(Boc)2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity >99.0% (HPLC) Falegaosimea Puipuiga Puipuiga
Shanghai Ruifu Chemical Co., Ltd. o le taʻutaʻua taʻutaʻua o Di-tert-Butyl Iminodicarboxylate ((Boc) 2NH) (CAS: 51779-32-9) faʻatasi ai ma le maualuga.O le Ruifu Chemical o lo'o tu'uina atu se fa'asologa o mea fa'apipi'i fa'apipi'i.E mafai ona matou tuʻuina atu i le lalolagi atoa le tuʻuina atu, tau faʻatauvaʻa, laʻititi ma tele aofaʻi avanoa.Fa'atau Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com
Igoa Vailaau | Di-tert-Butyl Iminodicarboxylate |
Synonyms | (Boc)2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic Acid Di-tert-Butyl Ester;Bis(tert-Butoxycarbonyl)amonia |
Tulaga Fa'asoa | E tele |
Numera CAS | 51779-32-9 |
Fuafua mole | C10H19NO4 |
Molecular Weight | 217.27 g/mol |
Lisi Lisi | 114.0~120.0 ℃ |
Malosi | 1.037±0.06 g/cm3 |
Ma'ale'ale | Ma'ale'ale Ea, Ma'ale'ale Malamalama |
Suavai Solubility | E le mafai ona solu i le Vai |
Solubility | Chloroform, Methanol |
Temp. | Nofoaga malulu ma mago (2~8℃) |
COA & MSDS | Avanoa |
Vaega | Puipuiga Reagents |
Fa'ailoga | Ruifu Chemical |
Aitema | Tulaga Fa'atonu | I'uga |
Fa'aaliga | Pa'u tioata Pa'epa'e | E usitaia |
Lisi Lisi | 114.0~120.0 ℃ | 118.8~119.3 ℃ |
Ma'imau ile Fa'amago | <0.50% | 0.10% |
Mama / Suʻesuʻega Metotia | >99.0% (HPLC) | 99.6% |
Alaleo Infrared | E tusa ma le Fauga | E usitaia |
NMR Alaleo | E tusa ma le Fauga | E usitaia |
Fa'ai'uga | Ua uma ona fa'ata'ita'iina le oloa ma fa'amalieina fa'atonuga |
Koluma Chromatographic: SE-54 30m×0.25mm×0.5μm;
Su'esu'e: FID
Muamua vevela: 100℃
Vaitaimi amata: 1min
Fa'avevela fua: 20℃/min
vevela mulimuli: 190℃
I le faaiuga: 10 min
vevela tui: 160 ℃
Maalili ole su'esu'e: 200℃
Vaevae fua: 50:1;
Fa'ata'ita'iga tele: 0.2μl;
Suavai: methanol
I'uga: O le mama na sili atu nai lo le 99.0% e ala i le fa'aogaina o le vaega.
afifi:Fagu, Ato pepa alumini, 25kg/Kati Pusa, pe tusa ai ma manaoga o tagata faatau.
Tulaga teuina:Teu i totonu o pusa faʻamaufaʻailoga i le malulu ma mago (2 ~ 8 ℃) faleteuoloa mai mea e le fetaui.Puipui mai le malamalama ma le susu.
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Fa'afefea ona Fa'atau?Fa'amolemole fa'afeso'ota'iDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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Tulaga leleiFaamautinoaga?Fa'atonuga lelei faiga.O meafaigaluega faʻapitoa mo suʻesuʻega e aofia ai le NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc.
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MOQ?Leai MOQ.Laititi oka e talia.
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Pepa?A maeʻa le faʻatau atu auaunaga: COA, MOA, ROS, MSDS, ma isi mea e mafai ona tuʻuina atu.
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Fa'ailoga Mata'utia Xi - Itaita
Fa'ailoga Tulaga lamatia 36/37/38 - Fa'aitaita'i i mata, faiga manava ma le pa'u.
Fa'amatalaga o le Saogalemu S26 - Pe a pa'i i mata, fufulu vave i le tele o vai ma saili fautuaga fa'afoma'i.
S37/39 - Fai totigilima talafeagai ma mata/mata puipui
WGK Siamani 3
HS Code 29241990
Mata'utia Fa'amatalaga Fa'aitaita
Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Talosaga Di-tert-Butyl Iminodicarboxylate o se vailaʻau vaʻaia, lea e mafai ona saunia e ala i le tasi-laasaga faʻaalia o le formamide ma le Boc2O.
O le faʻaogaina o loʻo faʻaaogaina e avea o se reagent mo le sauniuniga o amine muamua mai alkyl halides.Na faʻalauiloaina o se isi mea i le Gabriel synthesis mo le liua tutusa.E mafai fo'i ona saunia amine mai 'ava malosi e ala i le fa'amama e fa'aaoga ai le tali a Mitsunobu.I le faʻatinoga masani o le reagent e deprotonated e tuʻuina atu le masima potassium, o le N-alkylated.Ole vaega ole puipuiga ole Boc e toe aveese i lalo ole tulaga oona.
Di-tert-Butyl Iminodicarboxylate ose vaega amine puipuia lea e fa'aaogaina e saunia ai spirocycles fa'atulafonoina e pei o CCR1 antagonists.
Saunia le vaifofo o le DMAP (0.61g, 5.0mmol) i le MeCN (15ml) e faʻaopoopo lemu ile fofo ole formamide (2.5g,56mmol) ma Boc2O (24).g, 110mol) i le MeCN (15ml).A maeʻa ona faʻaoso i le vevela o le potu mo le 4h, o le vaifofo samasama na faʻamafanafana i le 0 ° C, ma N, N-diethylenediamine (6.97g, 60mmol) na faʻaopoopo lemu ile 0 ℃.O le faʻafefiloi na maua na faʻafefeteina i le vevela o le potu mo le 12h ma faʻamama e ala i se pusa silica manifinifi;o le faʻafefiloi na maua na faʻamamaina i le vevela o le potu.Ona fa'amama lea o le solvent i lalo o le fa'aitiitia o le mamafa.O le oloa mama na fa'amamāina ile silica gel chromatography ma fa'amama ile EtOAc/hexane (1:5) e maua ai le igoa oloa, o se pa'epa'e malo (10.99g, 92%).