L-(+) - Lysine Monohydrochloride CAS 657-27-2 (H-Lys-OH·HCl) Assay 98.5 ~ 101.0% Factory High Quality
Shanghai Ruifu Chemical Co., Ltd. shine babban masana'anta da mai ba da kaya na L- (+) -Lysine Monohydrochloride (H-Lys-OH · HCl) (CAS: 657-27-2) tare da babban inganci, ƙarfin samarwa 1000 Tons ta kowace. shekara.A matsayin daya daga cikin manyan masu samar da amino acid a kasar Sin, Ruifu Chemical yana samar da amino acid har zuwa matsayin kasa da kasa, kamar AJI, USP, EP, JP da FCC.Za mu iya samar da COA, isarwa a duniya, ƙanana da yawa da ake samu.Idan kuna sha'awar L-(+) - Lysine Monohydrochloride,Please contact: alvin@ruifuchem.com
| Sunan Sinadari | L- (+) - Lysine Monohydrochloride |
| Makamantu | H-Lys-OH · HCl;L-Lysine Monohydrochloride;L-Lysine Hydrochloride;L-Lysine HCl;Laevo-Lysine Hydrochloride;lysine hydrochloride;Monohydrochloride lysine;(S) -2,6-Diaminohexanoic Acid Monohydrochloride |
| Matsayin Hannun jari | A hannun jari, Ƙarfin Samar da Ton 1000 a kowace shekara |
| Lambar CAS | 657-27-2 |
| Tsarin kwayoyin halitta | C6H14N2O2·HCl |
| Nauyin Kwayoyin Halitta | 182.65 |
| Matsayin narkewa | 263 ℃ (Dec.) (lit.) |
| Yawan yawa | 1.28g/cm3 (20 ℃) |
| Ruwan Solubility | Mai narkewa a cikin Ruwa, Kusan Gaskiya |
| Solubility | Soluble a cikin Ruwa da Formic Acid.Soluble sosai a cikin Ethanol.A zahiri Insouble a cikin Ether |
| Adana Yanayin. | An rufe shi a bushe, Ajiye a Zazzabin ɗaki |
| COA & MSDS | Akwai |
| Rabewa | Amino Acid da Abubuwan Haɓakawa |
| Alamar | Ruifu Chemical |
| Lambobin haɗari | 34- Yana haifar da kuna |
| Bayanin Tsaro | S24/25 - Guji hulɗa da fata da idanu. |
| ID na UN | UN 1789 8/PG 3 |
| WGK Jamus | 2 |
| HS Code | 2922419000 |
| Abubuwa | Ka'idojin dubawa | Sakamako |
| Bayyanar | Farin lu'ulu'u ko lu'ulu'u ko foda | Ya dace |
| Ganewa | Infrared Absorption Spectrum | Ya dace |
| Takamaiman Juyawa [α] 20/D | +20.4° zuwa +21.4°(C=8 a 6N HCl) | + 20.8 ° |
| Yanayin Magani (Transmittance) | Bayyananne kuma mara launi ≥98.0% | 98.8% |
| Chloride (Cl) | 19.0 zuwa 19.6% | 19.15% |
| Sulfate (SO4) | ≤0.020% | <0.020% |
| Ammonium (NH4) | ≤0.020% | <0.020% |
| Iron (F) | ≤10ppm | <10ppm |
| Karfe masu nauyi (Pb) | ≤10ppm | <10ppm |
| Arsenic (As2O3) | ≤1.0pm | <1.0pm |
| Sauran Amino Acids | ≤0.50% (TLC) | Ya dace |
| Asara akan bushewa | ≤0.40% (a 105 ℃ na 3 hours) | 0.25% |
| Ragowa akan ƙonewa (Sulfated) | ≤0.10% | 0.06% |
| Assay | 98.5 zuwa 101.5% (kamar bushewar tushen) | 99.7% |
| Najasa maras tabbas | Cika Bukatun | Ya dace |
| Gwajin pH | 5.0 zuwa 6.0 (1.0g a cikin 10ml na H2O) | 5.2 |
| Ragowar Magani | Ya dace | Ya dace |
| Kammalawa | Haɗu da Ma'auni na AJI97;USP;JP | |
| Rayuwar Rayuwa | Watanni 24 Daga Ranar Ƙirƙira Idan An Ajiye shi Da kyau | |
| Babban Amfani | Amino acid;Abubuwan Abincin Abinci / Ciyarwa;Magunguna;Ingantaccen Abinci;da dai sauransu. | |
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) AJI 97 Hanyar Gwaji
Ganewa: Kwatanta nau'in infrared na samfurin tare da ma'auni ta hanyar fayafai bromide.
Takamaiman Juyawa [α] 20/D: Samfurin Busasshen, C=8, 6mol/L HCl
Halin Magani (Mai watsawa): 1.0g a cikin 10ml na H2O spectrophotometer, 430nm, 10nm kauri.
Chloride (Cl): Samfurin Busassun, 370mg, B-1
Ammonium (NH4): B-1
Sulfate (SO4): 1.2g, (1), ref: 0.50ml na 0.005mol/L H2SO4
Iron (Fe): 1.5g, (1), Ref: 1.5ml na Iron Std.(0.01mg/ml)
Karfe masu nauyi (Pb): 2.0g, (4), Ref: 2.0ml na Pb Std.(0.01mg/ml)
Arsenic (As2O3): 2.0g, (1), ref: 2.0ml na As2O3 Std.
Sauran Amino Acids: Samfurin Gwaji: 50μg, S-6-a, sarrafawa: L-Lys HCl 0.25μg
Asarar bushewa: a 105 ℃ na 3 hours.
Gwajin: samfurin bushe, 110mg, (3), 2ml na formic acid, 0.1mol/L HCLO4 1ml=9.133mg C6H14N2O2·HCl
Gwajin pH: 1.0g a cikin 10ml na H2O
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) Hanyar Gwajin USP35
BAYANI
Lysine Hydrochloride ya ƙunshi NLT 98.5% da NMT 101.5% na L-Lysine Hydrochloride (C6H14N2O2 · HCl), ƙididdiga akan busasshen tushe.
GANO
A. RASHIN NUTSUWA <197K>
ASSAY
TSARI
Misali: 90 MG na Lysine Hydrochloride
Blank: Mix 3 ml na formic acid da 50 ml na glacial acetic acid.
Titrimetric tsarin
(Duba Titrimetry <541>)
Yanayin: Kai tsaye titration
Titrant: 0.1 N perchloric acid VS
Gano ƙarshen ƙarshen: Potentiometric
Analysis: Narkar da Samfurin a cikin 3 ml na formic acid da 50ml na glacial acetic acid.Ƙara 10 ml na mercuric acetate TS, kuma titrate tare da Titrant.Yi ƙudurin Blank.
Yi lissafin adadin Lysine Hydrochloride (C6H14N2O2·HCl) a cikin Samfurin da aka ɗauka:
Sakamako = {[(VS-VB) xNxF]/W} x100
VS= Girman titrant da Samfurin (mL) ke cinyewa
VB= Girman titrant da Blank (mL) ke cinyewa
N = ainihin al'ada na Titrant (mEq/ml)
F= ma'aunin daidai, 91.33 mg/mEq
W= Nauyin Nauyin (mg)
Sharuɗɗan karɓa: 98.5% ~ 101.5% akan busasshiyar tushe
SAURAN ABUBUWA
Abun ciki na chloride
Misali: 350 MG na Lysine Hydrochloride
Blank: 140 ml na ruwa
Titrimetric tsarin
(Duba Titrimetry <541>)
Yanayin: Kai tsaye titration
Titrant: 0.1 N azurfa nitrate VS
Gano ƙarshen ƙarshen: Na gani
Analysis: Canja wurin Samfurin zuwa kwanon rufi, kuma ƙara 140 ml na ruwa da 1 ml na dichlorofluorescein TS.Titrate tare da Titrant har sai chloride na azurfa yana yawo kuma cakuda ya sami launin ruwan hoda mara nauyi.Yi ƙudurin Blank.
Yi lissafin adadin chloride (Cl) a cikin Samfurin da aka ɗauka:
Sakamako = {[(VS - VB) × N × F]/W} × 100
VS = Girman titrant yana cinye ta Samfurin (mL)
VB = Girman titrant da Blank (mL) ke cinyewa
N = ainihin al'ada na Titrant (mEq/ml)
F = daidaitattun ma'auni, 35.45 mg/mEq
W = Nauyin Nauyin (mg)
Sharuɗɗan karɓa: 19.0% ~ 19.6%
RASHIN ZUCIYA
SAURAN WUTA <281>: NMT 0.1%
chloride da sulfate, sulfate <221>
Daidaitaccen bayani: 0.10ml na 0.020 N sulfuric acid
Misali: 0.33g na Lysine Hydrochloride
Sharuɗɗan karɓa: NMT 0.03%
IRON <241>: NMT 30ppm
Share abubuwan masu zuwa:
KARFE MAI KYAU, Hanyar I <231>: NMT 15ppm
Abubuwan da suka danganci
Daidaitaccen bayani: 0.05 mg/mL na USP L-Lysine Hydrochloride RS a cikin ruwa.[NOTE-Wannan bayani yana da maida hankali daidai da 0.5% na na samfurin bayani.]
Maganin samfurin: 10mg/mL na Lysine Hydrochloride a cikin ruwa
Maganin dacewa da tsarin: 0.4 mg/mL kowanne na USP L-Lysine Hydrochloride RS da USP Arginine Hydrochloride RS
Tsarin Chromatographic (Duba Chromatography <621>, Chromatography na bakin-Layer.)
Yanayin: TLC
Adsorbent: 0.25-mm Layer na chromatographic silica gel cakuda
Girman aikace-aikacen: 5μL
Haɓaka tsarin ƙarfi: isopropyl barasa da ammonium hydroxide (7: 3)
Fesa reagent: 0.2 g na ninhydrin a cikin cakuda butyl barasa da 2N acetic acid (95: 5)
Dacewar tsarin
Bukatun dacewa: chromatogram na tsarin dacewa da tsarin yana nuna aibobi biyu a sarari.
Bincike
Samfura: Daidaitaccen bayani, Maganin dacewa da tsarin, da Samfurin bayani.
Bushe farantin tsakanin 100° da 105° har sai ammonia ya ɓace gaba ɗaya.Fesa da Reagent Fesa, kuma zafi tsakanin 100 ° da 105 ° na 15 min.Yi nazarin farantin a ƙarƙashin farin haske.
Sharuɗɗan karɓa: Duk wani wuri na biyu na samfurin samfurin bai fi girma ko mafi tsanani fiye da ainihin tabo na daidaitaccen bayani ba.
Najasa ɗaya: NMT 0.5%
Jimlar ƙazanta: NMT 2.0%
MAKAMMAN JARRABAWA
Juyawa ta gani, Jujjuya ta musamman <781S>
Maganin samfurin: 80 mg/mL a cikin 6 N hydrochloric acid
Sharuɗɗan karɓa: +20.4° zuwa +21.4°
RASHIN RASHI <731>: bushe samfurin a 105 ℃ na 3 h: yana rasa NMT 0.4% na nauyinsa.
KARIN BUKATA
KYAUTA DA AJIYA: Ajiye a cikin kwantena da aka rufe sosai.
MATSAYIN NAZARI NA USP <11>
USP Arginine Hydrochloride RS
USP L-Lysine Hydrochloride RS
L-(+) - Lysine Monohydrochloride (CAS: 657-27-2) Hanyar Gwajin JP17
L-Lysine Hydrochloride, lokacin da aka bushe, ya ƙunshi ba kasa da 98.5% na L-lysine hydrochloride (C6H14N2O2.HCl).
Bayanin L-Lysine Hydrochloride yana faruwa azaman farin foda.Yana da ɗanɗano kaɗan, ɗanɗano halaye.
Yana iya narkewa cikin ruwa kuma a cikin formic acid, kuma a zahiri baya narkewa a cikin ethanol (95).
Yana nuna crystal polymorphism.
Identification (1) Ƙayyade nau'in shayarwar infrared na L-Lysine Hydrochloride, wanda aka bushe a baya, kamar yadda aka umarce shi a cikin hanyar faifan potassium bromide a ƙarƙashin Infrared Spectrophotometry <2.25>, kuma kwatanta bakan tare da Spectrum Reference: duka bakan suna nuna irin ƙarfin sha a. lambobin kalaman guda ɗaya.Idan wani bambanci ya bayyana tsakanin bakan, narke L-Lysine Hydrochloride a cikin ruwa, ƙafe ruwan zuwa bushewa a 60 ℃, kuma maimaita gwajin tare da ragowar.
(2) Maganin L-Lysine Hydrochloride (1 a cikin 10) yana amsawa ga Gwaje-gwaje masu inganci <1.09> don chloride.
Juyawar gani <2.49>[α]20/D: +19.0 - +21.5° (bayan bushewa, 2 g, 6 mol/L hydrochloric acid TS, 25 ml, 100 mm)
pH <2.54> Narke 1.0 g na L-Lysine Hydrochloride a cikin 10 ml na ruwa: pH na wannan maganin yana tsakanin 5.0 da 6.0.
Tsafta (1) Tsaftace da launi na bayani-Narke 1.0 g na L-Lysine Hydrochloride a cikin 10 ml na ruwa: bayani a bayyane yake kuma mara launi.
(2) Sulfate <1.14> -Yi gwajin tare da 0.6 g na L-Lysine Hydrochloride.Shirya maganin sarrafawa tare da 0.35 ml na 0.005 mol / L sulfuric acid VS (ba fiye da 0.028%) ba.
(3) Ammonium <1.02> -Yi gwajin tare da 0.25 g na L-Lysine Hydrochloride.Shirya maganin sarrafawa tare da 5.0 ml na Standard Ammonium Solution (ba fiye da 0.02%) ba.
(4) Karfe masu nauyi <1.07> - Ci gaba da 2.0 g na L-Lysine Hydrochloride bisa ga Hanyar 1, kuma yi gwajin.Shirya maganin sarrafawa tare da 2.0 ml na Maganin Gubar Daidaitawa (bai wuce 10 ppm ba).
(5) Arsenic <1.11> -Shirya maganin gwajin tare da 1.0 g na L-Lysine Hydrochloride bisa ga Hanyar 1, kuma yi gwajin (ba fiye da 2 ppm ba).
(6) Abubuwan da ke da alaƙa-Narke 0.10 g na L-Lysine Hydrochloride a cikin 25 ml na ruwa, kuma amfani da wannan maganin azaman maganin samfurin.Pipet 1 ml na maganin samfurin, ƙara ruwa don yin daidai 50 ml, pipet 5 ml na wannan maganin, ƙara ruwa don yin daidai 20 ml, kuma amfani da wannan maganin azaman daidaitaccen bayani.Yi gwajin tare da waɗannan mafita kamar yadda aka umurce su ƙarƙashin Thin-Layer Chromatography <2.03>.Spot 5μL kowane samfurin samfurin da daidaitaccen bayani akan farantin gel silica don chromatography na bakin ciki-Layer.Ci gaba da farantin tare da cakuda 1-propanol da ruwan ammonia (28) (67:33) zuwa nisa na kimanin 10 cm, kuma bushe farantin a 100 ℃ na minti 30.Fesa farantin a ko'ina tare da maganin ninhydrin a cikin acetone (1 a cikin 50) kuma zafi a 80 ℃ na minti 5: aibobi banda babban tabo daga maganin samfurin ba su da ƙarfi fiye da tabo daga daidaitaccen bayani.
Asarar bushewa <2.41> Ba fiye da 1.0% (1 g, 105 ℃, 3 hours).
Ragowa akan kunnawa <2.44> Bai wuce 0.1% ba (1 g).
Assay Yi nauyi daidai game da 0.1 g na L-Lysine Hydrochloride, wanda a baya busasshe, narkar da a cikin 2 ml na formic acid, ƙara daidai 15 ml na 0.1 mol/L perchloric acid VS, da zafi a kan wanka na ruwa na minti 30.Bayan sanyaya, ƙara 45 ml na acetic acid (100), kuma titrate <2.50> wuce haddi perchloric acid tare da 0.1 mol/L sodium acetate VS (potentiometric titration).Yi ƙudiri mara kyau, kuma a yi duk wani gyara da ya dace.
Kowane ml na 0.1 mol/L perchloric acid VS 9.132 MG na C6H14N2O2.HCl
Kwantena da Akwatunan ajiya - Kwantena masu tsauri.
Kunshin: Fluorinated Bottle, 25kg/bag, 25kg / Kwali Drum, ko bisa ga abokin ciniki ta bukata.
Yanayin Ajiya:Ajiye a cikin kwantena da aka rufe a wuri mai sanyi, bushe da iska mai nisa daga abubuwan da ba su dace ba.Kare daga haske da danshi.Ka nisantar da abubuwa masu ƙarfi masu ƙarfi.
Yadda ake siya?Da fatan za a tuntuɓiDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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Misali?Yawancin samfurori suna ba da samfurori kyauta don ƙima mai kyau, farashin jigilar kaya ya kamata a biya ta abokan ciniki.
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L- (+) Lysine Monohydrochloride (H-Lys-OH·HCl) (CAS: 657-27-2) ana amfani dashi sosai azaman kayan abinci mai gina jiki a masana'antar abinci da abin sha.Hakanan ana iya amfani dashi a cikin abincin dabbobi azaman tushen L-Lysine.Ana iya amfani da L-Lysine Monohydrochloride a cikin masana'antu iri-iri da suka haɗa da: samar da abinci, abin sha, magunguna, aikin gona/abincin dabbobi, da sauran masana'antu daban-daban.
Ayyuka & Aikace-aikace:
1. Lysine HCL wani abinci ne mai ƙarfafa abinci mai gina jiki, wanda ke da ayyuka na haɓaka ci na dabbobi da kaji, inganta juriya na cututtuka, inganta warkar da raunuka, inganta ingancin nama, inganta ƙwayar ciki, da kuma haɗakar da jijiyoyi na kwakwalwa, ƙwayoyin ƙwayoyin cuta, sunadarai da haemoglobin masu mahimmanci. abubuwa.Gabaɗaya adadin da aka ƙara a cikin abincin shine 0.1-0.2%.
2. Lysine HCL shine amino acid mai mahimmanci a cikin jikin mutum, wanda zai iya inganta aikin hematopoietic, inganta ƙwayar jijiyar ciki, ƙara yawan amfani da furotin, ƙara yawan juriya na cututtuka, kula da ma'auni na rayuwa, da kuma taimakawa wajen bunkasa ci gaban littafin sinadarai na yara na jiki da tunani.Kasar Sin ta kayyade cewa ana amfani da fulawa, biscuits da burodi da za a iya amfani da su wajen sarrafa noodles a cikin adadin 1 zuwa 2g/kg;0.3 zuwa 0.8g/kg a cikin ruwan sha.
3. Lysine HCL yana ɗaya daga cikin mahimman amino acid, kuma masana'antar amino acid yanzu ta zama masana'anta mai girma da mahimmanci.An fi amfani da Lysine a abinci, magani da abinci.
Aiki:
1. Matsayin abinci: kayan haɓaka abinci mai gina jiki, ana amfani da su don kayan yaji a cikin mayonnaise, madara, abinci na noodles nan take
2. Magani grade: shirye-shirye don fili amino acid transfusion, inganta yadda ya dace da kwayoyi
3. Matsayin ciyarwa: sanya ma'aunin abinci na kaji, inganta ingancin nama da yawan aiki
L- (+) - Lysine Monohydrochloride an samar da shi ne ta hanyar fermentation ta amfani da nau'in corynebacteria, musamman Corynebacterium glutamicum, wanda ya ƙunshi tsari mai yawa wanda ya hada da fermentation, rabuwar tantanin halitta ta hanyar centrifugation ko ultrafiltration, samfurin samfurin da tsarkakewa, evaporation da bushewa.Saboda L-Lysine mai girma da mahimmanci, ana yin ƙoƙari akai-akai don inganta hanyoyin fermentation, wanda ya ƙunshi nau'i da ci gaban tsari da kuma ingantawar kafofin watsa labaru da sarrafa ƙasa don samar da L-lysine da sauran L-amino acid. aiki a cikin hadawa tanki ko iska daga fermenters.
