Inosine CAS 58-63-9 Assay 98.0 ~ 102.0% Babban Ingancin Factory

Inosine (CAS: 58-63-9) Hanyar Gwajin ChP2020
Inosin - BAYANI
Abubuwan da ke cikin C10H12N4O5 za su kasance tsakanin 98.0% da 102.0% da aka lissafta akan busasshen samfurin.
Inosine - Hali Wannan samfurin shine farin crystalline foda;Mara wari.Wannan samfurin yana ɗan narkewa a cikin ruwa, wanda ba zai iya narkewa a cikin ethanol, kuma yana narkewa a cikin ruwa mai narkewa a cikin hydrochloric acid da sodium hydroxide.
Inosine - GANE
1. Dauki daidai adadin 0.01% bayani na wannan samfurin, ƙara daidai adadin 3, 5-dihydroxytoluene bayani (dauki 3, 5-dihydroxytoluene da ferric chloride 0.lg, ƙara hydrochloric acid don yin 100ml), haɗuwa da kyau, bayan haka. dumama a cikin wanka na ruwa na kimanin minti 10, an ga launin kore.
2. A cikin chromatogram da aka rubuta a ƙarƙashin abin ƙaddamar da abun ciki, lokacin riƙewa na babban kololuwar maganin gwajin ya kamata ya kasance daidai da lokacin riƙewa na babban kololuwar bayani.
3. Bakan shayarwar infrared na wannan samfurin ya kamata ya kasance daidai da na sarrafawa (Spectrum set 605).
Inosin - Analysis
Isar da Magani
Ɗauki 0.5g na wannan samfurin, ƙara 50ml na ruwa don narke, bisa ga UV-bayyana spectrophotometry (General law 0401), ƙayyade watsawa a tsawon 430nm, ba kasa da 98.0%.(Don allura)
Abubuwa masu alaƙa
Ɗauki wannan samfurin, ƙara ruwa don narkar da kuma tsarma don yin bayani mai dauke da 0.5mg da 1ml a matsayin maganin gwaji;Ɗauki 1ml don auna daidai, saka shi a cikin gilashin aunawa 100ml, tsoma shi da ruwa zuwa ma'auni, a matsayin maganin sarrafawa.Dangane da yanayin chromatographic a ƙarƙashin abin ƙaddara abun ciki, 20 u1 na maganin gwajin da maganin sarrafawa ana allura bi da bi a cikin chromatograph na ruwa, kuma ana yin rikodin chromatogram zuwa sau 2 na lokacin riƙewa na babban kololuwa.Idan akwai kololuwa na ƙazanta a cikin chromatogram na maganin gwajin, jimillar kowane yanki mai ƙazanta ba zai zama mafi girma fiye da babban yanki mafi girma na maganin sarrafawa (1.0%) ba.
Asara akan bushewa
Ɗauki wannan samfurin, bushe zuwa madaidaicin nauyi a 105 ° C, asarar nauyi ba zai wuce 1.0% ba (Gaba ɗaya doka 0831).
Ragowa akan ƙonewa (Sulfated)
Ba fiye da 0.1% (don allura), ko fiye da 0.2% (don yin amfani da baki) (Gaba ɗaya doka 0841).
Karfe masu nauyi
Ɗauki wannan samfurin 1.0g, dubawa bisa ga doka (Gaba ɗaya ƙa'idodin 0821 doka ta biyu), mai ɗauke da ƙarfe mai nauyi ba zai wuce sassa 10 a kowace miliyan ba.
Rashin Dafi
Ɗauki wannan samfurin, ƙara allurar sodium chloride don narkewa da tsarma maganin da ke dauke da inosine 10mg a kowace 1ml, duba bisa ga doka (Gaba ɗaya doka 1141), ya kamata ya bi tanadi.(Don allura)
Inosine - Ƙaddamar da abun ciki
An auna ta Babban Ayyukan Liquid Chromatography (Janar 0512).
An yi amfani da yanayin chromatographic da dacewa da tsarin gwajin gel ɗin silica wanda aka haɗa tare da alkyl silane goma sha takwas azaman filler;An yi amfani da methanol-ruwa (10:90) azaman lokacin motsi;Tsayin da aka gano shine 248nm.A sha kamar 10mg na inosine reference, ƙara 1 mol/L hydrochloric acid bayani (1ml), zafi a cikin ruwa wanka a 80 ℃ for 10 minutes, bar shi sanyi, ƙara 1ml na 1 mol/L sodium hydroxide bayani, ƙara ruwa zuwa 50ml. 20u1 allurar ruwa chromatograph, daidaita tsarin chromatographic, matakin rabuwa na inosine ganiya da ƙarancin ƙazanta kusa yakamata ya dace da buƙatun, adadin farantin ka'idar bisa ga ƙididdigar ƙarancin inosine ba ƙasa da 2000 ba.
Assay
Sai ki samu adadin da ya dace na wannan samfurin, ki auna shi daidai, a zuba ruwa ya narke sannan a tsoma shi da yawa, a yi maganin mai dauke da kusan 20ug a kowace lml, a girgiza shi, sannan a yi amfani da shi azaman maganin gwaji, chromatograph na allurar 20ul daidai an auna shi kuma an rubuta chromatogram.An ƙididdige adadin da ya dace na inosine daidai kuma an ƙaddara ta hanya ɗaya, kuma an ƙididdige mafi girman yanki bisa ga daidaitattun hanyar waje.
Inosine - Category
Kwayoyin metabolism suna inganta magunguna.
Inosin - Adanawa
Kariyar haske, ma'ajin da aka rufe.
Magunguna: (1) Maganin Baki na Inosine (2) Allunan Inosine (3) Inosine Allurar (4) Inosine Capsules (5) Inosine da Glucose Allurar (6) Inosine da Sodium Chloride Allurar (7) Inosine don allura