β-Phenylethylamine (PEA) CAS 64-04-0 Kev Ntsuam Xyuas> 99.0% (GC) Hoobkas High Purity
Shanghai Ruifu Chemical Co., Ltd. yog cov chaw tsim khoom thiab cov chaw muag khoom ntawm β-Phenylethylamine (PEA) (CAS: 64-04-0) nrog cov khoom zoo.Peb tuaj yeem muab kev xa khoom thoob ntiaj teb, me me thiab ntau qhov ntau.Please contact: alvin@ruifuchem.com
Tshuaj npe | β-Phenylethylamine |
Synonyms | Phenethylamine;2-Phenylethylamine;PEA;1-Amino-2-Phenylethane |
Tshuag xwm txheej | Hauv Tshuag |
CAS Nr | 64-04-0 |
Molecular Formula | C8H11 N |
Molecular Luj | 121.18 Nws |
Melting Point | -60 ℃ (lit.) |
Boiling Point | 197.0 ~ 200.0 ℃ (lit.) |
Qhov ntom | 0.962 g / mL ntawm 20 ℃ (lit.) |
rhiab heev | Huab cua Sensitive |
Hom | Ruifu Tshuaj |
Yam khoom | Specifications |
Qhov tshwm sim | Colorless Oily Liquid, Tsis Siv Neeg Mechanical impurities |
Moisture (KF) | <0.50% |
Assay / Analysis Method | > 99.0% (GC) |
Qhov ceev (20 ℃) | 0.960 ~ 0.965 hli |
Refractive Index n20/D | 1.530-1.535 Nws |
Infrared Spectrum | Raws li tus qauv |
Test Standard | Enterprise Standard |
Kev siv | Pharmaceutical Intermediate;Cov tshuaj zoo |
Pob: Lub raj mis, Nruas, 25kg / Nruas, 180kg / Nruas, lossis raws li cov neeg siv khoom xav tau.
Cia txias:Khaws rau hauv cov thawv ntim khoom ntawm qhov chaw txias thiab qhuav;Tiv thaiv los ntawm lub teeb, noo noo.Yuav tsum tsis txhob muab khaws cia nrog cov khoom corrosive thiab cov khoom uas tawm corrosive gases lossis vapors.
4 Txoj kev xeem
4.1 Kev tshwm sim
Kev tshuaj xyuas qhov muag.
4.2 Kev txiav txim siab dawb huv
4.2.1 Reagents thiab cov ntaub ntawv
a) Nitrogen: purity tsis tsawg dua 99.9%, tom qab kev kho kom huv
b) Hydrogen: purity tsis tsawg dua 99.9%, tom qab kev kho kom huv
C) Cua: tom qab kev kho kom huv
4.2.2 Cov cuab yeej thiab cov cuab yeej siv
a) Gas chromatograph: rhiab heev thiab ruaj khov ua tau raws li qhov yuav tsum tau muaj ntawm GB / T9722;
Ntes: hydrogen nplaim taws ionization ntes;
Cov xim kem yog SE-54 nrog txoj kab uas hla ntawm 30m * 0.32mm * 0.4μm.
b) Kev ua cov ntaub ntawv: N2000 chemical workstation, siv cheeb tsam normalization txoj kev los xam cov feem pua ntawm cov khoom.
c) 10μm qauv.
4.2.3 Kev khiav hauj lwm tej yam kev mob rau roj chromatography
a) Gasification kub: 250 ℃;
b) Kev ntsuas kub: 220 ℃;
c) Kem kub: 160 ℃;
d) Carrier roj siab: 0.06MPa;
e) Hydrogen siab: 0.1MPa;
f) Cua siab: 0.2MPa;
g) Qauv txhaj tshuaj ntim: 0.2ul;
h) Lub sijhawm khaws cia: 2.693
Cov saum toj no yog cov kev ua haujlwm raug cai, cov neeg ua haujlwm tuaj yeem hloov kho kom tsim nyog raws li cov yam ntxwv ntawm cov cuab yeej, txhawm rau ua tiav cov txiaj ntsig sib cais zoo tshaj plaws.
4.2.4 Cov txheej txheem ntsuas
Nyob rau hauv cov xwm txheej saum toj no chromatographic, 0.2ul cov qauv tau muab rho tawm nrog 10ul sampler tom qab qhov ntsuas tau ruaj khov, thiab tau txais daim duab chromatographic.Lub purity ntawm β-phenylethylamine yog ntsuas los ntawm cheeb tsam normalization txoj kev.
4.2.5 Tso cai sib txawv
Qhov sib txawv ntawm ob qhov kev ntsuas qhov sib npaug tsis ntau tshaj 0.25%, thiab tus lej lej ntsuas tus nqi raug coj los ua qhov ntsuas ntsuas.
4.3 Kev txiav txim siab ntawm cov ntsiab lus pub dawb
Raws li JJF1070.
5 Cov kev cai xeem
5.1 β-Phenethylamine yuav tsum tau soj ntsuam los ntawm lub Hoobkas kev soj ntsuam zoo, thiab txuas nrog rau daim ntawv pov thawj ua ntej xa khoom.
5.2 Ib qho khoom siv hluav taws xob yuav tsum tau siv ua ib pawg, thiab txhua pawg ntawm cov khoom yuav tsum tsis pub ntau tshaj 1 tuj
5.3 Txoj Kev Sampling
Qauv raws li GB / T 6680-2003, tag nrho cov qauv tsis pub tsawg tshaj 50g.
5.4 Thaum lub sijhawm tshuaj xyuas, yog tias ib yam khoom tsis tsim nyog, nws raug tso cai coj mus kuaj ob lub pob ntawm cov khoom rau kev tshuaj xyuas.Yog tias tseem muaj ib qho kev ntsuas tsis tsim nyog hauv qhov kev tshuaj xyuas rov qab, cov khoom lag luam yuav raug txiav txim tias tsis tsim nyog.
Daim ntawv lo, ntim, thauj thiab khaws cia
6.1 Label
Cov khoom lag luam ntshiab yuav tsum tau luam tawm lossis muab tso rau ntawm lub ntim ntim, suav nrog cov npe khoom, purity, qib zoo, cov khoom lag luam ua tiav tus qauv, hnub tsim khoom, ntau tus lej, qhov hnyav tag nrho thiab cov ntsiab lus hnyav ntawm cov khoom.Cov duab kos yuav tsum ua raws li GB / T191.
6.2 Ntim
Yas nruas packing
6.3 Kev thauj mus los
Cov khoom tuaj yeem thauj tau los ntawm cov qauv siv thiab txhais tau tias, uas yuav tsum tsis txhob los nag, kub kub thiab foob pob hluav taws, thiab yuav tsum tsis txhob sib xyaw nrog cov khoom corrosive thiab cov khoom emitting corrosive gases lossis vapors.
6.4 Cia khoom
Cov khoom yuav tsum tau muab khaws cia rau hauv ib qho chaw txias, qhuav thiab yuav tsum tsis txhob muab khaws cia nrog cov khoom corrosive thiab cov khoom uas tawm corrosive gases lossis vapors.
64-04-0 - Kev pheej hmoo thiab kev nyab xeeb
Hazard Symbols C - Corrosive
Risk Codes R22 - Ua phem yog tias nqos
R34 - Ua rau kub hnyiab
Kev Nyab Xeeb Kev Nyab Xeeb S26 - Nyob rau hauv rooj plaub ntawm qhov muag, yaug tam sim ntawd nrog dej txaus thiab nrhiav kev kho mob.
S36/37/39 - Hnav cov khaub ncaws tiv thaiv, hnab looj tes thiab tiv thaiv qhov muag / ntsej muag.
S45 - Thaum muaj xwm txheej lossis yog tias koj tsis xis nyob, nrhiav kev kho mob tam sim ntawd (qhia daim ntawv lo thaum twg los tau.)
UN IDs UN 2922 8/PG 2
WGK Germany 1
RTECS SG8750000
FLUKA BRAND F CODE 9-23
TSCA Yes
HS Code 2921440000
Hazard Chav Kawm 8
Packing Group III
Toxicity LD50 qhov ncauj hauv Luav: 300 mg / kg
Shanghai Ruifu Chemical Co., Ltd. yog cov chaw tsim khoom thiab cov chaw muag khoom ntawm β-Phenylethylamine (PEA) (CAS: 64-04-0) nrog cov khoom zoo, dav siv hauv cov organic synthesis, synthesis ntawm cov tshuaj intermediates thiab zoo tshuaj synthesis.β-Phenylethylamine yog ib qho kev sib tw nruab nrab nrog ntau yam kev siv.β-Phenylethylamine muaj ntses tsw.β-Phenylethylamine yog ib qho tshuaj tsw qab amine, uas yog cov kua tsis muaj xim ntawm chav tsev kub.Nws yog soluble hauv dej, ethanol, thiab ether.Zoo ib yam li lwm cov amines uas tsis tshua muaj molecular, nws muaj cov ntxhiab tsw tsw.Thaum raug huab cua, nws tsim cov khoom siv ntsev carbonate nrog carbon dioxide.Phenethylamine yog ib qho yooj yim heev thiab tsim ib tug ruaj khov crystalline hydrochloride ntsev nrog ib tug melting point ntawm 217 oC.Phenethylamine kuj yog cov tawv nqaij khaus thiab ua tau sensitizer.Phenethylamine kuj muaj ib qho kev cai lij choj isomer (+)-phenylethylamine (1-phenylethylamine), uas muaj ob lub stereoisomers: (R)-(+)-1-phenylethylamine thiab (S)-(-)-1-phenylethylamine.