6-Aminohexanoic Acid CAS 60-32-2 (ε-aminocaproic Acid) Assay 98.5 ~ 100.5% Factory

6-Aminohexanoic Acid (ε-Aminocaproic Acid) (CAS: 60-32-2) Usoro ule AJI97
ε-Aminocaproic Acid, mgbe agbakọrọ na anhydrous ndabere, nwere ọ bụghị ihe na-erughị 98.5 percent na ọ bụghị ihe karịrị 100.5 percent nke Aminocaproic Acid (C6H13NO2).
Nkọwa: kristal ọcha ma ọ bụ ntụ ntụ kristal, uto dị ilu.
Na-agbaze kpamkpam na mmiri yana n'ime glacial acetic acid, soluble na methanol, ọ fọrọ nke nta ka ọ bụrụ ihe a na-adịghị ahụkebe na ethanol.
Solubility (H2O, g/100g): Na-agbaze kpamkpam na mmiri
Nchọpụta: Tụlee ụdị nnabata infrared nke ihe nlele ahụ na nke ọkọlọtọ site na usoro diski bromide potassium.
Nkọwapụta:
Ọnọdụ Ngwọta (Nfefe): 0.5g na 10ml nke H2O, spectrophotometer, 430nm, ọkpụrụkpụ sel 10mm.
Chloride (Cl): 0.7g, A-1, ntụgharị: 0.40ml nke 0.01mol/L HCl
Ammonium (NH4): B-1
Sulfate (SO4): 1.2g, (1), ntụgharị: 0.50ml nke 0.005mol/L H2SO4
Ígwè (Fe): 0.5g, ntụgharị: 1.5ml nke Ígwè Std.(0.01mg/ml)
Ọla dị arọ (Pb): 2.0g, (1), pH=7, ntụgharị: 2.0ml nke Pb Std.(0.01mg/ml)
Arsenic (As2O3): 2.0g, (1), ntụgharị: 2.0ml nke As2O3 Std.
Amino acid ndị ọzọ: Nnwale ule: 100μg, B-1-a, njikwa;ε-Acp 0.6μg
Mmiri: 500mg, methanol: ethyleneglycol (1:2) maka usoro Karl Fischer, A, maka nkeji iri na ise.
Ihe fọdụrụ na mgbanye (Sulfated): AJI Test 13
Nyocha: Sample gbakọrọ na anhydrous ndabere, 130mg, (1), 3ml nke formic acid, 50ml nke glacial acetic acid, 0.1mol/L HCLO4 1ml=13.117mg C6H13NO2
pH: 1.0g na 10ml nke H2O
Oke nchekwa akwadoro na ọnọdụ: arịa ndị siri ike echekwara na ụlọ okpomọkụ a na-achịkwa (afọ 2).

6-Aminohexanoic Acid (ε-Aminocaproic Acid) (CAS: 60-32-2) Ule ule USP35
Aminocaproic acid nwere ihe na-erughị 98.5 pasent na ọ bụghị karịa 101.5 pasent nke C6H13NO2, gbakọọ na anhydrous ndabere.
Nkwakọ ngwaahịa na nchekwa - Chekwaa n'ime akpa siri ike.Na-echekwa na ụlọ okpomọkụ.
Ụkpụrụ ntụaka USP <11>-
USP Aminocaproic acid RS
Identification, Infrared Absorption <197K>.
Mmiri, Usoro m <921>: ọ bụghị karịa 0.5%.
Ihe fọdụrụ na mgbanye <281>: ọ bụghị karịa 0.1%.
Ọla dị arọ, Usoro II <231>: 0.002%.
Nyocha -
Ngwọta A- Nyefee 0.55 g nke sodium 1-heptanesulfonate na 1000-mL volumetric flask, gbazee na mmiri na-atụgharị na mmiri na olu, na mix.
Usoro mkpanaaka - Nyefee 10 g nke monobasic potassium phosphate na beaker 1000-mL, gbazee na 300 ml nke Ngwọta A, tinye 250 ml nke methanol, na-esote 300 ml ọzọ nke Ngwọta A, na mix.Gbanwee ngwakọta na phosphoric acid na pH nke 2.2.Nyefee ngwakọta dum na 1000-mL volumetric flask, gbanye ya na Ngwọta A na olu, na mix.Nyo na degas.Mee mgbanwe ma ọ bụrụ na ọ dị mkpa (lee Dabara Sistemu n'okpuru Chromatography <621>).
Ihe ngwọta dị n'ime - Kwadebe ngwọta nke methionine n'ime mmiri nwere 1.25 mg kwa ml.
Nkwadebe ọkọlọtọ-Gbasa oke USP Aminocaproic Acid RS nke a tụrụ n'ụzọ ziri ezi n'ime mmiri iji nweta ihe ngwọta ngwaahịa nwere njiri mara nke 12.5 mg kwa ml.Nyefee 5.0 ml nke ihe ngwọta nke ngwaahịa na 100-mL volumetric flask, tinye 2.0 ml nke ihe ngwọta nke Internal, gbanye mmiri na olu, ma gwakọta ya.
Nkwadebe nyocha-Bugharịa ọnụọgụ nke 1.25 g Aminocaproic Acid a tụrụ n'ụzọ ziri ezi na flask volumetric 100-mL, gbazee ma gbanye mmiri ka ọ bụrụ olu, wee gwakọta ya.Nyefee 5.0 ml nke ngwọta a na 100-mL volumetric flask, tinye 2.0mL nke Internal ọkọlọtọ ngwọta, gbanye na mmiri na olu, na mix.
Usoro Chromatographic (lee Chromatography <621>) -Kromatograph mmiri mmiri nwere ihe nchọpụta 210-nm na kọlụm 4.6-mm × 15-cm nke nwere ngwugwu L1 ma na-edobe ya na 30°.Onu ogugu bu ihe dika 0.7 ml kwa nkeji.Chromatograph the Standard nkwadebe, na dekọọ nzaghachi kacha elu dị ka eduzi maka Usoro: oge ​​njide ikwu ihe dị ka 0.76 maka aminocaproic acid na 1.0 maka methionine;Mkpebi, R, n'etiti aminocaproic acid na methionine abụghị ihe na-erughị 2.0;na ndị ikwu ọkọlọtọ ndiiche maka oyiri injections abụghị ihe karịrị 2.0%.
Usoro-iche iche, gbanye nha nha nha (ihe dịka 20 µL) nke nkwado ọkọlọtọ na nkwadebe Assay n'ime chromatograph, ma kwe ka nkwadebe Assay pụta maka ihe na-erughị ugboro abụọ n'oge njide aminocaproic acid.Dekọọ chromatogram, ma tụọ nzaghachi kacha elu.Gbakọọ ọnụọgụ, na g, nke C6H13NO2 n'ime akụkụ Aminocaproic Acid nke usoro a were were:
2C (RU / RS)
nke C bụ ntinye uche, na mg kwa ml, nke USP Aminocaproic Acid RS na nkwadebe Standard;na RU na RS bụ oke nke nzaghachi aminocaproic acid na nzaghachi ọnụ ọgụgụ dị n'ime nke enwetara site na nkwadebe Assay na nkwado ọkọlọtọ, n'otu n'otu.