Fmoc-Asp(OtBu)-OH CAS 71989-14-5 Purity>99.0% (HPLC) Factory
Shanghai Ruifu Chemical Co., Ltd. ndi omwe amapanga Fmoc-L-Aspartic Acid β-tert-Butyl Ester (Fmoc-Asp(OtBu)-OH) (CAS: 71989-14-5) yokhala ndi khalidwe lapamwamba.Ruifu Chemical imapereka ma amino acid angapo.Titha kupereka padziko lonse lapansi, mtengo wampikisano, zochepa komanso zochulukirapo zomwe zilipo.Gulani Fmoc-Asp(OtBu)-OH,Please contact: alvin@ruifuchem.com
Dzina la Chemical | Fmoc-L-Aspartic Acid β-tert-Butyl Ester |
Mawu ofanana ndi mawu | Fmoc-Asp(OtBu)-OH;Fmoc-L-Asp(OtBu)-OH;N-Fmoc-L-Aspartic Acid 4-tert-Butyl Ester;Fmoc-L-Aspartic Acid beta-tert-Butyl Ester;N-α-Fmoc-L-Aspartic Acid β-tert Butyl Ester;4-tert-Butyl N-Fmoc-L-Aspartate;4-tert-Butyl N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-L-Aspartate;N- [(9H-Fluoren-9-ylmethoxy)carbonyl]-L-Aspartic Acid 4-tert-Butyl Ester;N-(9-Fluorenylmethoxycarbonyl) -L-Aspartic Acid β-tert-Butyl Ester;N-(9-Fluorenylmethoxycarbonyl)aspartic Acid 4-tert-Butyl Ester |
Stock Status | Zilipo |
Nambala ya CAS | 71989-14-5 |
Molecular Formula | C23H25NO6 |
Kulemera kwa Maselo | 411.45 g / mol |
Melting Point | 145.0 ~ 160.0 ℃ |
Kuchulukana | 1.251 |
Kusungunuka kwamadzi | Zosungunuka pang'ono m'madzi |
Kusungirako Temp. | Malo Ozizira & Owuma (2~8℃) |
COA & MSDS | Likupezeka |
Gulu | Fmoc-amino Acids |
Mtundu | Ruifu Chemical |
Zinthu | Miyezo Yoyendera | Zotsatira |
Maonekedwe | Ufa Woyera | Ufa Woyera |
Kusinthasintha Kwachindunji [α]20/D | -24.0°±2.5° (C=1 mu DMF) | -25.10 ° |
Melting Point | 145.0 ~ 160.0 ℃ | 146.8 ~ 147.5 ℃ |
Kuyera kwa Optical | <0.20% D-Enantiomer | 0.0271% |
Kumveka kwa Yankho | 0.3 magalamu mu 2ml DMF Clear Solution | Zimagwirizana |
Kaiser Test | <0.05% | <0.05% |
Madzi ndi Karl Fischer | <0.50% | 0.37% |
Kutaya pa Kuyanika | <0.50% (70 ℃, 2h) | 0.23% |
Fmoc-β-Ala-OH | <0.10% (HPLC) | Zimagwirizana |
Fmoc-β-Ala-Asp (OtBu)-OH | <0.10% (HPLC) | Zimagwirizana |
Fmoc-Asp(OtBu)-Asp(OtBu)-OH | <0.10% (HPLC) | Zimagwirizana |
Fmoc-Asp-OH | <0.10% (HPLC) | Zimagwirizana |
Assay Free Amino Acid | <0.20% (GC) | Zimagwirizana |
Ethyl Acetate | <0.50% (GC) | Zimagwirizana |
Kuyera / Kusanthula Njira | >99.0% (HPLC) | 99.84% |
Misa Spectrum | Mogwirizana ndi Mulingo | Zimagwirizana |
Chithunzi cha NMR | Mogwirizana ndi Mulingo | Zimagwirizana |
Mapeto | Chogulitsacho chayesedwa ndipo chikugwirizana ndi zomwe zaperekedwa |
Phukusi: Botolo la Fluorinated, thumba la Aluminiyamu zojambulazo, 25kg / Cardboard Drum, kapena malinga ndi zomwe kasitomala amafuna.
Mkhalidwe Wosungira:Sungani m'mitsuko yomata pamalo ozizira komanso owuma (2~8 ℃) kutali ndi zinthu zomwe sizingagwirizane.Tetezani ku kuwala ndi chinyezi.
Kodi kugula?Chonde lemberaniDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Zaka 15 Zokumana nazo?Tili ndi zaka zopitilira 15 pakupanga ndi kutumiza kunja kwamitundu yambiri yamankhwala apamwamba kwambiri kapena mankhwala abwino.
Misika Yaikulu?Gulitsani kumsika wapakhomo, North America, Europe, India, Korea, Japan, Australia, etc.
Ubwino wake?Ubwino wapamwamba, mtengo wotsika mtengo, ntchito zamaluso ndi chithandizo chaukadaulo, kutumiza mwachangu.
UbwinoChitsimikizo?Njira yoyendetsera bwino kwambiri.Zida zaukadaulo zowunikira zikuphatikizapo NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.
Zitsanzo?Zogulitsa zambiri zimapereka zitsanzo zaulere zowunikira zabwino, mtengo wotumizira uyenera kulipidwa ndi makasitomala.
Factory Audit?Takulandilani ku fakitale.Chonde panganitu nthawi yokumana.
MOQ?Palibe MOQ.Dongosolo laling'ono ndilovomerezeka.
Nthawi yoperekera? Ngati mkati mwa katundu, kubweretsa masiku atatu kutsimikizika.
Mayendedwe?Ndi Express (FedEx, DHL), ndi Air, ndi Nyanja.
Zolemba?Pambuyo pa ntchito yogulitsa: COA, MOA, ROS, MSDS, ndi zina zotero.
Custom Synthesis?Itha kukupatsirani ntchito zophatikizira zomwe zikugwirizana bwino ndi zosowa zanu zofufuza.
Malipiro Terms?Invoice ya Proforma idzatumizidwa kaye mukatsimikizira kuyitanitsa, ndikuyika zambiri zathu zakubanki.Malipiro a T/T (Telex Transfer), PayPal, Western Union, etc.
Zizindikiro Zowopsa Xi - Zokwiyitsa
Zizindikiro Zowopsa 36/37/38 - Zokwiyitsa maso, kupuma komanso khungu.
Kufotokozera Zachitetezo S24/25 - Pewani kukhudzana ndi khungu ndi maso.
S36/37/39 - Valani zovala zodzitchinjiriza zoyenera, magolovesi ndi chitetezo chamaso/nkhope.
S27 - Chotsani nthawi yomweyo zovala zonse zowonongeka.
S26 - Mukakhudzana ndi maso, muzimutsuka nthawi yomweyo ndi madzi ambiri ndipo funsani malangizo achipatala.
WGK Germany 3
HS kodi 2922491990
Kalasi Yowopsa IRRITANT
Fmoc-L-Aspartic Acid β-tert-Butyl Ester (Fmoc-Asp(OtBu)-OH) (CAS: 71989-14-5) ndi mankhwala apakatikati, omwe amagwiritsidwa ntchito popanga polypeptide synthesis process, pofuna kuteteza amino acid.Fmoc-amino acids, omwe amagwiritsidwa ntchito popanga peptide, amagwiritsidwa ntchito ngati organic synthesis wapakatikati, mankhwala apakatikati, biochemical reagent kapena reagent mankhwala.
Kukonzekera: Onjezani 581g wa tert-Butyl Acetate ndi 133g wa Aspartic Acid mu botolo la pakamwa patatu la ML, yambitsani, ndi kuwonjezera perchloric acid dropwise, zochita pa 10 ℃ kwa maola 48, utakhazikika ku 0 ℃, kenaka kuwonjezera 700ml ya madzi, yotengedwa (otsala tert-Butyl Acetate monga zosungunulira m'zigawo), neutralized ndi Na2CO3 kuti pH = 7, madzi kulekana, ndi tert-Butyl Acetate wosanjikiza anali anaikira pansi pa kupanikizika yafupika kupeza chisakanizo cha Asp(OtBu)2, Asp(OtBu) ndi mafuta a Asp-OtBu, omwe adaphatikizidwa ndi wosanjikiza wamadzi kuti agwiritsidwe ntchito.The chifukwa osakaniza anasamutsidwa kwa 125 ml atatu mabotolo, G cuso4 · 5H2O anawonjezera, ndi pH zinasinthidwa 3 ndi anaikira hydrochloric acid.Chosakanizacho chinagwedezeka ndikutenthedwa mpaka 50 ℃.Kwa maola 12 kukonzekera Cu[Asp(OtBu)]x.(x = 1~2);Kenako mpaka kutentha kwa chipinda, onjezerani 116.2G tetramethylethylenediamine ndi 300ml dioxane, ndiyeno sinthani pH kukhala 8 ~ 9 ndi triethylamine kukonzekera Asp(OtBu);kenako onjezerani 82gFmoc-OSu mu Asp(OtBu), sungani pH 8 ~ 9, gwirani kwa maola 8, kenako kuchotsa ndi ethyl acetate, acidify, kusamba ndi madzi, vacuum distillation, crystallization, kuyanika, 85g wa Fmoc-L-aspartic acid beta -tert-butyl ester inapezedwa muzokolola za 20.7%.Ndi HPLC kusanthula kwa Fmoc-L-Aspartic Acid β-tert-Butyl Ester.