(Boc) 2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Tsarkake>99.0% (HPLC) Reagent Kariyar Factory
Shanghai Ruifu Chemical Co., Ltd. shine babban kamfani na Di-tert-Butyl Iminodicarboxylate ((Boc) 2NH) (CAS: 51779-32-9) tare da babban inganci.Ruifu Chemical yana ba da jerin abubuwan kariya da reagents masu haɗawa.Za mu iya samar da isarwa a duniya, farashi mai gasa, ƙanana da yawa da ake samu.Sayi Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com
Sunan Sinadari | Di-tert-Butyl Iminodicarboxylate |
Makamantu | (Boc) 2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic acid Di-tert-Butyl Ester;Bis (tert-Butoxycarbonyl) ammonia |
Matsayin Hannun jari | A Stock |
Lambar CAS | 51779-32-9 |
Tsarin kwayoyin halitta | Saukewa: C10H19NO4 |
Nauyin Kwayoyin Halitta | 217.27 g/mol |
Matsayin narkewa | 114.0 ~ 120.0 ℃ |
Yawan yawa | 1.037± 0.06 g/cm3 |
M | Mai Sauraron Iska, Mai Haske |
Ruwan Solubility | Mara narkewa a cikin Ruwa |
Solubility | Chloroform, methanol |
Adana Yanayin. | Wuri Mai sanyi & Busassun wuri (2 ~ 8 ℃) |
COA & MSDS | Akwai |
Kashi | Kare Reagent |
Alamar | Ruifu Chemical |
Abubuwa | Ka'idojin dubawa | Sakamako |
Bayyanar | Farin Crystalline Foda | Ya bi |
Matsayin narkewa | 114.0 ~ 120.0 ℃ | 118.8 ~ 119.3 ℃ |
Asara akan bushewa | <0.50% | 0.10% |
Tsarkake / Hanyar Bincike | > 99.0% (HPLC) | 99.6% |
Infrared Spectrum | Yayi daidai da Tsarin | Ya bi |
Farashin NMR Spectrum | Yayi daidai da Tsarin | Ya bi |
Kammalawa | An gwada samfurin kuma ya bi ƙayyadaddun da aka bayar |
Shafin Chromatographic: SE-54 30m×0.25mm × 0.5μm;
Mai ganowa: FID
Zazzabi na farko: 100 ℃
Lokacin farko: 1min
Yawan dumama: 20 ℃/min
Zazzabi na ƙarshe: 190 ℃
A karshen: 10 min
Zafin allura: 160 ℃
Zazzabi na ganowa: 200 ℃
Raba rabo: 50:1;
Girman samfurin: 0.2μl;
Mai narkewa: methanol
Sakamako: Tsaftar ya fi 99.0% ta hanyar daidaita yanki.
Kunshin:Bottle, Aluminum tsare jakar, 25kg / Kwali Drum, ko bisa ga abokin ciniki ta bukata.
Yanayin Ajiya:Ajiye a cikin kwantena da aka rufe a wurin sanyi da bushe (2 ~ 8 ℃) nesa da abubuwan da ba su dace ba.Kare daga haske da danshi.
Jirgin ruwa:Bayarwa ga duniya ta FedEx / DHL Express.Bayar da isarwa cikin sauri kuma abin dogaro.
Yadda ake siya?Da fatan za a tuntuɓiDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Kwarewar Shekaru 15?Muna da fiye da shekaru 15 na gwaninta a cikin ƙira da fitarwa na matsakaicin matsakaicin magunguna masu inganci ko sinadarai masu kyau.
Manyan Kasuwanni?Sayarwa zuwa kasuwannin cikin gida, Arewacin Amurka, Turai, Indiya, Koriya, Jafananci, Australia, da sauransu.
Fa'idodi?Babban inganci, farashi mai araha, sabis na ƙwararru da tallafin fasaha, bayarwa da sauri.
inganciTabbaci?Tsananin kula da ingancin inganci.Kayan aikin ƙwararru don bincike sun haɗa da NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, gwajin ƙayyadaddun ƙwayoyin cuta, da sauransu.
Misali?Yawancin samfurori suna ba da samfurori kyauta don ƙima mai kyau, farashin jigilar kaya ya kamata a biya ta abokan ciniki.
Binciken Masana'antu?Ma'aikata duba maraba.Da fatan za a yi alƙawari a gaba.
MOQ?Babu MOQ.Karamin tsari abin karɓa ne.
Lokacin Bayarwa? Idan cikin hannun jari, garantin isar da kwana uku.
Sufuri?By Express (FedEx, DHL), ta Air, ta Teku.
Takardu?Bayan sabis na tallace-tallace: COA, MOA, ROS, MSDS, da dai sauransu za a iya ba da su.
Haɗin Kan Al'ada?Zai iya ba da sabis na haɗawa na al'ada don dacewa da buƙatun bincikenku.
Sharuɗɗan Biyan kuɗi?Za a fara aiko da daftari na Proforma bayan tabbatar da oda, an rufe bayanan bankin mu.Biya ta T/T (Telex Transfer), PayPal, Western Union, da dai sauransu.
Alamomin haɗari Xi - Haushi
Lambobin haɗari 36/37/38 - Haɗa kai ga idanu, tsarin numfashi da fata.
Bayanin Tsaro S26 - Idan ana hulɗa da idanu, kurkura nan da nan da ruwa mai yawa kuma ku nemi shawarar likita.
S37/39 - Saka safofin hannu masu dacewa da kariya / ido
WGK Jamus 3
Farashin 29241990
Hazard Note Irritant
Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Aikace-aikacen Di-tert-Butyl Iminodicarboxylate matsakaicin magunguna ne, wanda za'a iya shirya ta hanyar amsawar mataki ɗaya na formamide da Boc2O.
Ana amfani da fili a matsayin reagent don shirye-shiryen amines na farko daga alkyl halides.Ya shahara a matsayin madadin kirarin Jibrilu don wannan juyi.Hakanan ana iya shirya amines daga barasa ta hanyar bushewa ta amfani da amsawar Mitsunobu.A cikin aiwatarwa na yau da kullun an cire reagent don ba da gishirin potassium, wanda yake N-alkylated.An cire ƙungiyoyin kare Boc daga baya a ƙarƙashin yanayin acidic.
Di-tert-Butyl Iminodicarboxylate ƙungiya ce ta amintaccen kariya wacce ake amfani da ita don shirya ƙayatattun spirocycles azaman masu adawa da CCR1.
Shirye-shiryen maganin DMAP (0.61g, 5.0mmol) a cikin MeCN (15ml) ana ƙara sannu a hankali zuwa maganin foramide (2.5g,56mmol) da Boc2O (24)g, 110mol) a cikin MeCN (15ml).Bayan yin motsawa a dakin da zafin jiki na 4h, an sanyaya maganin rawaya zuwa 0 ° C, kuma N, N-diethylenediamine (6.97g, 60mmol) an kara a hankali a 0 ℃.Sakamakon cakuda an motsa shi a dakin da zafin jiki na 12h kuma an tace shi ta hanyar siliki na bakin ciki;An tace ruwan da aka samu a dakin da zafin jiki.Ana fitar da sauran ƙarfi a ƙarƙashin rage matsi.An tsarkake danyen samfurin ta silica gel chromatography kuma an cika shi da EtOAc/hexane (1: 5) don samun samfurin take, wanda shine fari mai ƙarfi (10.99g, 92%).