L-(+)-Lysine Monohydrochloride CAS 657-27-2 (H-Lys-OH·HCl) Assay 98.5~101.0% Factory High Quality
Ko Shanghai Ruifu Chemical Co., Ltd. te kaihanga matua me te kaiwhakarato o L-(+)-Lysine Monohydrochloride (H-Lys-OH·HCl) (CAS: 657-27-2) me te kounga teitei, te kaha whakaputa 1000 Tons ia tau.Ko tetahi o nga kaiwhakarato waikawa amino nui rawa atu i Haina, ka tukuna e Ruifu Chemical nga waikawa amino tae noa ki nga paerewa o te ao, penei i nga paerewa AJI, USP, EP, JP me FCC.Ka taea e matou te whakarato COA, te tuku i te ao, te iti me te rahinga e waatea ana.Mena kei te pirangi koe ki te L-(+)-Lysine Monohydrochloride,Please contact: alvin@ruifuchem.com
| Ingoa matū | L-(+)-Lysine Monohydrochloride |
| Nga kupu taurite | H-Lys-OH·HCl;L-Lysine Monohydrochloride;L-Lysine Hydrochloride;L-Lysine HCl;Laevo-Lysine Hydrochloride;Lysine Hydrochloride;Lysine Monohydrochloride;(S)-2,6-Diaminohexanoic Acid Monohydrochloride |
| Tūnga Taonga | I roto i te Stock, Production Raukaha 1000 Tons ia Tau |
| Tau CAS | 657-27-2 |
| Tātai rāpoi | C6H14N2O2·HCl |
| Taumaha rāpoi | 182.65 |
| Iwi Whakarewa | 263 ℃(tikuri)(marama) |
| Kiato | 1.28 g/cm3 (20 ℃) |
| Wairewa wai | Wairewa ki te Wai, Tata Puata |
| Wairewa | Ka Rere noa ki te Wai me te Waikawa Formic.He Iti Wairewa ki te Ewaro.Tino Insouble i roto i te Etera |
| Rokiroki Temp. | He mea hiri ki te maroke, rokiroki i te pāmahana rūma |
| COA & MSDS | Kei te waatea |
| whakarōpūtanga | Waikawa Amino me nga Paariki |
| Waitohu | Ruifu Chemical |
| Waehere Morearea | 34 - He weranga |
| Whakaahuatanga Haumaru | S24/25 - Kaua e pa ki te kiri me nga kanohi. |
| UN ID | UN 1789 8/PG 3 |
| WGK Tiamana | 2 |
| Waehere HS | 2922419000 |
| Nga taonga | Nga Paerewa Tirotiro | Hua |
| Te ahua | Tioata ma, paura Tioata ranei | Ka rite |
| Tautuhinga | Spectrum Absorption Infrared | Ka rite |
| Hurihuri Tau [α]20/D | +20.4° ki te +21.4°(C=8 i roto i te 6N HCl) | +20.8° |
| State of Solution (Whakawhiti) | Maama me te Taekore ≥98.0% | 98.8% |
| Chloride (Cl) | 19.0 ki te 19.6% | 19.15% |
| pūkawa (SO4) | ≤0.020% | <0.020% |
| Haukinia (NH4) | ≤0.020% | <0.020% |
| Rino (Fe) | ≤10ppm | <10ppm |
| Konga Taamaha (Pb) | ≤10ppm | <10ppm |
| Arsenic (As2O3) | ≤1.0ppm | <1.0ppm |
| Ētahi atu waikawa Amino | ≤0.50% (TLC) | Ka rite |
| Ngaronga i te whakamaroke | ≤0.40% (i te 105 ℃ mo te 3 haora) | 0.25% |
| Te toenga i runga i te mura (Sulfated) | ≤0.10% | 0.06% |
| Te whakamatautau | 98.5 ki te 101.5% (hei turanga maroke) | 99.7% |
| Ko nga poke o te pararopi | Whakaaetia te Whakaritenga | Ka rite |
| Whakamātautau pH | 5.0 ki te 6.0 (1.0g i te 10ml o H2O) | 5.2 |
| Wairewa toenga | Ka rite | Ka rite |
| Whakamutunga | Ka tutaki ki te Paerewa o AJI97;USP;JP | |
| Te Ora Papa | 24 Marama Mai i te Ra Hanganga mena ka penapena tika | |
| Nga Whakamahinga Matua | Waikawa Amino;Kai / Whāngai tāpiritanga;Rongoa;Kai Whakanui;etc. | |
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) AJI 97 Tikanga Whakamatau
Tautuhinga: Whakatauritea te awhiowhiotanga infrared absorption o te tauira ki tera o te paerewa ma te tikanga kōpae pāhare pāporo bromide.
Hurihuri Tau [α]20/D: Tauira maroke, C=8, 6mol/L HCl
State o Solution (Transmittance): 1.0g i roto i te 10ml o H2O spectrophotometer, 430nm, 10nm matotoru pūtau.
Chloride (Cl): Tauira maroke, 370mg, B-1
Haukinia (NH4): B-1
Putakawa (SO4): 1.2g, (1), ref: 0.50ml o 0.005mol/L H2SO4
Rino (Fe): 1.5g, (1), ref: 1.5ml o Iron Std.(0.01mg/ml)
Nga Kourarahi Taumaha (Pb): 2.0g, (4), ref: 2.0ml o Pb Std.(0.01mg/ml)
Arsenic (As2O3): 2.0g, (1), ref: 2.0ml o As2O3 Std.
Ētahi atu waikawa Amino: Tauira Whakamātautau: 50μg, S-6-a, mana whakahaere: L-Lys HCl 0.25μg
Ngaronga i te whakamaroke: i te 105 ℃ mo te 3 haora.
Te whakamatautau: Tauira maroke, 110mg, (3), 2ml o te waikawa formic, 0.1mol/L HCLO4 1ml=9.133mg C6H14N2O2·HCl
Whakamātautau pH: 1.0g i te 10ml o H2O
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) USP35 Tikanga Whakamatau
WHAKAMAHI
Kei roto i te Lysine Hydrochloride te NLT 98.5% me te NMT 101.5% o te L-Lysine Hydrochloride (C6H14N2O2·HCl), kua tatauhia i runga i te kaupapa maroke.
WHAKATAUTANGA
A. KAUPAPA INFRARED <197K>
WHAKAMAHI
WHAKAMAHI
Tauira: 90 mg o Lysine Hydrochloride
Watea: Whakaranuhia te 3 mL o te waikawa formic me te 50 mL o te waikawa ahetiki hukapapa.
Pūnaha Titrimetric
(Tirohia Titrimetry <541>)
Aratau: Te titration tika
Titrant: 0.1 N te waikawa perchloric VS
Te kitenga ira mutunga: Potentiometric
Tātaritanga: Whakarewahia te Tauira ki te 3 mL o te waikawa formic me te 50mL o te waikawa ahetiki hukapapa.Tāpirihia te 10 mL o te mēkuri acetate TS, ka titrate ki te Titrant.Mahia te whakatau Patea.
Tātaihia te ōrau o Lysine Hydrochloride (C6H14N2O2·HCl) i roto i te Tauira i tangohia:
Hua = {[(VS-VB) xNxF]/W} x100
VS= Rōrahi titrant i pau i te Tauira (mL)
VB= Rōrahi titrant pau i te Pātea (mL)
N= te noho noa o te Titrant (mEq/mL)
F= tauwehe taurite, 91.33 mg/mEq
W= Tauira taumaha (mg)
Paearu whakaae: 98.5% ~ 101.5% i runga i te whakamaroke
ATU ATU
TE KAUPAPA KAUPAPA
Tauira: 350 mg o Lysine Hydrochloride
Patea: 140 mL wai
Pūnaha Titrimetric
(Tirohia Titrimetry <541>)
Aratau: Te titration tika
Titrant: 0.1 N hiriwa pākawa VS
Te kitenga ira mutunga: Ataata
Tātaritanga: Whakawhitihia te Tauira ki te ipu porcelain, ka tāpirihia te 140 mL wai me te 1 mL o te dichlorofluorescein TS.Whakawetohia ki te Titrant kia pupuhi te hauhautanga hiriwa ka whiwhi te ranunga ki te tae mawhero ngoikore.Mahia te whakatau Patea.
Tātaihia te ōrau o te pūhaumāota (Cl) i te Tauira i tangohia:
Hua = {[(VS − VB) × N × F]/W} × 100
VS = rōrahi titrant i pau i te Tauira (mL)
VB = rōrahi titrant i pau i te Patea (mL)
N = te noho noa o te Titrant (mEq/mL)
F = tauwehe taurite, 35.45 mg/mEq
W = Tauira taumaha (mg)
Paearu whakaae: 19.0%~19.6%
NGA POKE
TOHUTOHU I RUNGA I TE MAHI <281>: NMT 0.1%
CHLORIDE AND SULFATE, Sulfate <221>
Wairewa paerewa: 0.10mL o te 0.020 N te waikawa pungatara
Tauira: 0.33g o Lysine Hydrochloride
Paearu whakaae: NMT 0.03%
RINO <241>: NMT 30ppm
Mukua enei e whai ake nei:
NGA METAL TAITAHA, Tikanga I <231>: NMT 15ppm
NGA KAUPAPA KAUPAPA
Te otinga paerewa: 0.05 mg/mL o USP L-Lysine Hydrochloride RS i roto i te wai.[FAKATOKANGA-He kukū tenei otinga ki te 0.5% o te otinga Tauira.]
Tauira otinga: 10mg/mL o Lysine Hydrochloride i roto i te wai
Te otinga pai o te punaha: 0.4 mg/mL ia USP L-Lysine Hydrochloride RS me USP Arginine Hydrochloride RS
Pūnaha Chromatographic (Tirohia Chromatography <621>, Chromatography Apa Angiangi.)
Aratau: TLC
Adsorbent: 0.25-mm te paparanga o te ranunga chromatographic silica gel
Rōrahi tono: 5μL
Te whakawhanake i te punaha whakarewa: Isopropyl alcohol and ammonium hydroxide (7:3)
Reagent reagent: 0.2 g ninhydrin i roto i te ranunga o te waipiro butyl me te waikawa 2N acetic (95:5)
Te pai o te punaha
Nga whakaritenga e tika ana: E whakaatu ana te chromatogram o te otinga pai o te punaha e rua nga waahi kua wehea.
Tātaritanga
Tauira: Te otinga Paerewa, Te otinga pai o te punaha, me te otinga Tauira.
Me whakamaroke te pereti i waenga i te 100° me te 105° kia ngaro rawa atu te haukini.Rehu ki te Reagent Reagent, ka whakamahana i waenga i te 100° me te 105° mo te 15 min.Tirohia te pereti i raro i te marama ma.
Paearu whakaae: Ko nga waahi tuarua o te otinga Tauira kaore i te nui ake, i te kaha ake ranei i te waahi matua o te otinga Paerewa.
He poke takitahi: NMT 0.5%
Tapeke poke: NMT 2.0%
NGA WHAKAMATAUTANGA
TE WHAKATAUTANGA OPTICAL, Te Hurihanga Motuhake <781S>
Tauira otinga: 80 mg/mL i roto i te 6 N waikawa pūhaumāota
Paearu whakaae: +20.4° ki +21.4°
TE WHAKAMAROKE NGARO <731>: Me whakamaroke he tauira ki te 105 ℃ mo te 3 haora: ka ngaro te NMT 0.4% o tona taumaha.
HE WHAKAMAHI ATU
PAKITANGA ME TE WHAKAPUTANGA: Tiakina ki roto i nga ipu kua kati pai.
USP REFERENCE STANDARD <11>
USP Arginine Hydrochloride RS
USP L-Lysine Hydrochloride RS
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) JP17 Tikanga Whakamatau
Ko te L-Lysine Hydrochloride, ina whakamarokehia, kaua e iti iho i te 98.5% o te L-lysine hydrochloride (C6H14N2O2.HCl).
WhakaahuaL-Lysine Hydrochloride ka puta hei paura ma.He paku, he reka ahuatanga.
He memeha noa ki te wai me te waikawa formic, me te kore e rewa ki te waiwaro (95).
E whakaatu ana i te polymorphism tioata.
Tautuhinga (1) Whakatauhia te tuāwhiorangi whakauru infrared o L-Lysine Hydrochloride, i whakamarokehia i mua, pera i te whakahau i roto i te tikanga kōpae pāhare pāporo bromide i raro i te Spectrophotometry Infrared <2.25>, ka whakatairitehia te tūāwhiorangi ki te Tūāwhiorangi Tohutoro: e whakaatu ana nga tūāwhiorangi e rua te kaha o te horomanga i te nga tau ngaru rite.Mena ka puta he rerekee i waenga i te awhiowhiotanga, whakakorehia te L-Lysine Hydrochloride ki te wai, whakaeto i te wai kia maroke i te 60 ℃, ka whakahoki ano i te whakamatautau me te toenga.
(2) He otinga o te L-Lysine Hydrochloride (1 i roto i te 10) ka whakautu ki nga Whakamātautau Tohu <1.09> mo te pūhaumāota.
Te hurihanga whatu <2.49>[α]20/D: +19.0 - +21.5° (i muri i te whakamaroketanga, 2 g, 6 mol/L waikawa pūhaumāota TS, 25 mL, 100 mm)
pH <2.54> Whakarewahia te 1.0 g o L-Lysine Hydrochloride ki te 10 mL wai: ko te pH o tenei otinga kei waenganui i te 5.0 me te 6.0.
Maama (1) Maama me te tae o te wairewa-Whakarewa 1.0 g o L-Lysine Hydrochloride ki te 10 mL wai: he maamaa te otinga me te kore tae.
(2) Sulfate <1.14>-Mahia te whakamatautau me te 0.6 g o te L-Lysine Hydrochloride.Whakaritehia te otinga whakahaere me te 0.35 mL o te 0.005 mol/L waikawa pungatara VS (kaua e neke ake i te 0.028%).
(3) Ammonium <1.02>-Mahia te whakamatautau me te 0.25 g o te L-Lysine Hydrochloride.Whakapaia te otinga mana me te 5.0 mL o te Waihanga Haukini Paerewa (kaua e neke ake i te 0.02%).
(4) Nga konganuku taumaha <1.07>-Haere ki te 2.0 g o L-Lysine Hydrochloride kia rite ki te Tikanga 1, ka mahia te whakamatautau.Whakapaia te otinga mana me te 2.0 mL o te Wairewa Aratohu Paerewa (kaua e neke ake i te 10 ppm).
(5) Arsenic <1.11>-Whakaritea te otinga whakamatautau me te 1.0 g o te L-Lysine Hydrochloride kia rite ki te Tikanga 1, ka mahia te whakamatautau (kaua e neke ake i te 2 ppm).
(6) Nga matū e pa ana-Whakarewahia te 0.10 g o L-Lysine Hydrochloride ki te 25 mL wai, ka whakamahi i tenei otinga hei tauira otinga.Pipet 1 mL o te tauira otinga, tapirihia he wai kia rite ki te 50 mL, paipa 5 mL o tenei wairewa, tapirihia he wai kia rite ki te 20 mL, ka whakamahi i tenei otinga hei otinga paerewa.Mahia te whakamatautau me enei rongoatanga pera i te whakahau i raro i te Thin-layer Chromatography <2.03>.Tuhia te 5μL o ia tauira otinga me te otinga paerewa ki runga i te pereti kirikiri mo te chromatography paparanga angiangi.Whakawhanakehia te pereti me te ranunga o te 1-propanol me te wai haukini (28) (67:33) kia tata ki te 10 cm te tawhiti, ka whakamarokehia te pereti i te 100℃ mo te 30 meneti.Mahia kia taurite te pereti me te wairewa ninhydrin i roto i te acetone (1 i roto i te 50) me te whakamahana i te 80 ℃ mo te 5 meneti: ko nga waahi i tua atu i te waahi matua mai i te tauira otinga kaore i te kaha ake i te waahi mai i te otinga paerewa.
Ngaronga i te whakamaroke <2.41> Kaua e neke ake i te 1.0% (1 g, 105℃, 3 haora).
Te toenga i runga i te mura <2.44> Kaua e neke ake i te 0.1% (1 g).
Whakamātautau Kia tika te pauna mo te 0.1 g o te L-Lysine Hydrochloride, kua whakamarokehia i mua, memeha ki te 2 mL o te waikawa formic, tāpirihia kia rite ki te 15 mL o te 0.1 mol/L waikawa perchloric VS, ka whakamahana ki te pati wai mo te 30 meneti.Whai muri i te whakamatao, tāpirihia te 45 mL o te waikawa acetate (100), ka whakatairitea <2.50> te taikaha o te waikawa perchloric ki te 0.1 mol/L konutai acetate VS (potentiometric titration).Whakaritehia he whakatau patea, me te whakatika i nga mea e tika ana.
Ia mL o te 0.1 mol/L waikawa perchloric VS ＝9.132 mg o C6H14N2O2.HCl
Ipu me te rokiroki Ipu-Tight ipu.
Mōkī: Pounamu Fluorinated, 25kg / putea, 25kg / Cardboard Drum, kia rite ki te hiahia a te kaihoko.
Tikanga Rokiroki:Rokiroki i roto i nga ipu hiri ki te whare putunga matao, maroke me te whai hau kia matara atu i nga matū hotokore.Tiaki i te marama me te makuku.Kia matara atu i nga mea whakahaora kaha.
Me pehea te hoko?Whakapā maiDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
15 tau te wheako?Neke atu i te 15 tau o matou wheako ki te hanga me te kaweake i te whānuitanga o nga momo takawaenga rongoa kounga teitei, matū pai ranei.
Nga maakete matua?Hokona ki te maakete kaainga, Amerika Te Tai Tokerau, Uropi, Inia, Korea, Hapani, Ahitereiria, aha atu.
Nga painga?Ko te kounga teitei, te utu utu, nga ratonga ngaio me te tautoko hangarau, te tuku tere.
KoungaWhakapumautanga?Pūnaha whakahaere kounga tino.Ko nga taputapu ngaio mo te tātari ko te NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.
Tauira?Ko te nuinga o nga hua e whakarato ana i nga tauira kore utu mo te aromatawai kounga, me utu nga utu kaipuke e nga kaihoko.
Te arotake a wheketere?Nau mai te arotake wheketere.Whakaritea he hui i mua.
MOQ?Kaore he MOQ.Ka whakaaetia te ota iti.
Wā Tukunga? Mena kei roto i nga taonga, e toru nga ra ka whakamanahia te tuku.
Te kawe waka?Ma te Express (FedEx, DHL), ma te Air, ma te Moana.
Tuhinga?I muri i te ratonga hokohoko: COA, MOA, ROS, MSDS, me etahi atu ka taea te whakarato.
Whakaritenga Whakaritenga?Ka taea te whakarato ratonga whakahiato ritenga kia pai ai to hiahia rangahau.
Nga tikanga utu?Ko te nama Proforma ka tukuna tuatahi i muri i te whakapumautanga o te ota, ka kohia o maatau korero peeke.Te utu ma te T/T (Telex Transfer), PayPal, Western Union, etc.
Ko te L-(+)-Lysine Monohydrochloride (H-Lys-OH·HCl) (CAS: 657-27-2) e whakamahia whānuitia ana hei taapiri kai i roto i nga umanga kai me te inu.Ka taea hoki te whakamahi ki nga kai kararehe hei puna o L-Lysine.Ka taea te whakamahi i te L-Lysine Monohydrochloride i roto i te maha o nga momo ahumahi tae atu ki: hanga kai, inu, rongoa, ahuwhenua / whangai kararehe, me etahi atu ahumahi.
Nga Mahi Hua me nga Taumahi:
1. Ko te Lysine HCL he kai whakapakari kai, he mahi hei whakanui ake i te hiahia o te kararehe me te heihei, te whakapai ake i te mate o te mate, te whakatairanga i te whakaora i te patunga, te whakapai ake i te kounga kai, te whakarei ake i te hunanga puku, me te whakahiato i nga nerves roro, nga pūtau iroriki, nga pūmua me te hemoglobin tino nui. matū.Ko te tikanga ko te nui o te taapiri i roto i te kai ko te 0.1-0.2%.
2. Ko te Lysine HCL he waikawa amino tino nui i roto i te tinana o te tangata, ka taea te whakarei ake i te mahi hematopoietic, te whakarei ake i te hunanga wai pekitiki, te whakanui ake i te whakamahinga o te pūmua, te whakanui ake i te mate o te mate, te pupuri i te toenga metabolic, me te awhina i te whakawhanaketanga o te pukapuka matū a nga tamariki ki te whakawhanaketanga tinana me te hinengaro.Ka whakatauhia e Haina ko te paraoa, te pihikete me te taro ka taea te whakamahi mo te tukatuka kihu ka whakamahia i roto i te nui o te 1 ki te 2g/kg;0.3 ki te 0.8g/kg i roto i te wai inu.
3. Ko Lysine HCL tetahi o nga waikawa amino tino nui, a kua noho te ahumahi waikawa amino hei umanga nui me te hiranga.Ka whakamahia te Lysine ki te kai, te rongoa me te kai.
Taumahi:
1. Te karaehe kai: te whakaniko i te kai, whakamahia mo te kinaki ki te mayonnaise, te miraka, te kai kihu inamata
2. Koeke Medcine: te whakarite mo te whakawhitinga waikawa amino pūhui, te whakapai ake i te pai o nga raau taero
3. Whangai kōeke: hanga toenga kai tōtika heihei, whakapai ake te kounga kai me te hua
Ko te L-(+)-Lysine Monohydrochloride te nuinga o te whakaputa ma te fermentation ma te whakamahi i nga riaka o te corynebacteria, ina koa ko Corynebacterium glutamicum, kei roto he mahinga maha-taahiraa tae atu ki te fermentation, te wehenga o te pūtau ma te centrifugation, te ultrafiltration ranei, te wehenga hua me te purenga, te whakaetonga me te whakamaroke.Na te mea nui o te L-Lysine, kei te kaha tonu te mahi ki te whakapai ake i nga tukanga FERMENTATION, kei roto ko te riaka me te whanaketanga o te tukanga tae atu ki te arotautanga pāpāho me te tukatuka o raro e whakamahia ana mo te hanga L-lysine me etahi atu waikawa L-amino, mahi i roto i te ranu tank fermenters ara rangi ranei.
