Bacitracin Zinc CAS 1405-89-6 Ike ≥70 IU/mg Ụlọ ọrụ Antibiotic Peptide
Shanghai Ruifu Chemical Co., Ltd bụ onye na-emepụta ihe na onye na-ebubata Bacitracin Zinc (Zinc Bacitracin) (CAS: 1405-89-6) nwere oke mma.Anyị nwere ike ịnye COA, nnyefe zuru ụwa ọnụ, obere na nnukwu ọnụọgụ dị.Ọ bụrụ na ị nwere mmasị na Bacitracin Zinc (Zinc Bacitracin),Please contact: alvin@ruifuchem.com
| Aha Chemical | Bacitracin Zinc |
| Ụdị okwu | Bacitracin Zinc Nnu;Zinc Bacitracin |
| Ọnọdụ Ahịa | N'ahịa, ikike nrụpụta 10 tọn kwa afọ |
| Nọmba CAS | 1405-89-6 |
| Usoro ihe omimi | C66H101N17O16SZn |
| Ibu molekụla | 1486.07 |
| Ebe Na-agbaze | 250 ℃ (Dec.) |
| Mmiri Solubility | 5.1 g/L |
| COA & MSDS | Dị |
| Ihe atụ | Dị |
| Ụdị | Ruifu Chemical |
| Ihe | Nkọwapụta | Nsonaazụ |
| Ọdịdị | Ọcha ma ọ bụ Light Yellow-Gray ma ọ bụ Beige ntụ ntụ | Dabara |
| njirimara | Zute ihe ndị a chọrọ | Pụta mmeghachi omume dị mma |
| pH | 6.0-7.5 | 7.1 |
| Ọnwụ na ihicha | ≤5.0% | 2.7% |
| Zinc (ihe akpọnwụwo) | 4.0% ~ 6.0% | 4.20% |
| Ike | ≥70 IU/mg Microbial Assay (Akpọrọ nkụ) | 71 IU/mg |
| Ọdịnaya nke Bacitracin A | ≥40.0% | 58.2% |
| Ọdịnaya nke Bacitracin nọ n'ọrụ | ≥70.0% (Bacitracin A, B1, B2, na B3) | 86.1% |
| Oke nke Peptides n'oge mbụ | ≤20.0% | 7.6% |
| Mbelata nke Bacitracin F | ≤6.0% | 1.1% |
| Ngụkọta ọnụ ọgụgụ ikuku ikuku nwere ike ime | <100 CFU/gram | Dabara |
| Mmechi | Ngwaahịa ahụ dabara na ụkpụrụ USP44 | |
| Isi ojiji | Ọgwụ nje peptide | |
ngwugwu:Kalama, Aluminom foil bag, 25kg / Cardboard Drum, ma ọ bụ dị ka ndị ahịa chọrọ.
Ọnọdụ Nchekwa:Debe akpa ahụ nke ọma ma chekwaa n'ebe dị jụụ, kpọrọ nkụ (2 ~ 8 ℃) yana ụlọ nkwakọba ihe nke ọma na-esi na ihe ndị na-adabaghị adaba.Chebe site na ìhè na mmiri mmiri.
Mbupu:Jiri ikuku na-ebuga ụwa niile site na FedEx / DHL Express.Nye nnyefe ngwa ngwa na ntụkwasị obi.
Bacitracins, mgbagwoju zinc.
Bacitracins zinc complexes [1405-89-6].
» Bacitracin Zinc bụ zinc complex nke bacitracin, nke mejupụtara ngwakọta nke antimicrobial polypeptides, ihe ndị bụ isi bụ bacitracins A, B1, B2, na B3.Ọ nwere ike na-erughị 65 Bacitracin Units kwa mg, gbakọọ na akpọnwụwo ndabere.O nwere ihe na-erughị 4.0 pasent na ọ bụghị ihe karịrị 6.0 pasent nke zinc (Zn), gbakọọ na a mịrị amị ndabere.
Nkwakọ ngwaahịa na nchekwa - Chekwaa n'ime akpa siri ike, ma chekwaa n'ebe dị mma.
Ịkpọ aha-kpọ aha ya iji gosi na a ga-eji ya mee naanị ọgwụ ndị na-abụghị ndị nne na nna.N'ebe a na-achịkọta ya maka ịgbakọta ndenye ọgwụ, kpọọ ya ka ọ gosi na ọ bụghị ike ime nakwa na ike ahụ enweghị ike ijide n'aka ruo ogologo oge karịa ụbọchị 60 ka emepechara, na ikwupụta ọnụọgụ Bacitracin kwa milligram.N'ebe e bu n'obi ka e jiri ya mee ihe n'ịkwadebe ụdị usoro onunu ogwu, akara ahụ na-ekwu na ọ dịghị mma ma ọ bụ na a ga-edozi ya n'ihu nhazi n'oge nkwadebe nke ụdị usoro onunu ogwu.
Ụkpụrụ ntụaka USP <11>-
USP Bacitracin Zinc RS
njirimara-
A: Nnwale njirimara Chromatographic nke dị larịị <201BNP>: na-emezu ihe achọrọ.
B: Ọ na-emezu ihe achọrọ nke usoro chromatographic mmiri mmiri na ule maka ihe mejupụtara.
Sterility <71>-Ebe akara ahụ na-ekwu na ọ dị ọcha, ọ na-emezu ihe achọrọ mgbe a nwalere ya dị ka akwadoro maka nzacha Membrane n'okpuru Nnwale maka Sterility nke ngwaahịa a ga-enyocha, belụsọ iji Fluid A na L nke ọ bụla agbakwunyere 20. g nke edetate disodium.
pH <791>: n'etiti 6.0 na 7.5, na ngwọta (juputara) nwere ihe dịka 100 mg kwa ml.
Ọnwụ na ihicha <731>-Kọ ihe dịka 100 mg na karama capillary-stoppered na oghere na 60 maka awa 3: ọ na-efunahụ karịa 5.0% nke ibu ya.
Ọdịnaya Zinc- [ndeba ama-Nkwadebe ọkọlọtọ na nkwadebe ule nwere ike iji 0.001 N hydrochloric acid mee ya nke ọma, ma ọ bụrụ na ọ dị mkpa, iji nweta azịza nke mkpokọta kwesịrị ekwesị, na-agbanwe na linear ma ọ bụ ụdị ọrụ nke akụrụngwa.]
Nkwadebe ọkọlọtọ- Nyefee 3.11 g nke zinc oxide, nke a tụrụ nke ọma, na flask volumetric 250-mL, tinye 80 ml nke 1 N hydrochloric acid, na-ekpo ọkụ ka igbari, dị jụụ, gbanye mmiri na olu, na mix.Ihe ngwọta a nwere 10 mg nke zinc kwa ml.Tinyegharịa ihe ngwọta a na 0.001 N hydrochloric acid iji nweta nkwadebe ọkọlọtọ nwere 0.5, 1.5, na 2.5 µg nke zinc kwa ml, n'otu n'otu.
Nkwadebe nwale - Nyefee ihe dịka 200 mg nke Zinc Bacitracin, nke a tụrụ nke ọma, gaa na flask volumetric 100-mL.Gbanyụọ na 0.01 N hydrochloric acid, gbanye ya na otu ihe mgbaze na olu, na mix.Pipet 2 ml nke ihe ngwọta a n'ime 200-mL volumetric flask, gbanye na 0.001 N hydrochloric acid ka olu, na mix.
Usoro-Concomitantly chọpụta absorbances nke Standard nkwadebe na Nnwale Nkwadebe na zinc resonance ahịrị nke 213.8 nm, na kwesịrị ekwesị atomiki absorption spectrophotometer (lee Spectrophotometry na Light-agbasa <851>), onwem na zinc oghere-cathode oriọna na ire ọkụ ikuku-acetylene, na-eji 0.001 N hydrochloric acid dị ka oghere.Chee echiche banyere nnabata nke ọkọlọtọ Standard na itinye uche, na µg kwa ml, nke zinc, wee see ahịrị kwụ ọtọ nke dabara adaba na isi ihe atọ a kpara nkata.Site na eserese nke enwetara, chọpụta ntinye, na µg kwa ml, nke zinc na nkwadebe ule.Gbakọọ ọdịnaya nke zinc, na pasent, n'akụkụ Bacitracin Zinc nke usoro a were were:
1000C / W
nke C bụ ntinye na µg kwa ml, nke zinc na nkwadebe ule;na W bụ ibu, na mg, nke akụkụ Bacitracin Zinc were.
Ihe mejupụtara -
Ihe nchekwa - gbazee 34.8 g nke potassium phosphate, dibasic, na 1 l mmiri.Gbanwee na 27.2 g nke potassium phosphate, monobasic, etisasịwo na 1 L mmiri, na pH nke 6.0.
Usoro mkpanaaka - Kwadebe ngwakọta nke methanol, mmiri, ihe nchekwa, na acetonitrile (26:15:5:2).Mix ọma, na degas.
Diluent-gbari 40 g nke edetate disodium na 1 l mmiri.Gbanwee na itughari sodium hydroxide na pH nke 7.0.
Ngwọta kwesịrị ekwesị nke sistemu - gbazee ọnụọgụ USP Bacitracin Zinc RS nke a tụrụ n'ụzọ ziri ezi na diluent iji nweta ngwọta nwere ntinye aha nke ihe dịka 2.0 mg kwa ml.
Ngwọta ọnụ ụzọ na-akọ akụkọ-Gbagharịa n'ụzọ dị iche iche, jiri mmiri, olu kwesịrị ekwesị nke ngwọta dabara adaba na sistemụ iji nweta ngwọta nwere ntinye ama ama nke 0.01 mg kwa ml.
Ngwọta njirimara kacha elu - gbazee ọnụọgụ USP Bacitracin Zinc RS tụrụ atụ n'ime oke diluent kwesịrị ekwesị iji nweta ngwọta nwere ntinye aha nke ihe dịka 2.0 mg kwa ml.Kpoo ọkụ na mmiri esi mmiri saa maka nkeji iri atọ.Jụụ ruo ụlọ okpomọkụ.
Ngwọta nwale-Kwụsa Zinc Bacitracin a tụrụ n'ụzọ ziri ezi na diluent iji nweta ngwọta nwere ntinye aha nke ihe dịka 2.0 mg kwa ml.
Usoro Chromatographic (lee Chromatography <621>) -Kromatograph mmiri mmiri nwere ihe nchọta nnabata yana kọlụm 4.6- × 250-mm nwere ngwụcha nke nwere 5-µm mbukota L1.Onu ogugu mmiri bu 1.0 ml kwa nkeji.Tọọ ogologo wavelength nke ihe nchọpụta na 300 nm.Tinye ihe dị ka 100 µL nke ngwọta njirimara Peak, wee chọpụta ebe bacitracin F dị, nke bụ adịghị ọcha a ma ama, na-eji oge njide ikwu na-egosi na Tebụl 1.
Tebụl 1
Oge njide dị n'akụkụ aha (ihe dị ka)
Bacitracin C1 0.5
Bacitracin C2 0.6
Bacitracin C3 0.6
Bacitracin B1 0.7
Bacitracin B2 0.7
Bacitracin B3 0.8
Bacitracin A 1.0
Bacitracin F 2.4
Gbanwee ogologo wavelength nke ihe nchọpụta wee tọọ ya na 254 nm.Chromatograph nke dabara adaba nke sistemu, wee dekọọ nzaghachi kacha elu dị ka akwadoro maka Usoro: chọpụta ọnụ ọgụgụ kacha arụ ọrụ nke bacitracin (bacitracins A, B1, B2 na B3), peptides na-ebulite ngwa ngwa (ndị na-apụ n'ihu n'ihu elu n'ihi bacitracin B1). ) na adịghị ọcha, bacitracin F, na-eji oge njigide oge enyere na Tebụl 1. Gbakọọ ọnụ ọgụgụ kasị elu na ndagwurugwu site na iji usoro:
Hp / HV
nke Hp dị elu n'elu ntọala nke elu n'ihi bacitracin B1;na HV bụ ịdị elu n'elu ntọala nke ebe kachasị ala nke mgbanaka na-ekewa bacitracin B1 elu site na ọnụ ọgụgụ kasị elu n'ihi bacitracin B2.Ọnụ ọgụgụ kasị elu na ndagwurugwu erughị 1.2.
Usoro-iche iche, gbanye mpịakọta nha nha (100 µL) nke ihe nrịbama, ngwọta nnwale, na ngwọta ọnụ ụzọ mkpesa.Dekọọ chromatograms ihe dị ka ugboro atọ oge njide nke bacitracin A. Chọpụta ọnụ ọgụgụ kachasị elu site na iji oge njide ikwu na-egosi na Tebụl 1. Tulee ebe kachasị elu nke ọnụ ọgụgụ niile na ngwọta ule.[mara-Nleghara anya elu ọ bụla na ngwọta Nnwale na-enwe mpaghara na-erughị ebe bacitracin A ọnụ ọgụgụ kasị elu na nkwubi okwu ngwọta;leghara ọnụ ọgụgụ ọ bụla a hụrụ na Diluent anya.]
ndetu-Mkpokọta mpaghara na mgbako ndị a ka akọwara dị ka mpaghara ọnụ ọgụgụ kacha elu ma ewezuga oke mkpesa.
ọdịnaya nke bacitracin a-gbakọọ pasent nke bacitracin A site na iji usoro:
(rA/Mkpokọta mpaghara) × 100
nke rA bụ nzaghachi mpaghara sitere na bacitracin A. Bacitracin A ọdịnaya erughị 40.0% nke mkpokọta mpaghara.
Ọdịnaya nke bacitracin na-arụ ọrụ-gbakọọ pasent nke bacitracin na-arụ ọrụ (bacitracin A, B1, B2, na B3) site na iji usoro:
(rA + rB1 + rB2 + rB3 / mkpokọta mpaghara) × 100
nke rA, rB1, rB2, na rB3 bụ nzaghachi mpaghara sitere na bacitracin A, B1, B2, na B3, n'otu n'otu.Nchikota bacitracin A, B1, B2, na B3 erughị 70.0% nke mkpokọta mpaghara.
njedebe nke peptides n'oge-gbakọọ pasent nke ọnụ ọgụgụ kasị elu na-apụta tupu elu n'ihi bacitracin B1 site na iji usoro:
(rPreB1 / mkpokọta mpaghara) × 100
N'ime nke rPreB1 bụ nchikota nzaghachi nke ọnụ ọgụgụ kasị elu na-apụta tupu ọnụ ọgụgụ kasị elu maka bacitracin B1.Oke nke peptides n'oge (ndị na-ebuli elu n'ihu elu n'ihi bacitracin B1) abụghị ihe karịrị 20.0%.
njedebe nke bacitracin f- Gbakọọ pasent bacitracin F site na iji usoro:
100 × (rF / rA)
nke rF bụ nzaghachi nke bacitracin F sitere na ngwọta ule;na rA bụ nzaghachi nke bacitracin A sitere na ngwọta ule.Oke bacitracin F, adịghị ọcha amara, erughị 6.0%.
Nyochaa-Gaa n'ihu na Bacitracin Zinc dị ka eduzi ya n'okpuru Antibiotics-Microbial Assays 81.
Kedu ka esi azụta?Biko kpọtụrụDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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Koodu mpaghara:: 2941909099
A na-ewepụta Bacitracin site na ngwọta omenala nke lichen (Bacillus licheniformis) ma bụrụ ọgwụ nje polypeptide.Ọcha ọcha ma ọ bụ ntụ ntụ na-acha odo odo, enweghị isi ma ọ bụ na-esi ísì ụtọ, uto ilu, hygroscopic.Dị mfe soluble na mmiri na ethanol, ejighị n'aka, aqueous ngwọta na-adị mfe inactivated na ụlọ okpomọkụ, ejighị n'aka na pH 9, na kwesịrị refrigerated na refrjiraeto mgbe mgbasa.A na-agbakọ ngwaahịa a dị ka ngwaahịa kpọrọ nkụ, na titer kwa milligram agaghị erughị nkeji 55 bacitracin.Bacitracin zinc bụ bacitracin zinc nnu, nke kwụsiri ike karịa bacitracin.A na-eji ya dị ka ihe mgbakwunye nri ma nwee ọrụ nke ịkwalite uto na mmepe nke anụ ụlọ na anụ ọkụkọ, igbochi ọrịa eriri afọ, na ịba ụba ụgwọ nri nri.Usoro onunu ogwu a bu bacitracin.Ụdị nje bacteria Bacitracin yiri penicillin, nke nwere mmetụta antibacterial siri ike na nje bacteria gram-positive na enweghị mmetụta doro anya na nje bacteria gram-adịghị mma.Maka ọrịa siri ike nke Staphylococcus aureus na-eguzogide ọgwụ.A naghị etinye ọnụ nchịkwa ọnụ ma jiri ya mee ihe maka ọrịa eriri afọ.Ojiji nke mpụga na-adịkwa irè maka elu ahụ, ọnụ na ọrịa anya na mastitis nke nje bacteria na-enwe mmetụta na-akpata.Nwere mmetụta na-emebi emebi na akụrụ.A na-eji Bacitracin zinc mee ihe dị ka ihe mgbakwunye ọgwụ nri.A naghị etinye aka na nchịkwa ọnụ, n'ihi ya, a na-ekwenyekarị na ọ dịghị nsogbu ọgwụ fọdụrụnụ na anụ ụlọ na anụ ọkụkọ.Ngwaahịa a bụ ọgwụ nje dị warara dị warara, nke nwere mmetụta antibacterial siri ike na ọtụtụ nje gram-positive.Ọ dịkwa irè megide spirochetes na actinomycetes, mana ọ naghị arụ ọrụ megide nje bacteria gram-adịghị mma.Ọ nwere mmetụta synergistic na ọgwụ nje dị iche iche dị ka penicillin G, streptomycin, neomycin, polymyxin, wdg. A na-ejikarị nnu zinc eme ihe dị ka ihe mgbakwunye nri, nke nwere ọrụ nke igbochi ọrịa eriri afọ, na-akwalite uto na imeziwanye ụgwọ ọrụ nri.Nje bacteria nwere ike jiri nwayọọ nwayọọ malite iguzogide ngwaahịa a, mana enweghị mgbochi n'etiti ngwaahịa a na ọgwụ nje ndị ọzọ.Ngwaahịa a dị oke nsi na enweghị ike ịgba ya.Enwere ike were ya n'ọnụ iji gwọọ afọ ọsịsa nje na anụ ụlọ yana ọnyụnyụ Treponema na ezi.N'ụlọ ọgwụ, a na-ejikarị ya na ọgwụ nje dị iche iche dị ka penicillin, streptomycin, neomycin, polymyxin B, wdg. iji mee ka ọ dị irè.
Bacitracin Zinc bụ mgbagwoju anya nke bacitracin na zinc ion hibere.ọ bụ ọgwụ nje polypeptide na ọ bụ ihe mgbakwunye nri ọgwụ nje a na-ejikarị eme ihe ugbu a.zinc ọdịnaya bụ n'ozuzu 2% ~ 12%.Ngwaahịa sịntetik na-acha ọcha ma ọ bụ ntụ ntụ, na-esi ísì pụrụ iche, dị mfe igbari n'ime ihe ndị na-adịghị ike alkaline, na-adị mfe soluble na mmiri, methanol na ethanol.Bacitracin zinc nwere mmetụta antibacterial siri ike megide nje bacteria gram-positive, ma nweekwa ihe na-egbu egbu megide ụfọdụ nje bacteria gram-adịghị mma.Ojiji zinc bacitracin na nri nri zuru oke nwere ike ịkwalite ọnụego uto, melite ụgwọ ọrụ nri, ma gbochie afọ ọsịsa nke nje na ọrịa iku ume na-adịghị ala ala.Mgbakwunye mgbakwunye na-abụkarị 10 ~ 100mg / kg, na mmetụta adịghị eme ka ọ dịkwuo mma karịa mgbakwunye mgbakwunye.Bacitracin Zinc anaghị etinye aka na eriri afọ ezi, yabụ na ọ nweghị nsogbu ọ bụla fọdụrụnụ.Ọ bụ ihe mgbakwunye nje na-echekwa na a pụrụ ịdabere na ya.Bacitracin Zinc na-egbu egbu nke ukwuu na eriri afọ anaghị etinye ya ngwa ngwa, yabụ enweghị ike iji ya dịka ọgwụgwọ maka ọrịa sistemu.
Ọgwụ nje polypeptide nwere mmetụta antibacterial siri ike na nje bacteria gram-positive, ma nwee mmetụta antibacterial na nje bacteria ole na ole gram-adịghị mma, spirochetes, actinomycetes na ọbụna staphylococci na-eguzogide penicillin.Usoro nje bacteria bụ igbochi nguzobe nke mgbidi cell nje ma mebie akpụkpọ ahụ plasma cell nke nje bacteria.Ọ nwere ike ịkwalite uto nke microorganisms bara uru na eriri afọ, na-abawanye permeability nke mucosa eriri afọ, ma kwalite nnabata nke nri.A na-ejikarị akwalite uto nke anụ ụlọ na anụ ọkụkọ, igbochi na ịchịkwa afọ ọsịsa nke anụ ụlọ na anụ ọkụkọ na ọnyụnyụ ọbara nke Treponema kpatara.Bacitracin zinc anaghị etinye uche n'ime ya, ọtụtụ n'ime ya na-esikwa na nsị n'ime ụbọchị 2, n'ihi ya, ọ dịghị mfe ịnọgide na anụ ụlọ na anụ ọkụkọ;nje bacteria na-adịkarịghị etolite iguzogide bacitracin, na enweghị mgbochi mgbochi na ọgwụ nje ndị ọzọ, ma nwee mmetụta synergistic na penicillin, streptomycin, neomycin, aureomycin, polymyxin, wdg. Ngwaahịa a dị oke nsi na enweghị ike ịgbanye ya.Akwụsịla ngwaahịa a na olaquindox, kitasamycin, virginiamycin na Enramycin.
Dị ka ndepụta mgbakwunye, a na-ejikarị eme ihe iji kwalite uto anụ ụlọ na anụ ọkụkọ, gbochie afọ ọsịsa nje nke anụ ụlọ na anụ ọkụkọ na ọnyụnyụ ọbara nke treponema kpatara.Bacitracin zinc anaghị etinye uche n'ime ya, ọtụtụ n'ime ya na-esikwa na nsị n'ime ụbọchị 2, n'ihi ya, ọ dịghị mfe ịnọgide na anụ ụlọ na anụ ọkụkọ;nje bacteria na-adịkarịghị etolite iguzogide bacitracin, na enweghị mgbochi mgbochi na ọgwụ nje ndị ọzọ, ma nwee mmetụta synergistic na penicillin, streptomycin, neomycin, aureomycin, polymyxin, wdg. Ngwaahịa a dị oke nsi na enweghị ike ịgbanye ya.Akwụsịla ngwaahịa a na olaquindox, kitasamycin, virginiamycin na Enramycin.
Bacitracin Zinc bụ ọgwụ nje polypeptide, nke nwere mmetụta nje na nje bacteria gram-positive.Usoro ya bụ tumadi igbochi nje mgbidi njikọ nke nje bacteria, na nwekwara ike ikpokọta na cell akpụkpọ ahụ nke mmetụta nje bacteria, imebi iguzosi ike n'ezi ihe nke cell akpụkpọ ahụ, na-eme ka The outflow nke dị mkpa bekee na cell.Na-egbochi nje bacteria gram-positive na ụfọdụ nje gram-adịghị mma;Ọnụ ọgụgụ nke iguzogide nje bacteria na bacitracin zinc na-adị nwayọọ, ọ dịghịkwa ihe mgbochi na ọgwụ nje ndị ọzọ.Ọgwụ nje polypeptide na-egbochi dephosphorylation nke lipid pyrophosphate, si otú a na-egbochi njikọ nke mgbidi cell nje.
