L-Leucine Methyl Ester Hydrochloride CAS 7517-19-3 (H-Leu-OMe·HCl) Nyocha > Ụlọ ọrụ 99.0%
Shanghai Ruifu Chemical Co., Ltd bụ onye na-emepụta L-Leucine Methyl Ester Hydrochloride (H-Leu-OMe·HCl) (CAS: 7517-19-3) nwere oke mma.Ruifu Chemical na-enye amino acids na ihe nrụpụta, nwere ike ịnye nnyefe zuru ụwa ọnụ, obere na nnukwu dị.Ọ bụrụ na ịchọrọ ya,Please contact: alvin@ruifuchem.com
Aha Chemical | L-Leucine Methyl Ester Hydrochloride |
Ụdị okwu | H-Leu-OMe·HCl;L-Leu-OMe·HCl;L-Leucine Methyl Ester HCl;Methyl L-Leucinate Hydrochloride;(S) -2-Amino-4-Methyl-Pentanoic Acid Methyl Ester Hydrochloride;(S) - Leucine Methyl Ester Hydrochloride;Leucine Methyl Ester Hydrochloride;Methyl (S) -2-Amino-4-Methylpentanoate Hydrochloride;Methyl (S) - Leucinate Hydrochloride |
Ọnọdụ Ahịa | N'ahịa, Ikike Mmepụta Tọn 30 kwa ọnwa |
Nọmba CAS | 7517-19-3 |
Usoro ihe omimi | C7H15NO2 · HCl |
Ibu molekụla | 181.66 |
Ebe Na-agbaze | 148.0 ~ 150.0 ℃ |
Mmetụta | Hygroscopic |
Mmiri Solubility | Soluble na Mmiri |
Okpomọkụ nchekwa. | Okpomọkụ ụlọ |
Mbupu | Nkịtị |
COA & MSDS | Dị |
Nhazi | Amino Acids na mmepụta |
Ụdị | Ruifu Chemical |
Koodu egwu | Xi | WGK Germany | 3 |
Nkwupụta ihe egwu | 36/37/38 | Klas Hazard | Iwe |
Nkwupụta nchekwa | 22-24/25-36/37/39-27-26 | Koodu HS | 2922491990 |
WGK Germany | 3 |
Ihe | Ụkpụrụ nyocha | Nsonaazụ |
Ọdịdị | Microcrystalline ntụ ntụ na-acha ọcha ma ọ bụ gbanyụọ | Dabara |
Ntụgharị a kapịrị ọnụ [α]20/D | +12.0° ruo +14.0°(C=2 na H2O) | +13.0° |
Ebe Na-agbaze | 148.0 ~ 150.0 ℃ | 148.0 ~ 150.0 ℃ |
300 MHz 1H-NMR ụdịdị dị iche iche | Dakọtara na Standard | Na-agbanwe agbanwe |
Nyocha TLC | Otu ntụpọ | Dabara |
Ọnwụ na ihicha | <0.50% | 0.21% |
Sulfate ntụ ntụ | <0.20% | 0.11% |
D-Enantiomer | <0.50% | Dabara |
Ihe Amonia anaghị ebuli ya | <0.50% | Dabara |
Nyocha | > 99.0% | 99.2% |
Solubility na Mmiri | Dị ọcha ma ọ bụ ntakịrị uzuzu (50mg / ml) | Dabara |
Mmechi | Ngwaahịa a site na nkwekọrịta nyocha na ọkọlọtọ ụlọ ọrụ | |
Isi ojiji | Amino acids na mmepụta ihe;Ndị na-ahụ maka ọgwụ |
1. Ọdịdị
Were ngwaahịa a kwesịrị ekwesị, tinye ya na akwụkwọ ọcha na-acha ọcha ma gbasaa 5 cm2 na 5 mm.Lelee ya na ebe na-egbuke egbuke.
2. Ịdị ọcha (HPLC)
2.1 Ngwa
chromatography mmiri mmiri na-arụ ọrụ dị elu, ihe nchọpụta PDA.
Ntụle nyocha eletrọnịkị
2.2 Reagent
Acetonitrile (ọkwa chromatographic), TFA (ọkwa chromatographic)
2.3 Ọnọdụ chromatographic
2.3.1 Ogidi: YMC-ODS-AM, 5 μl, 150 x 4.6 mm
2.3.2
Ogologo oge nchọpụta: INC220nm
Onu ogugu: 1.0ml/min
Olu ogwu ogbugba: 10 μL (maka ntụaka)
Ihe ngwọta: acetonitrile
Oge ịgba ọsọ: nkeji 20
2.4 Mobile usoro nkwadebe
Usoro mkpanaka A (0.1% mmiri trifluoroacetic acid): na-amịkọrọ 2.0ml TFA nke ọma, gbanye 2000ml na mmiri, mix na degas;
Usoro mkpanaaka B (0.1% trifluoroacetic acid acetonitrile): na-amịkọrọ 2.0ml TFA nke ọma, gbanye 2000ml na acetonitrile, mix na degas;
2.5 akụrụngwa akụrụngwa
Oge (nkeji) A% B%
0.00 90 10
12.00 10 90
15.00 10 90
15.01 90 10
20.00 90 10
2.6 Nkwadebe nke ngwọta sample
Tụọ ma gbarie 0.1g sample na acetonitrile, itughari ka 100ml, maa jijiji nke ọma maka ojiji, ma ọ bụ otu itinye uche.Kwadebe ihe atụ abụọ n'otu aka ahụ.
2.7 Nnwale mkpebi
Nyochaa ihe nlele ahụ dịka usoro nlele ndị a si dị:
Ihe kariri ogwu ogwu efu 1
1 ihe ngwọta nke agịga 1 #
1 ihe ngwọta nke agịga 2 #
2.8 Mgbakọ nsonaazụ
2.8.1 A na-eji usoro nhazi nke mpaghara kacha elu iji gbakọọ ịdị ọcha HPLC site n'iwepụ oghere oghere.
2.8.2 Ntugharị ikwu nke ịdị ọcha nke agịga abụọ agaghị adị karịa 1%
2.8.3 Ọ bụrụ na nsonaazụ nke injections abụọ ahụ na-agbaso ụkpụrụ nnabata, a na-ewere nkezi ịdị ọcha dị ka nsonaazụ ikpeazụ.
3, Ebe mgbaze -- RY-1 ihe mgbaze
4. Ọnwụ na usoro nyocha ihicha
4.1 Ngwa:
Igwe ọkụ ọkụ ọkụ eletrik, nguzozi 1/10,000.
4.2 Usoro:
N'ime karama na-atụ ihe dị larịị nke nwere ịdị arọ mgbe niile yana mkpuchi ọnụ ala na-akpọnwụ, tụọ gram 1 (nke ruru 0.0001 gram) nke nlele.The sample kwesịrị evenly gbasaa na ala nke arọ karama na a ọkpụrụkpụ nke ọ dịghị ihe karịrị 10mm, tinye na a thermostatic electric ihicha oven, nkụ na 105 ~ 110 ℃ maka 3 awa, wee banye n'ime ihicha ụlọ ka ajụkwa ka. ọnụ ụlọ okpomọkụ maka ịtụ.
Mgbakọ: Ọnwụ na ihicha %= (M1-M2) ÷M×100
Ebe: M1: arọ nke sample na karama nha tupu ihicha, gram
M2: ịdị arọ nke sample na karama atụ mgbe akpọchara, na gram
Nna-ukwu: Ịdị arọ, gram
5. Ntughari pụrụ iche
-- Specific ntụgharị ka a tụrụ dị ka GB/T613-1988 si dị
Nkwadebe ihe atụ: 1.0000g sample tụrụ n'ụzọ ziri ezi ma kwaga na karama volumetric 50ml dị ọcha ma kpọọ nkụ, 20ml mmiri gbakwunyere, karama ahụ kpuchie ma maa jijiji ka ọ gbazee, wee gbanye ya na mmiri.
Nnwale: Gbanwee efu nke gyroscope tupu ule ahụ, wee buo tube ule ahụ na ngwọta nlele, dekọọ akụkụ ntụgharị, wee gbakọọ ntụgharị a kapịrị ọnụ nke nlele ahụ na usoro a.
[a]D20 = (r×50) ÷ (L×W)
[а] D20: Ntugharị ngwa anya akọwapụtara na 20 ℃ nke ngwọta nlele
r: Ntugharị anya hụrụ na 20 ℃ maka ngwọta nlele
50: Mpịakọta nke ngwọta sample akwadoro (ml)
w: Nlereanya arọ (g)
L: Ogologo tube ntụgharị anya (dm)
ngwugwu: Fluorinated Bottle, Aluminom foil bag, 25kg / Cardboard Drum, ma ọ bụ dị ka ndị ahịa chọrọ.
Ọnọdụ Nchekwa:Chekwaa n'ime akpa mechiri emechi n'ụlọ nkwakọba ihe dị jụụ, kpọrọ nkụ na ikuku ikuku na-anọghị n'ihe na-ekwekọghị ekwekọ.Chebe site na ìhè na mmiri mmiri.
Kedu ka esi azụta?Biko kpọtụrụDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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L-Leucine Methyl Ester Hydrochloride (H-Leu-OMe·HCl) (CAS: 7517-19-3) bụ ihe nrụpụta leucine, nke a na-eji maka reagents biochemical, etiti ọgwụ.A na-eji Amino acid na amino acid eme ihe n'ahịa dị ka ndị na-ahụ maka ọgwụ na ụlọ ọrụ na-emepụta ọgwụ, ndị mmadụ na-etinyekwu uche na amino acids.