Potassium Bis (trimethylsilyl) amide CAS 40949-94-8 (0.5M Magani a cikin Toluene)
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Sunan Sinadari | Potassium bis (trimethylsilyl) amide |
Makamantu | Hexamethyldisilazane Potassium Gishiri;Potassium hexamethyldisilazane;KHMDS |
Lambar CAS | 40949-94-8 |
Lambar CAT | Saukewa: RF-PI2227 |
Matsayin Hannun jari | A cikin Hannun jari, Ma'aunin samarwa Har zuwa Ton |
Tsarin kwayoyin halitta | Saukewa: C6H18KNSi2 |
Nauyin Kwayoyin Halitta | 199.49 |
Wurin Tafasa | 111 ℃ |
Yawan yawa | 0.877 g/ml a 25 ℃ |
Matsayin Hazard | 3 (8);Liquid mai flammable, Mai lalacewa |
Rukunin tattarawa | II |
Solubility | Miscible Tare da Terahydrofuran, Ether, Benzene da Toluene |
Ruwan Solubility | Yana Amsa Da Ruwa |
Hydrolytic Sensitivity | 8: Yana Amsa Gaggawa Tare da Danshi, Ruwa, Magungunan PProtic |
Kwanciyar hankali | Danshi Mai Mahimmanci, Mai Daukar iska, Jin zafi.Ajiye Karkashin Nitrogen.Zai iya Samar da Hazo.Yanayin yanayi. |
Tsaro | Mai Haɗari-Ƙarin Haɗarin Kayayyakin Cajin Kayan Abinci na iya Aiwatar |
Alamar | Ruifu Chemical |
Abu | Ƙayyadaddun bayanai |
Bayyanar | Jawo zuwa Ruwan Ruwa |
Sauran Najasa | ≤3.00% |
Abun ciki na Tushen Aiki | 0.45 ~ 0.55 M |
Matsayin Gwaji | Matsayin Kasuwanci |
Kunshin:Kwalba, ko bisa ga buƙatun abokin ciniki.
Yanayin Ajiya:Yana da kula da danshi da iska.Ajiye a wuri mai sanyi.Ajiye akwati sosai a rufe a cikin busasshen wuri kuma yana da isasshen iska.Akwatunan da aka buɗe dole ne a sake rufe su da kyau kuma a ajiye su a tsaye don hana zubewa.Sarrafa da adanawa a ƙarƙashin iskar inert.Wanda bai dace ba tare da magunguna masu ƙarfi masu ƙarfi.
Bayanin Hazard:Ruwa mai ƙonewa sosai da tururi.Yana haifar da kunar fata mai tsanani da lalacewar ido.Yana haifar da mummunar lalacewar ido.Wanda ake zargin yana lalata haihuwa ko yaron da ba a haifa ba.Zai iya haifar da lalacewa ga gabobin ta hanyar tsayin daka ko maimaita bayyanarwa.Zai iya haifar da bacci ko dizziness.
Potassium Bis (trimethylsilyl) amide (0.5M Magani a cikin Toluene) (wanda aka fi sani da KHMDS) (CAS: 40949-94-8) wani tushe ne mai ƙarfi, wanda ba na nucleophilic tare da pKa na kusan 26 (kwatankwacin lithium diisopropylamide, a 36). ).Ana samunsa ta kasuwanci azaman mai ƙarfi kuma azaman bayani a cikin nau'ikan kaushi iri-iri (misali THF, 2Me-THF, toluene, da MTBE).Similar reagents sun hada da lithium bis (trimethylsilyl) amide (LiHMDS) da sodium bis (trimethylsilyl) amide (NaHMDS).Ba-nucleophilic megasteric karfi tushe.Matsakaicin magunguna, ana amfani da su wajen samar da cephalosporins na roba.KHMDSwani sinadaran reagent ne da ake amfani da shi a cikin shirye-shiryen babban aiki na ruwa chromatography.Ana amfani da shi don samar da barga masu ƙarfi tare da potassium, wanda sai a raba shi da ginshiƙi.Hakanan ana amfani da KHMDS a cikin bincike na sinadarai kuma azaman mai haɓaka haɓakar asymmetric.KHMDS tushe ne mai ƙarfi da aka yi amfani da shi a cikin mahaɗan carbonyl alkylation.Ana amfani da KHMDS a cikin shirye-shiryen 5-Azacytidine, maganin antineoplastic.Hakanan ana amfani da shi a cikin shirye-shiryen agonists na β3-AR da aka yi amfani da su a cikin abubuwan hana damuwa.Hakanan ana amfani dashi azaman reagent a cikin shirye-shiryen hadaddun lanthanide da aka yi amfani da su a cikin halayen cyclization na zaɓi.