Potassium Bis(trimethylsilyl)amide CAS 40949-94-8 (0.5M Solution i Toluene)
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Inoa Kimia | Potassium Bis(trimethylsilyl)amide |
Nā huaʻōlelo like | Hexamethyldisilazane Potassium Salt;Hexamethyldisilazane ka pāpaʻa;KHMDS |
Helu CAS | 40949-94-8 |
Helu CAT | RF-PI2227 |
Kūlana Kūʻai | Ma ka waihona, hoʻonui ʻia a hiki i nā tona |
ʻĀpana Molekala | C6H18KNSi2 |
Kaumaha Molecular | 199.49 |
Lae paila | 111 ℃ |
ʻO ka mānoanoa | 0.877 g/mL ma 25 ℃ |
Papa Hazard | 3 (8);ʻO ka wai ʻaʻa, ʻino |
Hui Pūʻulu | II |
Ka hikiwawe | Miscible me Terahydrofuran, Etera, Benzene a me Toluene |
Hiki i ka wai | Pane me ka wai |
Hydrolytic Sensitivity | 8: Hana wikiwiki me ka wai, ka wai, pProtic Solvents |
Paʻa | ʻO ka maʻemaʻe, ka ea, ka wela.Halekuai malalo o Nitrogen.Hiki ke hana i ka ua.Nā Mahana Kūlohelohe. |
Palekana | Hazardous-E pili ana ka uku ukana i nā ukana ʻino |
Brand | Kemika Ruifu |
'ikamu | Nā kikoʻī |
Ka nana aku | Melemele a Palaunu wai |
Nā mea haumia ʻē aʻe | ≤3.00% |
Maʻiʻo o ka Active Base | 0.45-0.55 M |
Kūlana hoʻāʻo | Kūlana ʻoihana |
Pūʻolo:ʻO ka'ōmole, aiʻole e like me ka makemake o ka mea kūʻai.
Kūlana mālama:He mea maʻalahi i ka makū a me ka ea.E mālama i kahi anuanu.E hoʻopaʻa paʻa i ka pahu ma kahi maloʻo a me ka makani maikaʻi.Pono e hoʻopaʻa hou ʻia nā pahu i wehe ʻia a hoʻopaʻa pololei ʻia e pale i ka leaka.E mālama a mālama ma lalo o ke kinoea inert.ʻAʻole kūpono me nā mea oxidizing ikaika.
Nā ʻōlelo hōʻino:ʻO ka wai wela a me ka mahu.Hoʻopilikia ka ʻili a me ka pōʻino o ka maka.Hoʻopilikia ka maka nui.Manaʻo ʻia no ka hōʻino ʻana i ka hānau ʻana a i ʻole ke keiki hānau ʻole.Hiki ke hoʻopōʻino i nā kino ma o ka loaʻa ʻana o ka lōʻihi a i ʻole ka ʻike pinepine ʻana.Hiki ke hoʻoulu a hiamoe paha.
ʻO ka Potassium Bis(trimethylsilyl)amide (0.5M Solution i Toluene) (hoʻopau pinepine ʻia ʻo KHMDS) (CAS: 40949-94-8) he kumu ikaika, non-nucleophilic me kahi pKa kokoke o 26 (hoʻohālikelike i ka lithium diisopropylamide, ma 36 ).Hiki ke kūʻaiʻia ma keʻano he paʻa a me ka hoʻonāʻana i nāʻano solvents (ex. THF, 2Me-THF, toluene, a me MTBE).ʻO nā reagents like me ka lithium bis(trimethylsilyl)amide (LiHMDS) a me ka sodium bis (trimethylsilyl)amide (NaHMDS).Non-nucleophilic megasteric kumu ikaika.ʻO nā lāʻau lapaʻau waena, hoʻohana ʻia i ka hana ʻana i nā cephalosporins synthetic.KHMDShe mea hoʻoheheʻe kemika i hoʻohana ʻia i ka chromatography wai hana kiʻekiʻe.Hoʻohana ʻia ia e hana i nā paʻakikī paʻa me ka potassium, a laila hoʻokaʻawale ʻia e ke kolamu.Hoʻohana ʻia ʻo KHMDS i ka noiʻi biochemical a ma ke ʻano he asymmetric synthesis catalyst.ʻO KHMDS kahi kumu ikaika i hoʻohana ʻia i nā pūhui carbonyl alkylation.Hoʻohana ʻia ʻo KHMDS i ka hoʻomākaukau ʻana o 5-Azacytidine, kahi lāʻau antineoplastic.Hoʻohana pū ʻia i ka hoʻomākaukau ʻana i nā agonists β3-AR i hoʻohana ʻia i nā hana anti-stress.Hoʻohana ʻia ʻo ia ma ke ʻano he reagent i ka hoʻomākaukau ʻana i nā paʻakikī lanthanide i hoʻohana ʻia i nā hopena cyclization koho.