1-Methyl-3-Pyrrolidinol CAS 13220-33-2 Puritas >98.0% (GC)

Description:

Nomen chemicum: 1-Methyl-3-Pyrrolidinol

Synonyma: 3-Hydroxy-I-Methylpyrrolidine

CAS: 13220-33-2

Puritas: >98.0% (GC)

Aspectus: Lux Yellow Liquid

Contactus: Dr

Mobile/Wechat/Whatsapp: +86-15026746401

E-Mail: alvin@ruifuchem.com

Mitte ad nos inscriptio

Product Detail

Product Tags

Descriptio:

Ruifu Chemical est primarium opificem 1-Methyl-3-pyrrolidinoli (3-Hydroxy-1-Methylpyrrolidinis) (CAS: 13220-33-2) magna qualitate.Ruifu Chemical traditio totius terrarum, quantitatis competitive pretium, optimum servitium, parvas et moles in promptu habere potest.Purchase 1-Methyl-3-Pyrrolidinol,Please contact: alvin@ruifuchem.com

Chemical Properties:

Nomen chemicum	1-Methyl-3-Pyrrolidinol
Synonyma	N-Methyl-3-Pyrrolidinol;3-Hydroxy-1-Methylpyrrolidine;N-Methyl-Pyrrolidin-3-ol;N-Methyl-Pyrrolidinyl Alcohol;1-Methylpyrrolidin-3-ol
Stock Status	In Stock, Commercial Productio
CAS Number	13220-33-2
Formulae hypotheticae	C5H11NO
M. Pondus	101.15 g/mol
Ferveret	75℃/12 mmHg
Mico punctum	71℃
Density	0.921 g/mL ad 25℃ (lit.)
Index refractivus n20/D	1.464(lit.)
Sensitiva	Aer Sensitivus, Hygroscopic
Solubilitas	Solutum in aqua, solutum in Alcohol, Aether et Benzene
COA & MSDS	Praesto
Sample	Praesto
Origin	Shanghai, China
Brand	Ruifu Chemical

Specifications:

Items	Signa inspectionis	Proventus
Aspectus	Lux Yellow Liquid	Lux Yellow Liquid
Aquae Caroli Fischer	<0.20%	0.15%
Puritas / Analysis Methodus	>98.0% (GC)	98.57%
Densitas (20℃)	0.920~0.923	Obsequitur
Index refractivus n20/D	1.463~1.465	Obsequitur
Infrared Imaginis	Congruunt Structure	Obsequitur
1H NMR Imaginum	Congruunt Structure	Obsequitur
conclusio	Productum probatum est & obsequitur datis specificationibus

Sarcina / at /naviportans:

Sarcina:Utrem, aluminium foil, sacculum, 25kg/cardboard Drum, vel secundum exigentiam emptoris.

Repono Condition:Continentem arcte clausam et in loco frigido, sicco (2~8℃) reponunt et a cellis bene ventilatis ab substantiis incompossibilibus.A luce et humore protege.
Naviportans:Libera ad mundum ab aere, per FedEx / DHL Express.Ieiunium et certas traditiones provide.

13220-33-2 - Synthetica Route:

13220-33-2 - Methodus praeparationis;

1,2,4-Butanetriolum aceticum aceticum ad ollam reactionem, movendum et calorem ad 100 circiter, adde gas chloridum siccum, et ad 90~ 110' pro 30h, cum magna vis hydrogenii chloridi incepit. apparent in caudae gas, extremum punctum reactionis repressum est et hydrogenium chloride omissum est.Post refrigerationem, materia emissa est, solutione sodium sodium saturate abluta, et distillationis sub pressura reducta subiecta, et 120 ad 135℃.(12.6 ad 13. 3kPa) fractio, I .e., 1,4-Dichloro-2-Butanol materia pinguis, cede 50%~60%.
Cyclization aquea solutio 1,4-Dichloro-2-Butanol et Methylamina cyclizationi olla addita est, et ad 120℃ calefacta.Sub calefactione clausa, et per reactionem 10h commota est.Post refrigerationem, solida sodium hydroxidis adiecta est, et sal inorganicum praecipitatum eliquatum est.Stratum oleum separatum est et distillationis vacuum subiecta, et fractio 76-85℃.(2.1 kPa) opus factum esse coactum est.Extrac- tionis aquei cum benzene etiam portionem 1-Methyl-3-pyrrolidinol reddit.Fructus circiter 60% erat.
3. Key processuum:
3.1 Substitutus reactionem processum: reactionem control tempus et reactionem terminus deprehendere
3.2 Vacuum distillationis processum 1,4-Dichloro-2-Butanol: vacui gradus distillationis et fractionis temperaturae vacui.
3.3 cyclization reactionem processus: imperium reactionem temperatus et tempus
3.4 1-Methyl-3-Pyrrolidinolum processum vacuum distillationis: gradum control vacuum distillationis vacui et caloris fractionis
4. Qualitas puncta imperium:
Qualitas imperium punctum 1: 1,2,4-Butanetriol materia rudis qualitas vexillum
Quality control point 2: Central control quality standard for cyclization reaction .
Qualitas imperii punctum 3: 1,4-Dichloro-2-Butanol vexillum quale medium
Qualitas imperium punctum 4: 1-Methyl-3-pyrrolidinolum operis qualitas vexillum

13220-33-2 - Modus Test:

Humor Content: Hoc sume productum et proba secundum modum determinationis umoris (Prima methodus A APPENDIX M, 2010 Editio Pharmacopoeia Popularis Reipublicae Sinarum).Humor contentus non excedat 0.2%.
Densitas relativa: Densitas relativa productum (Appendix VI A partis II, 2010 editionis) est 0.920~0.923
Index refractivus: Index refractivus huius producti (Appendix VI F partis II editionis 2010) est 1.463~ 1.465
Contentum Determinatio: Contentum 1-Methyl-3-Pyrrolidinol non minus quam 98.0% per chromatographiam gasi (Appendix E, Pars II, 2010 editionis).
Columna: Capillaris in silica liquefacta SPB-5, diametro interna 0.32mm, longitudo 30m .
T Injector: 300℃
FID: 320℃
T Columna: 80℃ pro 5 minutis, 200℃ ad 5℃/m, deinde ad 200℃ pro 7 min
Carrier: Helium ad 1 ml/min
Discidium Ratio: 100:1
Iniectio: 1 microliter
Solutio test: solve 200mg specimen sub analysi in 10ml methanoli.Injicere 1 microliter.1µl in chromatographum gasi iniectum est, ut chromatogrammum notaret.Contentum 1-Methyl-3-pyrrolidinol computatum est per apicem area ordinationem methodi.

commoda:

Satis capacitas: sufficientes facilities et technici

Professional Service: One stop acquireing service

Altera Package: Custom sarcina ac titulus praesto

Ieiunium Delivery: Si intra stirpem, tres dies partus praestatur

Supple firmum: Esse rationabile stirpe

Technical Support: Technology solution praesto

Custom Synthesis Service: Range from P. to kilos

High Quality: Constitutus ratio completa qualitas certitudinis

FAQ:

Quam mercari?Quaeso contactumDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

15 Years Experience?Plus quam XV annos experientiae habemus in fabricando et exportando amplis intermediis pharmaceuticis vel alchimicis pharmaceuticis amplis.

Mercatus principalis?Vendere mercatum domesticum, Americam septentrionalem, Europam, Indiam, Coream, Iaponicam, Australiam etc.

Commodi?Superior qualitas, parabilis pretium, officia professionalia et subsidia technica, ieiunium partus.

Qualitasfides?Qualitas strictioris temperantiae ratio.Pro instrumento analysi professionali includuntur NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Claritas, Solubilitas, Microbialis limes test, etc.

Exempla?Pleraque producta praebent exempla gratuita pro qualitate aestimationis, sumptus naviculas a clientibus solvendos.

Factory Audit?Factory audit gratissimum.Quaeso ante constitutum.

MOQ?Nec MOQ.Parvus ordo placet.

Tempus adferendi? Si intus prosapia, tres dies partus praestatur.

Transportatio?Per Express (FedEx, DHL), ab Air, per Mare.

Documenta?Post servitium venditionis: COA, MOA, ROS, MSDS, etc. praeberi possunt.

Consuetudo Synthesis?Consuetudo synthesis officia praebere potest ad optimas investigationes tuas necessitates aptandas.

Pensio conditio?Proforma cautionis primum post confirmationem ordinis mittetur, informationes nostrae ripae inclusas.Payment by T/T (Telex Transfer), PayPal, Western Union, etc.

13220-33-2 - Periculum et Salus;

Periculosam symbola Xi - Irritant
Periculum Codes
36/37/38 - Irritando ad oculos, systema respiratorium et cutem.
Salus Descriptio
S26 - In contactu cum oculis, statim cum aqua multa ablue et consilium medicinae quaeras.
S36/37/39 - Indumentum tutelae idoneum, caestus et oculi/facies tutelam gerunt.
WGK Germania 3
HS Code 2933900099

13220-33-2 - Applicatio:

1-Methyl-3-pyrrolidinolum (3-Hydroxy-1-Methylpyrrolidinum) (CAS: 13220-33-2) adhibetur ut synthesis organica media, ut pharmaceutica media in pharmaceutica industria adhibita.