Fmoc-Gly-OH CAS 29022-11-5 Fmoc-Glycine Dị ọcha> Ụlọ ọrụ 99.0% (HPLC)
Shanghai Ruifu Chemical Co., Ltd bụ onye na-emepụta Fmoc-Glycine (Fmoc-Gly-OH) (CAS: 29022-11-5) nwere oke mma.Ruifu Chemical na-enye usoro amino asịd.Anyị na-enye nnyefe zuru ụwa ọnụ, ọnụahịa asọmpi, obere na nnukwu ọnụọgụ dị.Ịzụta Fmoc-Glycine,Please contact: alvin@ruifuchem.com
Aha Chemical | Fmoc-glycine |
Ụdị okwu | Fmoc-Gly-OH;N-Fmoc-Glycine;Fmoc-L-glycine;Fmoc-L-Gly-OH;N-[(9H-Fluoren-9-ylmethoxy) carbonyl] glycine;N- (9-Fluorenylmethoxycarbonyl) - Glycine |
Ọnọdụ Ahịa | N'ahịa, Ikike Mmepụta Tọn 20 kwa ọnwa |
Nọmba CAS | 29022-11-5 |
Usoro ihe omimi | C17H15NO4 |
Ibu molekụla | 297.31 g/mol |
Ebe Na-agbaze | 165.0 ~ 185.0 ℃ |
Njupụta | 1.316 |
Solubility na methanol | Ihe fọrọ nke nta ka ọ bụrụ nghọta |
Okpomọkụ nchekwa. | Ebe dị jụụ na nkụ (2 ~ 8 ℃) |
COA & MSDS | Dị |
Otu | Fmoc-amino acid |
Ụdị | Ruifu Chemical |
Ihe | Ụkpụrụ nyocha | Nsonaazụ |
Ọdịdị | Ọcha ntụ ntụ | Ọcha ntụ ntụ |
Ụzọ ịdị ọcha / nyocha | > 99.0% (HPLC) | 99.85% |
Ebe Na-agbaze | 165.0 ~ 185.0 ℃ | 177.0 ~ 177.1 ℃ |
Mmiri nke Karl Fischer | <0.50% | 0.26% |
Ngwọta doo anya | 0.3 gram na 2ml DMF Clear Solution | Na-akwado |
Fmoc-β-Ala-OH | <0.10% (HPLC) | Na-akwado |
Fmoc-β-Ala-Gly-OH | <0.10% (HPLC) | Na-akwado |
Fmoc-Gly-Gly-OH | <0.10% (HPLC) | Na-akwado |
Fmoc-Val-OH | <0.10% (HPLC) | Na-akwado |
Fmoc-Ala-OH | <0.10% (HPLC) | Na-akwado |
Fmoc-Leu-OH | <0.10% (HPLC) | Na-akwado |
Fmoc-lle-OH | <0.10% (HPLC) | Na-akwado |
Ọdịghị ọcha ọ bụla akọwapụtaghị | <0.20% (HPLC) | Na-akwado |
Amino acid n'efu | <0.20% (GC) | Na-akwado |
Ethyl acetate | <0.50% (GC) | Na-akwado |
Mass Spectrum | N'ikwekọ na Standard | Na-akwado |
Ọnụ ego nke NMR Spectrum | N'ikwekọ na Standard | Na-akwado |
Mmechi | A nwalela ngwaahịa a wee kwado nkọwa ndị enyere |
ngwugwu: Fluorinated Bottle, Aluminom foil bag, 25kg / Cardboard Drum, ma ọ bụ dị ka ndị ahịa chọrọ.
Ọnọdụ Nchekwa:Chekwaa n'ime akpa mkpuchi mkpuchi n'ụlọ nkwakọba ihe dị jụụ na nkụ (2 ~ 8 ℃) pụọ na ihe ndị na-ekwekọghị ekwekọ.Chebe site na ìhè na mmiri mmiri.
Kedu ka esi azụta?Biko kpọtụrụDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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Fmoc-Glycine (Fmoc-Gly-OH) (CAS: 29022-11-5) bụ ụdị Glycine echekwara N-Fmoc.Glycine bụ amino acid na-adịghị mkpa.Fmoc-amino acid, eji na peptide njikọ, eji dị ka ihe organic synthesis intermediate, pharmaceutical intermediate, biochemical reagent ma ọ bụ kemịkalụ reagent.
Okwu mmalite: Fmoc-Glycine bụ Glycine na-echebe site na Fmoc.Fluorene methoxycarbonyl (Fmoc) bụ otu nchebe na-eche nche, nke enwere ike iji na mmiri amonia ma ọ bụ dioxane-methanol-4N NaOH (30: 9: 1) na piperidine, ethanolamine, cyclohexylamine, 1,4-Dioxane, pyrrolidone na ọzọ amonia 50% dichloromethane ngwọta.N'okpuru ọnọdụ alkaline adịghị ike dị ka sodium carbonate ma ọ bụ sodium bicarbonate, Fmoc-Cl ma ọ bụ Fmoc-OSu na-ebute otu nchekwa Fmoc.
Ngwa: Fmoc-Glycine bụ Fmoc-echebe Glycine, nke a na-ejikarị eme polypeptides.Ọdịiche nke otu nchebe amino acid nwere mmetụta dị ukwuu na arụmọrụ na mkpụrụ nke njikọ polypeptide.Dịka ọmụmaatụ, enwere ike iji Fmoc-Glycine kwadebe ihe mgbochi corrosion na-emepụta glycine, na otu Fmoc-echebe na ogologo ogologo hydrophobic na-ejikọta ya na molekul Glycine site na mmeghachi omume amidation, na heteroatom (N, O, wdg) ma ọ bụ. unsaturated bonds) na mgbanaka bisphenyl nwere π electrons na-adaba na metal, na ogologo ogologo hydrophobic na-egbochi ụmụ irighiri mmiri, nke mere na ọ na-emepụta ihe nkiri nchebe n'elu ígwè iji nweta nzube nke nchebe corrosion.
Nkwadebe: Fmoc-Glycine njikọ kpọmkwem nzọụkwụ bụ ndị a: 3.0g Glycine na-etisasịwo na 115ml nke 10% Na2CO3, mma ka -4 ~ 0℃,11.2g Fmoc-Cl etisasịwo na 35.0ml nke acetone na gbakwunyere na usoro dropwise, Mgbe mgbakwunye na dropwise, na-akpali na ice bat maka 30min, wee na-akpali na ụlọ okpomọkụ maka 2.0h.A na-enyocha ọganihu mmeghachi omume site na chromatography nke dị obere.Mgbe emechara mmeghachi omume ahụ, a na-awụsa mmiri 400ml n'ime mmiri, a na-amịpụta ether ugboro abụọ, mee ka ọ dị jụụ ma dozie ya na pH2 na hydrochloric acid na-etinye uche, nnukwu ihe siri ike na-acha ọcha na-ekpo ọkụ, 50 ml nke ethyl acetate wepụtara ugboro atọ, magnesium na-ekpo ọkụ. sulfate akpọnwụwo, a na-agbaze ihe mgbaze n'okpuru nrụgide belatara, a na-eji ether petroleum mee ihe iji nweta 11.5g nke Fmoc-Glycine.Mgbe emechara ọcha, ịdị ọcha nke ngwaahịa ahụ bụ 97.35% site na arụmọrụ chromatography mmiri dị elu.