kuma ya bi ƙayyadaddun da aka bayar

Gwajin Tsafta:

Shafin Chromatographic: SE-54 30m×0.25mm × 0.5μm;
Mai ganowa: FID
Zazzabi na farko: 100 ℃
Lokacin farko: 1min
Yawan dumama: 20 ℃/min
Zazzabi na ƙarshe: 190 ℃
A karshen: 10 min
Zafin allura: 160 ℃
Zazzabi na ganowa: 200 ℃
Raba rabo: 50:1;
Girman samfurin: 0.2μl;
Mai narkewa: methanol
Sakamako: Tsaftar ya fi 99.0% ta hanyar daidaita yanki.

Kunshin/Ajiye/Jirgin ruwa:

Kunshin:Bottle, Aluminum tsare jakar, 25kg / Kwali Drum, ko bisa ga abokin ciniki ta bukata.
Yanayin Ajiya:Ajiye a cikin kwantena da aka rufe a wurin sanyi da bushe (2 ~ 8 ℃) nesa da abubuwan da ba su dace ba.Kare daga haske da danshi.
Jirgin ruwa:Bayarwa ga duniya ta FedEx / DHL Express.Bayar da isarwa cikin sauri kuma abin dogaro.

Amfani:

Isasshen Ƙarfin: isassun wurare da masu fasaha

Sabis na Ƙwararru: Sabis na siyan tasha ɗaya

Kunshin OEM: Kunshin al'ada da alamar akwai

Bayarwa da sauri: Idan yana cikin haja, garantin isar da kwanaki uku

Ƙarfin Ƙarfi: Kula da haja mai ma'ana

Taimakon Fasaha: Akwai maganin fasaha

Sabis na Haɗa na Musamman: Ya bambanta daga gram zuwa kilos

High Quality: An kafa cikakken tsarin tabbatar da inganci

FAQ:

Yadda ake siya?Da fatan za a tuntuɓiDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com 

Kwarewar Shekaru 15?Muna da fiye da shekaru 15 na gwaninta a cikin ƙira da fitarwa na matsakaicin matsakaicin magunguna masu inganci ko sinadarai masu kyau.

Manyan Kasuwanni?Sayarwa zuwa kasuwannin cikin gida, Arewacin Amurka, Turai, Indiya, Koriya, Jafananci, Australia, da sauransu.

Fa'idodi?Babban inganci, farashi mai araha, sabis na ƙwararru da tallafin fasaha, bayarwa da sauri.

inganciTabbaci?Tsananin kula da ingancin inganci.Kayan aikin ƙwararru don bincike sun haɗa da NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, gwajin ƙayyadaddun ƙwayoyin cuta, da sauransu.

Misali?Yawancin samfurori suna ba da samfurori kyauta don ƙima mai kyau, farashin jigilar kaya ya kamata a biya ta abokan ciniki.

Binciken Masana'antu?Ma'aikata duba maraba.Da fatan za a yi alƙawari a gaba.

MOQ?Babu MOQ.Karamin tsari abin karɓa ne.

Lokacin Bayarwa? Idan cikin hannun jari, garantin isar da kwana uku.

Sufuri?By Express (FedEx, DHL), ta Air, ta Teku.

Takardu?Bayan sabis na tallace-tallace: COA, MOA, ROS, MSDS, da dai sauransu za a iya ba da su.

Haɗin Kan Al'ada?Zai iya ba da sabis na haɗawa na al'ada don dacewa da buƙatun bincikenku.

Sharuɗɗan Biyan kuɗi?Za a fara aiko da daftari na Proforma bayan tabbatar da oda, an rufe bayanan bankin mu.Biya ta T/T (Telex Transfer), PayPal, Western Union, da dai sauransu.

51779-32-9 - Haɗari da Tsaro:

Alamomin haɗari Xi - Haushi
Lambobin haɗari 36/37/38 - Haɗa kai ga idanu, tsarin numfashi da fata.
Bayanin Tsaro S26 - Idan ana hulɗa da idanu, kurkura nan da nan da ruwa mai yawa kuma ku nemi shawarar likita.
S37/39 - Saka safofin hannu masu dacewa da kariya / ido
WGK Jamus 3
Farashin 29241990
Hazard Note Irritant

Aikace-aikace:

Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Aikace-aikacen Di-tert-Butyl Iminodicarboxylate matsakaicin magunguna ne, wanda za'a iya shirya ta hanyar amsawar mataki ɗaya na formamide da Boc2O.
Ana amfani da fili a matsayin reagent don shirye-shiryen amines na farko daga alkyl halides.Ya shahara a matsayin madadin kirarin Jibrilu don wannan juyi.Hakanan ana iya shirya amines daga barasa ta hanyar bushewa ta amfani da amsawar Mitsunobu.A cikin aiwatarwa na yau da kullun an cire reagent don ba da gishirin potassium, wanda yake N-alkylated.An cire ƙungiyoyin kare Boc daga baya a ƙarƙashin yanayin acidic.
Di-tert-Butyl Iminodicarboxylate ƙungiya ce ta amintaccen kariya wacce ake amfani da ita don shirya ƙayatattun spirocycles azaman masu adawa da CCR1.
Shirye-shiryen maganin DMAP (0.61g, 5.0mmol) a cikin MeCN (15ml) ana ƙara sannu a hankali zuwa maganin foramide (2.5g,56mmol) da Boc2O (24)g, 110mol) a cikin MeCN (15ml).Bayan yin motsawa a dakin da zafin jiki na 4h, an sanyaya maganin rawaya zuwa 0 ° C, kuma N, N-diethylenediamine (6.97g, 60mmol) an kara a hankali a 0 ℃.Sakamakon cakuda an motsa shi a dakin da zafin jiki na 12h kuma an tace shi ta hanyar siliki na bakin ciki;An tace ruwan da aka samu a dakin da zafin jiki.Ana fitar da sauran ƙarfi a ƙarƙashin rage matsi.An tsarkake danyen samfurin ta silica gel chromatography kuma an cika shi da EtOAc/hexane (1: 5) don samun samfurin take, wanda shine fari mai ƙarfi (10.99g, 92%).

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