(Boc)2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity>99.0% (HPLC) Factory Protecting Reagent
Shanghai Ruifu Chemical Co., Ltd. ndi omwe amapanga Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9) yokhala ndipamwamba kwambiri.Ruifu Chemical imapereka ma reagents oteteza ndi ma reagents ophatikiza.Titha kupereka padziko lonse lapansi, mtengo wampikisano, zochepa komanso zochulukirapo zomwe zilipo.Gulani Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com
Dzina la Chemical | Di-tert-Butyl Iminodicarboxylate |
Mawu ofanana ndi mawu | (Boc) 2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic Acid Di-tert-Butyl Ester;Bis (tert-Butoxycarbonyl) ammonia |
Stock Status | Zilipo |
Nambala ya CAS | 51779-32-9 |
Molecular Formula | C10H19NO4 |
Kulemera kwa Maselo | 217.27 g / mol |
Melting Point | 114.0 ~ 120.0 ℃ |
Kuchulukana | 1.037±0.06 g/cm3 |
Zomverera | Simamva Kuwala, Kuwala |
Kusungunuka kwamadzi | Zosasungunuka m'madzi |
Kusungunuka | Chloroform, Methanol |
Kusungirako Temp. | Malo Ozizira & Owuma (2~8℃) |
COA & MSDS | Likupezeka |
Gulu | Kuteteza ma Reagents |
Mtundu | Ruifu Chemical |
Zinthu | Miyezo Yoyendera | Zotsatira |
Maonekedwe | White Crystalline Powder | Zimagwirizana |
Melting Point | 114.0 ~ 120.0 ℃ | 118.8 ~ 119.3 ℃ |
Kutaya pa Kuyanika | <0.50% | 0.10% |
Kuyera / Kusanthula Njira | >99.0% (HPLC) | 99.6% |
Infrared Spectrum | Zimagwirizana ndi Kapangidwe | Zimagwirizana |
Chithunzi cha NMR | Zimagwirizana ndi Kapangidwe | Zimagwirizana |
Mapeto | Chogulitsacho chayesedwa ndipo chikugwirizana ndi zomwe zaperekedwa |
Mzere wa Chromatographic: SE-54 30m×0.25mm×0.5μm;
Detector: FID
Kutentha koyamba: 100 ℃
Nthawi yoyamba: 1min
Kutentha kwapakati: 20 ℃ / min
Kutentha komaliza: 190 ℃
Pomaliza: 10min
Jekeseni kutentha: 160 ℃
Kutentha kwa detector: 200 ℃
Chiŵerengero chogawanika: 50: 1;
Kukula kwachitsanzo: 0.2μl;
Zosakaniza: methanol
Zotsatira: Chiyerocho chinali chachikulu kuposa 99.0% ndi njira yokhazikika yadera.
Phukusi:Botolo, Aluminiyamu zojambulazo thumba, 25kg/Cardboard Drum, kapena malinga ndi zofunika kasitomala.
Mkhalidwe Wosungira:Sungani m'mitsuko yomata pamalo ozizira komanso owuma (2~8 ℃) kutali ndi zinthu zomwe sizingagwirizane.Tetezani ku kuwala ndi chinyezi.
Manyamulidwe:Kutumiza kudziko lonse lapansi ndi FedEx / DHL Express.Perekani mwamsanga ndi yodalirika yobereka.
Kodi kugula?Chonde lemberaniDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Zaka 15 Zokumana nazo?Tili ndi zaka zopitilira 15 pakupanga ndi kutumiza kunja kwamitundu yambiri yamankhwala apamwamba kwambiri kapena mankhwala abwino.
Misika Yaikulu?Gulitsani kumsika wapakhomo, North America, Europe, India, Korea, Japan, Australia, etc.
Ubwino wake?Ubwino wapamwamba, mtengo wotsika mtengo, ntchito zamaluso ndi chithandizo chaukadaulo, kutumiza mwachangu.
UbwinoChitsimikizo?Njira yoyendetsera bwino kwambiri.Zida zaukadaulo zowunikira zikuphatikizapo NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.
Zitsanzo?Zogulitsa zambiri zimapereka zitsanzo zaulere zowunikira zabwino, mtengo wotumizira uyenera kulipidwa ndi makasitomala.
Factory Audit?Takulandilani ku fakitale.Chonde panganitu nthawi yokumana.
MOQ?Palibe MOQ.Dongosolo laling'ono ndilovomerezeka.
Nthawi yoperekera? Ngati mkati mwa katundu, kubweretsa masiku atatu kutsimikizika.
Mayendedwe?Ndi Express (FedEx, DHL), ndi Air, ndi Nyanja.
Zolemba?Pambuyo pa ntchito yogulitsa: COA, MOA, ROS, MSDS, ndi zina zotero.
Custom Synthesis?Itha kukupatsirani ntchito zophatikizira zomwe zikugwirizana bwino ndi zosowa zanu zofufuza.
Malipiro Terms?Invoice ya Proforma idzatumizidwa kaye mukatsimikizira kuyitanitsa, ndikuyika zambiri zathu zakubanki.Malipiro a T/T (Telex Transfer), PayPal, Western Union, etc.
Zizindikiro Zowopsa Xi - Zokwiyitsa
Zizindikiro Zowopsa 36/37/38 - Zokwiyitsa maso, kupuma komanso khungu.
Kufotokozera Zachitetezo S26 - Mukakhudzana ndi maso, yambani nthawi yomweyo ndi madzi ambiri ndikupempha upangiri wamankhwala.
S37/39 - Valani magolovesi oyenera komanso chitetezo chamaso / kumaso
WGK Germany 3
HS kodi 29241990
Hazard Note Irritant
Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Kugwiritsa ntchito Di-tert-Butyl Iminodicarboxylate ndi mankhwala apakatikati, omwe amatha kukonzedwa ndi gawo limodzi la formamide ndi Boc2O.
Pawiri amagwiritsidwa ntchito ngati reagent pokonzekera ma amines oyambira kuchokera ku alkyl halides.Idadziwika ngati njira ina ya kaphatikizidwe ka Gabriel pa kutembenuka komweko.Amines amathanso kukonzedwa kuchokera ku zakumwa zoledzeretsa pogwiritsa ntchito mphamvu ya Mitsunobu.Mwachizolowezi kukhazikitsa reagent ndi deprotonated kupereka potaziyamu mchere, amene ali N-alkylated.Magulu oteteza a Boc amachotsedwa pambuyo pake pansi pa acidic.
Di-tert-Butyl Iminodicarboxylate ndi gulu lotetezedwa la amine lomwe limagwiritsidwa ntchito pokonzekera ma spirocycle oletsedwa ngati CCR1 antagonists.
Kukonzekera yankho la DMAP (0.61g, 5.0mmol) mu MeCN (15ml) pang'onopang'ono anawonjezera yankho la formamide (2.5g,56mmol) ndi Boc2O (24)g, 110mol) mu MeCN (15ml).Pambuyo poyambitsa kutentha kwa 4h, njira yachikasu idakhazikika mpaka 0 ° C, ndipo N,N-diethylenediamine (6.97g, 60mmol) idawonjezeredwa pang'onopang'ono pa 0 ℃.The chifukwa osakaniza analimbikitsa firiji kwa 12h ndi osasankhidwa mwa woonda silika PAd;chifukwa osakaniza ankasefedwa firiji.Zosungunulirazo zimatuluka nthunzi pansi pa kupanikizika kocheperako.Zogulitsazo zidatsukidwa ndi silica gel chromatography ndikusinthidwa ndi EtOAc/hexane (1:5) kuti mupeze mutu wa mankhwala, omwe ndi olimba oyera (10.99g, 92%).