1- (3-Methoxypropyl) -4-Piperidinamine CAS 179474-79-4 Prucalopride Succinate Tsabtace Tsabtace>98.0% (GC)

Wannan samfurin shine 1- (3-Methoxypropyl) -4-Piperidinamine.Ya ƙunshi C9H20N2O ba zai ƙasa da 98.0% ba, ana ƙididdige shi akan tushen anhydrous.
[Properties: Wannan samfurin ba shi da launi zuwa ruwan rawaya mai haske.
Ɗauki adadin ruwan da ya dace na wannan samfurin, ƙara ƙarfi (methanol), narkar da shi, ƙayyade shi bisa ga hanyar ƙayyade ruwa (Shafi Ⅷ M, hanyar farko A), yi amfani da gwajin gwajin Fisher don ƙayyade har sai maganin ya canza daga rawaya mai haske. zuwa ja launin ruwan kasa mai nuna alamar ƙarshen, da kuma gudanar da wani gwajin mara komai.Yi lissafin bisa ga tsari mai zuwa: abun ciki na ruwa kada ya wuce 1.0%.
Abun ciki (%) = (AB) F/W×100%
Inda, A shine adadin ruwan Fisher da samfurin gwajin ya cinye (ml);
B shine ƙarar ruwan gwajin Fisher da babu sarari, ml;
F shine nauyin maganin gwajin Fisher daidai da ruwa a kowace 1ml, mg;
W shine nauyin samfurin gwajin, mg
Najasa ɗaya
Dangane da yanayin ganowa da hanyoyin da ke ƙarƙashin [ƙaddamar da abun ciki], an yi rikodin chromatogram kuma lokacin riƙewa daga babban kololuwa shine sau 3.Idan akwai ƙarancin ƙazanta a cikin maganin gwajin, ƙazanta ɗaya ba zai wuce 0.5% ba kuma jimlar duk ƙazanta bazai wuce 2.0% bisa ga hanyar daidaita yankin ba.
[Ƙaddarar Abun Ciki] Dangane da hanyar ƙayyadaddun ƙayyadaddun ƙarfi (Shafi Ⅷ P)
(6%) cyanopropyl phenyl - (94%) dimethylpolysiloxane (ko irin wannan polarity) a matsayin kafaffen ginshiƙi na capillary ruwa;
An yi amfani da tsarin dumama tsarin da aka tsara na tsarin samar da ginshiƙi na babban sararin samaniya tare da yanayin chromatographic gas.Zazzabi na farko ya kasance 100 ℃ na 5min, kuma an ɗaga zafin a 15 ℃ a minti daya zuwa 250 ℃ na 4min.Matsakaicin zafin jiki ya kai 250 ℃, kuma zafin mai ganowa ya kasance 280 ℃.Yawan kwarara ya kasance 4ml/min.Matsakaicin shunt shine 8: 1.
Game da 0.6g na wannan samfurin an dauki, daidai a auna, sanya shi a cikin kwalban 10ml, narkar da methanol da diluted zuwa sikelin, a matsayin gwajin samfurin bayani.An yi allurar maganin samfurin tare da 1μl aƙalla sau biyu a jere, bi da bi.An ƙayyade iyakar kololuwar da za a auna.Babban tsaftar kololuwa bai gaza 98.0% ba bisa ga hanyar daidaita yankin kololuwa.