(Boc) 2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Dị Ọcha>99.0% (HPLC) Ụlọ ọrụ na-echebe Reagent egosipụtara

(Boc) 2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Dị Ọcha>99.0% (HPLC) Ụlọ ọrụ Nchekwa Reagent

Nkọwa dị mkpirikpi:

Aha Chemical: Di-tert-Butyl Iminodicarboxylate

Ụdị okwu: (Boc)2NH;N-Boc-tert-Butylcarbamate

Nọmba: 51779-32-9

Dị ọcha:> 99.0% (HPLC)

Ọdịdị: White Crystalline ntụ ntụ

Nchekwa Reagent, Ogo dị elu

Kpọtụrụ: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

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Nkọwa ngwaahịa

Ngwaahịa ndị emetụtara

Mkpado ngwaahịa

Nkọwa:

Shanghai Ruifu Chemical Co., Ltd bụ onye na-emepụta Di-tert-Butyl Iminodicarboxylate ((Boc) 2NH) (CAS: 51779-32-9) na elu mma.Ruifu Chemical na-enye usoro nchekwa reagents na reagents njikọ.Anyị nwere ike ịnye nnyefe zuru ụwa ọnụ, ọnụahịa asọmpi, obere na nnukwu ọnụọgụ dị.Ịzụta Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com

Njirimara kemịkalụ:

Aha Chemical	Di-tert-Butyl Iminodicarboxylate
Ụdị okwu	(Boc)2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic acid Di-tert-Butyl Ester;Bis (tert-butoxycarbonyl) amonia
Ọnọdụ Ahịa	Dị na ngwaahịa
Nọmba CAS	51779-32-9
Usoro ihe omimi	C10H19NO4
Ibu molekụla	217.27 g/mol
Ebe Na-agbaze	114.0 ~ 120.0 ℃
Njupụta	1.037±0.06 g/cm3
Mmetụta	Mmetụta ikuku, Mmetụta ọkụ
Mmiri Solubility	Na-adịghị edozi n'ime mmiri
Solubility	Chloroform, methanol
Okpomọkụ nchekwa.	Ebe dị jụụ na nkụ (2 ~ 8 ℃)
COA & MSDS	Dị
Otu	Nchekwa Reagent
Ụdị	Ruifu Chemical

Nkọwapụta:

Ihe	Ụkpụrụ nyocha	Nsonaazụ
Ọdịdị	White Crystalline ntụ ntụ	Na-akwado
Ebe Na-agbaze	114.0 ~ 120.0 ℃	118.8-119.3 ℃
Ọnwụ na ihicha	<0.50%	0.10%
Ụzọ ịdị ọcha / nyocha	> 99.0% (HPLC)	99.6%
Spectrum infrared	Dabara na Ọdịdị	Na-akwado
Ọnụ ego nke NMR Spectrum	Dabara na Ọdịdị	Na-akwado
Mmechi	A nwalela ngwaahịa a wee kwado nkọwa ndị enyere

Nnwale ịdị ọcha:

Kọlụm Chromatographic: SE-54 30m×0.25mm ×0.5μm;
Ihe nchọpụta: FID
Okpomọkụ mbụ: 100 ℃
Oge mbido: 1 nkeji
Ọnụ ọkụ: 20 ℃ / min
Okpomọkụ ikpeazụ: 190 ℃
N'ikpeazụ: 10min
Okpomọkụ igba ogwu: 160 ℃
Okpomọkụ nke ihe nchọpụta: 200 ℃
Oke nkewa: 50:1;
Nlele nha: 0.2μl;
Ihe ngwọta: methanol
Nsonaazụ: Ịdị ọcha karịrị 99.0% site na usoro nhazi mpaghara.

Ngwugwu/Nkwakọba/Mbupu:

ngwugwu:Kalama, Aluminom foil bag, 25kg / Cardboard Drum, ma ọ bụ dị ka ndị ahịa chọrọ.
Ọnọdụ Nchekwa:Chekwaa n'ime akpa mkpuchi mkpuchi n'ụlọ nkwakọba ihe dị jụụ na nkụ (2 ~ 8 ℃) pụọ na ihe ndị na-ekwekọghị ekwekọ.Chebe site na ìhè na mmiri mmiri.
Mbupu:Nyefee n'ụwa niile site na FedEx / DHL Express.Nye nnyefe ngwa ngwa na ntụkwasị obi.

Uru:

Ike zuru oke: akụrụngwa na ndị ọrụ nka zuru oke

Ọrụ Ọkachamara: Otu nkwụsị ịzụrụ ọrụ

Ihe ngwugwu OEM: ngwugwu omenala na akara dị

Nnyefe ngwa ngwa: Ọ bụrụ n'ime ngwaahịa, ekwenyere nnyefe ụbọchị atọ

Nkwanye kwụsiri ike: Jikwaa ngwaahịa ezi uche dị na ya

Nkwado nka na ụzụ: Ngwọta teknụzụ dị

Ọrụ Synthesis Custom: sitere na gram ruo kilos

Ogo dị elu: guzobe usoro mmesi obi ike zuru oke

Ajụjụ:

Kedu ka esi azụta?Biko kpọtụrụDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

Ahụmịhe afọ 15?Anyị nwere ihe karịrị 15 afọ nke ahụmahụ na mmepụta na mbupụ nke a dịgasị iche iche nke elu mma pharmaceutical intermediates ma ọ bụ ezi kemịkal.

Isi ahịa?Na-ere ahịa ụlọ, North America, Europe, India, Korea, Japanese, Australia, wdg.

Uru?Ogo kachasị elu, ọnụ ahịa dị ọnụ ala, ọrụ ọkachamara na nkwado teknụzụ, nnyefe ngwa ngwa.

OgoNkwenye?Usoro njikwa mma siri ike.Ngwá ọrụ ọkachamara maka nyocha gụnyere NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, wdg.

Ihe atụ?Ọtụtụ ngwaahịa na-enye ihe nlele efu maka nyocha dị mma, ndị ahịa kwesịrị ịkwụ ụgwọ mbupu.

Nyocha ụlọ ọrụ?Nnabata nyocha ụlọ ọrụ.Biko mee oge oge tupu oge eruo.

MOQ?Enweghị MOQ.A na-anabata obere usoro.

Oge Mbuga ozi? Ọ bụrụ n'ime ngwaahịa, ekwenyere nnyefe ụbọchị atọ.

Ụgbọ njem?Site Express (FedEx, DHL), nke ikuku, site n'oké osimiri.

Akwụkwọ?Mgbe ọrụ ahịa gasịrị: COA, MOA, ROS, MSDS, wdg nwere ike ịnye.

Synthesis omenala?Nwere ike ịnye ọrụ nhazi ahaziri iche ka ọ dabara mkpa nyocha gị nke ọma.

Usoro ịkwụ ụgwọ?A ga-ebu ụzọ ziga akwụkwọ ọnụahịa Proforma mgbe nkwenye nke iwu, kpuchiri ozi ụlọ akụ anyị.Ịkwụ ụgwọ site na T/T (Telex Nyefee), PayPal, Western Union, wdg.

51779-32-9 - Ihe ize ndụ na nchekwa:

Ihe akara egwu Xi - iwe
Koodu ihe ize ndụ 36/37/38 - na-akpasu anya, sistem iku ume na akpụkpọ ahụ.
Nkọwa nchekwa S26 - Ọ bụrụ na ị na-ahụ anya, jiri mmiri buru ibu sachaa ozugbo wee chọọ ndụmọdụ ahụike.
S37/39 - Yiri uwe aka kwesịrị ekwesị na nchebe anya / ihu
WGK Germany 3
Koodu mpaghara:: 29241990
Ihe ndetu Hazard na-ewe iwe

Ngwa:

Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Ngwa Di-tert-Butyl Iminodicarboxylate bụ etiti ọgwụ, nke enwere ike ịkwadebe site na mmeghachi omume otu nzọụkwụ nke formamide na Boc2O.
A na-eji ogige ahụ dị ka reagent maka nkwadebe nke amines nke sitere na alkyl halides.A kwalitere ya dị ka ihe ọzọ na njikọ Gabriel maka otu ntụgharị ahụ.Enwere ike ịkwadebe Amines site na mmanya na-egbu egbu site na akpịrị ịkpọ nkụ site na iji mmeghachi omume Mitsunobu.Na mmejuputa a na-emebu, a na-ewepụ reagent iji nye nnu potassium, nke bụ N-alkylated.A na-ewepụkwa otu nchekwa Boc n'okpuru ọnọdụ acid.
Di-tert-Butyl Iminodicarboxylate bụ otu amine echedoro nke a na-eji akwadebe spirocycles na-agbanwe agbanwe dịka ndị na-emegide CCR1.
Nkwadebe ihe ngwọta nke DMAP (0.61g, 5.0mmol) na MeCN (15ml) ji nwayọọ nwayọọ na-agbakwunye na ngwọta nke foramide (2.5g,56mmol) na Boc2O (24).g, 110mol) na MeCN (15ml).Mgbe ọ gbasasịrị n'ime ụlọ okpomọkụ maka awa 4, a na-eme ka ihe ngwọta na-acha odo odo dị jụụ ka ọ bụrụ 0 Celsius C, na N, N-diethylenediamine (6.97g, 60mmol) ji nwayọọ nwayọọ tinye ya na 0 ℃.A na-eme ka ngwakọta a na-esi na ya pụta na ụlọ okpomọkụ maka 12h ma kpochaa site na mpempe silica dị mkpa;A na-enyocha ngwakọta nke sitere na ụlọ okpomọkụ.A na-ekpochapụ ihe mgbaze n'okpuru nrụgide belatara.Ejiri silica gel chromatography sachaa ngwaahịa crude a wee jiri EtOAc nweta ya/ hexane (1: 5) iji nweta ngwaahịa aha, nke bụ ọcha siri ike (10.99g, 92%).