L-(+)-Lysine Monohydrochloridis CAS 657-27-2 (H-Lys-OH·HCl) Assay 98.5~ 101.0% Factory Hcl.
Shanghai Ruifu Chemical Co, Ltd. est primarius fabricae et supplementi L-(+)-Lysinae Monohydrochloridis (H-Lys-OH·HCl) (CAS: 657-27-2) cum magna qualitate, productione capacitatis 1000 tons per anno secundo.Ut una ex maximis amino acida in Sinis, Ruifu acida amino acida usque ad signa internationalia supplent, ut AJI, USP, EP, JP et FCC signa.CoA praebere possumus, totius orbis partus, parvas et parvas quantitates in promptu habentes.Si interest in L-(+)-Lysine Monohydrochloride,Please contact: alvin@ruifuchem.com
| Nomen chemicum | L-(+)-Lysine Monohydrochloride |
| Synonyma | H-Lys-OH·HCl;L-Lysine Monohydrochloride;L-Lysine Hydrochloride;L-Lysine HCl;Laevo-Lysine Hydrochloride;Lycopersicon esculentum;Triticum aestivum;(S)-2,6-Diaminohexanoicum Acidum Monohydrochloridum |
| Stock Status | In Stock, Productio Capacity 1000 Tons per Year |
| CAS Number | 657-27-2 |
| Formulae hypotheticae | C6H14N2O2·HCl |
| M. Pondus | 182.65 |
| Liquescens punctum | 263*(decl.)(decl.) |
| Density | 1.28 g/cm3 (20℃) |
| Aqua Solubility | Solutum in aqua, diaphanum prope |
| Solubilitas | Libere solutum in aqua et acido formica.Leviter solutum in Ethanol.Fere Insouble in Ether |
| Repono Nativ. | Signatus in siccis, Store in Room Temperature |
| COA & MSDS | Praesto |
| Classification | Amino Acidum et Derivativa |
| Brand | Ruifu Chemical |
| Periculum Codes | 34 - Causae urit |
| Salus Descriptio | S24/25 - contactus cum cute et oculis fuge. |
| Consociatione Nationum IDs | UN 1789 8/PG 3 |
| WGK Germania | 2 |
| HS Code* | 2922419000 |
| Items | Signa inspectionis | Proventus |
| Aspectus | Crystal aut Crystallina pulveris alba | Conforms |
| Lepidium sativum | Infrared effusio Imaginis | Conforms |
| Imprimis rotationis [α]20/D | +20.4° ad +21.4°(C=8 in 6N HCl) | +20.8° |
| Status Solutio (Transmittance) | Patet et hyalina ≥98.0% | 98.8% |
| Chloride (Cl) | 19.0 ad 19.6% | 19.15% |
| Sulfate (SO4) | ≤0.020% | <0.020% |
| Aconitum (NH4) | ≤0.020% | <0.020% |
| Ferrum (Fe) | ≤10ppm | <10ppm |
| Metalla gravia (Pb) | ≤10ppm | <10ppm |
| Arsenicum (As2O3) | ≤1.0ppm | <1.0ppm |
| Alia Amino Acids | ≤0.50% (TLC) | Conforms |
| Damnum in Siccatio | ≤0.40% (ad CV" pro III horas) | 0.25% |
| Residere in Ignition (Sulfated) | ≤0.10% | 0.06% |
| Assay | 98.5 ad 101.5% (sicut arida Basis) | 99.7% |
| Organicum volatile immunditias | Occurrit opus est | Conforms |
| PH Test | 5.0 ad 6.0 (1.0g in 10ml of H2O) | 5.2 |
| RELICTUM Solvents | Conforms | Conforms |
| conclusio | AJI97 occurrit cum vexillifero;USP;JP | |
| Fasciae vita | XXIV Menses ex Manufacture Date si Repono Proprie | |
| Usus principalis | Amino acida;Food / Feed Additives;Pharmaceutical;Pellentesque consectetur;etc. | |
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) AJI 97 Methodus test.
Lepidium sativum: Confer spectrum ultrarubrum effusio exempli cum illa regulae per modum discus bromide potassium.
Imprimis rotationis [α]20/D: Aridae Sample, C=8, 6mol/L HCl
Status Solutionis (Transmittance): 1.0g in 10ml H2O spectrophotometri, 430nm, 10nm crassitudinis cellae.
Chloride (Cl): Sicca Sample, 370mg, B-1
Aconitum (NH4): B-1
Sulfate (SO4): 1.2g, (1), ref: 0.50ml ex 0.005mol/L H2SO4
Ferrum (Fe): 1.5g, (1), ref: 1.5ml of Iron Std.(0.01mg/ml)
Metalla gravia (Pb): 2.0g, (4), ref: 2.0ml of Pb Std.(0.01mg/ml)
Arsenicum (As2O3): 2.0g, (1), ref: 2.0ml de As2O3 Std.
Alia Amino Acides: Test Sample: 50μg, S-6-a, imperium: L-Lys HCl 0.25μg
Damnum in remittit: ad 105℃ pro 3 horis.
Intenta: Specimen siccatum, 110mg, (3), 2ml acidum formic, 0.1mol/L HCLO4 1ml=9.133mg C6H14N2O2·HCl
PH Test: 1.0g in 10ml de H2O
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) USP35 Methodus Test.
DEFINITIO
Lysine hydrochloridum continet NLT 98.5% et NMT 101.5% Hydrochloridis L-Lysinae (C6H14N2O2·HCl), in fundamento exsiccato computatum.
IDENTIFICATIO
A. INFRARED HAUSTUS <197K>
TEMPTATIO
MODO PROCEDENDI
Sample: 90 mg Hydrochloridis Lysinae
Blank: Misce 3 mL acidi formici et 50 mL acidi glacialis.
Systema titrimetricum
(Vide Titrimetrium<541>)
Modus: Direct titration
Titrant: 0.1 N acidum perchloricum VS
Endpoint deprehensio: Potentiometric
Analysis: Solve Sample in 3 mL acidi formici et 50mL acidi glacialis.Adde acetatis mercurialis 10 mL TS, titrate cum Titrant.Blank determinationem praestare.
Calculare recipis Lysinae hydrochloridis (C6H14N2O2·HCl) in Sample desumptum:
Exitus = {[(VS-VB) xNxF]/W} x100
VS = Titrant volumen consumpsit Sample (mL)
VB= Titrant volumen absumptum a Blank (mL)
N = re normalitatis de Titrant (mEq/mL)
F= aequivalentia factor, 91.33 mg/mEq
W = Sample pondus (medicamentum)
Acceptatio criteria: 98.5%~ 101.5% in fundamento exsiccato
Aliorum
CONTENT OF CHLORIDE
Sample: 350 mg Hydrochloridis Lysinae
Blank: 140 mL aquae
Systema titrimetricum
(Vide Titrimetrium<541>)
Modus: Direct titration
Titrant: 0.1 N nitrate argenti VS
Endpoint deprehensio: Visual
Analysis: Exemplar transfer ad fictilem murrinam, adde aquae 140 mL et 1 mL dichlorofluorescein TS.Titrate cum Titrante usque ad flocculatum chloridum argenteum et mixturam tenuem roseum acquirit colorem.Blank determinationem praestare.
Recipis chloridi (Cl) in Sample sumpta:
Exitus = {[(VS VB) N F]/W} 100
VS = Titrant volumen consumptum a Sample (mL)
VB = Titrant volumen absumptum a Blank (mL)
N = normalitas de Titrant (mEq/mL)
F = factor equivalency, 35.45 mg/mEq .
W = Sample pondus (medicamentum)
Acceptatio criteria: 19.0%~ 19.6%
IMPURITIES
RESIDUUM DE IGNIS <281>: NMT 0.1%
CHLORIDE ET SULFATE, Sulfate <221>
Solutio Standard: 0.10mL ex 0.020 Acidi sulphurici N
Sample: 0.33g Lysine Hydrochloridis
Acceptatio criteria: NMT 0.03%
FERRUM <241>: NMT 30ppm
Delere sequentia:
GRAVALIS METALS, Methodus I <231>: NMT 15ppm .
COGNATUS COMPONS
Solutio Standard: 0,05 mg/mL ex hydrochloride USP L-Lysine RS in aqua.[NOTA-Haec solutio retrahitur aequipollens 0.5% illius solutionis Samplei.]
Sample solutio: 10mg/mL Hydrochloridis Lysine in aqua
Solutio aptabilitas systematis: 0.4 mg/mL singulae ex USP L-Lysine hydrochloride RS et USP arginini hydrochloridi RS.
Systema chromatographicum (Vide Chromatographia <621>, chromatographia Thin-Layer.)
Modus: TLC
Adsorbent: 0.25-mm iacuit chromatographico silicae gel mixtionis
Applicationem voluminis: 5μL
Solvendo ratio explicandi: Isopropyl alcohol et ammonium hydroxidum (7:3)
Imbre reagens: 0.2 g ninhydrin in mixtione alcoholi et 2N acidi acetici (95:5)
Ratio convenientia
Opportunitas requisita: solutio chromatogramma Systematis convenientia ostendit duas maculas distincte separatas.
Analysis
Exempla: Solutio Standard, solutio ratio convenientiae, et solutionis Sample.
Patella inter 100° et 105° excoquatur donec ammoniaci penitus evanescat.Imbre cum Spray gerente, et calore inter 100° et 105° pro 15 min.Discute laminam sub lumine albo.
Criteria acceptationis: Quaelibet macula secundaria solutionis Sample non maior vel intensior est quam macula principalis solutionis Standardi.
Singulae immunditiae: NMT 0.5%
Totalis immunditiae: NMT 2.0%
IN SPECIE TESTS
ROTATIO OPTICALIS, Rotatio Imprimis <781S>
Sample solutio: 80 mg/mL in 6 N acidum hydrochloricum
Criteria acceptationis: +20.4° ad +21.4°
LOSSON EXsiccatio <731>: sicca specimen in 105℃ pro 3 h: amittit NMT 0.4% sui ponderis.
ADDITICIUS REQUISITIS
PACKAGING and storage: Conserva in vasis bene clausis.
USP Reference STANDARDS <XI>
USP Arginine Hydrochloride RS
USP L-Lysine Hydrochloride RS
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) JP17 Methodus Test
Hydrochlorida L-Lysina siccata, non minus quam 98.5% hydrochloridi L-lysinae (C6H14N2O2.HCl) continet.
DescriptionL-Lysine Hydrochloridis ut cerussa occurrit.Habet levem proprietatem saporis.
In aqua et in acido formico libere solubile, et in ethanolo fere solubile (95).
crystallum polymorphismum ostendit.
Lepidium sativum (1) Determinare absorptionem spectrum infrarubrum de Hydrochloride L-Lysine, antea exsiccato, ut in methodo bromidis potassii disci sub infrared spectrophotometriae <2.25> ordinatur, et spectrum spectrum cum Reference Imaginis conferas: utraque spectra similes intensitates absorptionis in idem fluctus numerorum.Si aliqua differentia inter spectra apparet, Hydrochloridem L-Lysinam in aqua solve, aquam in siccitatem ad 60℃ evaporare, et experimentum cum residuo repetere.
(2) Solutio Hydrochloridis L-Lysinae (1 in 10) respondet qualitativi probati <1.09> pro chloride.
Rotatione optica <2.49>[α]20/D: +19.0 - +21.5° (exsiccata 2 g, 6 mol/L acidum hydrochloricum TS, 25 mL, 100 mm).
pH <2.54> solve 1.0 g hydrochloridis L-Lysinae in 10 mL aquae: solutionis pH est inter 5.0 et 6.0.
Puritas (1) Claritas et color solutionis-Dissolve 1.0 g Hydrochloridis L-Lysinae in 10 mL aquae: Solutio clara et sine colore.
(2) Sulfate <1.14>-Perfice experimentum cum 0.6 g Hydrochloride L-Lysine.Praeparate solutionem solutionis cum 0.35 mL mol/L acidi sulphurici VS (non plus quam 0.028%).
(3) Aconitum <1.02>-Perfice experimentum 0.25 g Hydrochloridis L-Lysinae.Praeparate solutionem dicionis cum 5.0 mL solutionis Amoniorum Standard (non plus quam 0.02%).
(4) Metalla gravia <1.07>-Perge cum 2.0 g Hydrochloride L-Lysine secundum Methodum 1, et perfice experimentum.Praeparate solutionem solutionis cum 2.0 mL Solutio Standard Duc (non plus quam 10 ppm).
(5) Arsenicum <1.11> - Praepara experimentum solutionem cum 1.0 g Hydrochloridi L-Lysine secundum Methodum 1, et experimentum (non plus quam 2 ppm) perficies.
(6) Substantiae cognatae solve 0.10 g hydrochloridis L-Lysinae in 25 mL aquae et hac solutione utere solutione exempli.Pipet 1 mL solutionis specimen, aquam adde ut solutionis hujus exacte 50 mL, fistulae 5 mL, aquam addas ut prorsus 20 mL facias, et hac solutione utere solutionem regulae.Experimentum facere cum his solutionibus sicut sub tenui chromatographia <2.03> directae.Macula 5μL singulae solutionis specimen et solutionis normae in lamella silica gel pro chromatographia tenui.Evolvere laminam cum mixtura aquae propanoli et ammoniaci (28) (67:33) ad 10 cm fere distantiam, et laminam ad 100℃ pro 30 minutis excoquatur.Expande aequabiliter laminam cum solutione ninhydrini in acetono (1 in 50) et calore 80℃ pro 5 minuta; maculae praeter maculam principalem a solutione sample solutionis non vehementiores sunt quam macula a solutione vexillum.
Amissio siccationis <2.41> Non plus quam 1.0% (1 g, 105℃, 3 horae).
Residere ignitionem <2.44> Non plus quam 0,1% (1 g).
Perpende accurate circa 0.1 g Hydrochloridis L-Lysinae, antea exsiccatae, solve acidi formic in 2 mL, adde exacte 15 mL de acido perchlorico VS 0.1 mol/L, et caloris in balineo aquae per 30 minuta.Post refrigerationem adde acidi acetici 45 mL (100), et titrate <2.50> excessum acidi perchlorici cum 0.1 mol/L sodium acetatis VS (titrationis potentiometricae).Fac blank determinationes, et emendas quamlibet necessarias.
Singulae mL of 0.1 mol/L acidi perchlorici VS 9.132 mg C6H14N2O2.HCl
Vasa et repositiones continentia continens stricta.
sarcina: Fluorinated Utrem, 25kg/peram, 25kg/Cardboard Drum, vel secundum exigentiam emptoris.
Repono Condition:Copia in vasis obsignatis ad frigus, siccum et ventilatas horreis ab substantiis non repugnantibus.A luce et humore protege.Fortis oxidizing agentibus abstinete.
Quam mercari?Quaeso contactumDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
15 Annorum Usus?Plus quam XV annos experientiae habemus in fabricando et exportando amplis intermediis pharmaceuticis vel alchimicis pharmaceuticis amplis.
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L-(+)-Lysine Monohydrochloridis (H-Lys-OH·HCl) (CAS: 657-27-2) late adhibetur ut supplementa nutritionis in cibo et in potum industriis.Adhiberi etiam potest in pastu animalium fonte L-Lysine.L-Lysine Monohydrochloride adhiberi potest in varietate industriarum quae possidet: productionem cibi, potum, pharmaceuticum, agriculturam/animalem, et varias alias industrias.
Product functiones & Applications:
1. Lysine HCL nutritio nutriendi fortificans est, quae functiones habet augendi appetitus iumentorum et gallinarum, morborum resistentiae, vulneris sanationis promovendae, carnium qualitatem meliorem, excretionem gastricam amplificandi, ac nervos cerebri componendo, cellulis germinis, servo et haemoglobinis essentialibus. substantiae.Plerumque copia addita in cibario est 0.1-0.2%.
2. Lysine HCL est essentiale amino acidum in corpore humano, quod augere potest functionem hematopoieticam, augere secretionem suci gastrici, augere interdum utendo, augere morbo resistentiam, conservare stateram metabolicam, et fovere progressionem natorum chemicorum physicam et mentis progressionem.Sinae farinam, tortulas et panes, quae ad noodles expediendas uti possunt, in copia 1 ad 2g/kg adhibentur;0.3 ad 0.8g/kg in liquore bibendo.
3. Lysine HCL una e maximis amino acida est, et industria amino acidi nunc magni pretii et momenti industria facta est.Lysine maxime in cibo, potione, in cibo.
Officium:
1. Cibus gradus: nutritionis enhancer, usus ad condimentum in mayonnaise, lac, instant noodles cibum
2. Gradus medicinalis: praeparatio ad transfusionem acidi amino compositi, efficientiam medicamentorum emendandam
III. pasce gradus: facere stateram nutritionis gallinis, meliorem escam qualitatem et productivity
L-(+) - Monohydrochloride Lysine maxime fit per fermentationem cantilenarum corynebacteria utens, praesertim Corynebacterium glutamicum, quod comprehendit multi gradus processus inter fermentationem, separationem cellae per centrifugationem vel ultrafiltrationem, separationem et purgationem, evaporationem et exsictionem producti.Propter L-Lysinam magni momenti, conatus constanter fiunt ad fermentum processus emendandos, laborem complectentem et processum evolutionis necnon instrumentorum optimizationis et amni processus adhibentur ad productionem L-lysine et alia acida L-amino; operatio vitae miscentes tristique vel fermenters aeris.
