L-Glutamic Acid α-Benzyl Ester CAS 13030-09-6 (H-Glu-OBzl) Su'ega >98.5% (HPLC) Tulaga Maualuga
Shanghai Ruifu Chemical Co., Ltd. o le taʻutaʻua taʻutaʻua ma tuʻuina atu le L-Glutamic Acid α-Benzyl Ester (H-Glu-OBzl) (CAS: 13030-09-6) faʻatasi ai ma le maualuga.Ruifu Chemical o lo'o tu'uina atu se fa'asologa o amino acids ma mea e maua mai ai.E mafai ona matou tuʻuina atu i le lalolagi atoa le tuʻuina atu, laʻititi ma tele aofaʻi avanoa.Afai e te manaʻomia L-Glutamic Acid α-Benzyl Ester,Please contact: alvin@ruifuchem.com
Igoa Vailaau | L-Glutamic Acid α-Benzyl Ester |
Synonyms | H-Glu-OBzl;HL-Glu-OBzl;L-Glutamic Acid 1-Benzyl Ester;1-Benzyl L-Glutamate;L-Glutamic Acid alpha-Benzyl Ester;(S)-4-Amino-5-(Benzyloxy)-5-Oxopentanoic Acid |
Tulaga Fa'asoa | E tele |
Numera CAS | 13030-09-6 |
Fuafua mole | C12H15NO4 |
Molecular Weight | 237.26 |
Lisi Lisi | 140.0~150.0 ℃ |
Malosi | 1.245±0.06 g/cm3 |
Ma'ale'ale | Ma'ale'ale ea, Susū ma'ale'ale, Ma'ale'ale vevela |
Temp. | Faamaufa'ailoga i le mago, teu i le vevela o le potu |
COA & MSDS | Avanoa |
Fa'avasegaga | Amino Acids & Derivatives |
Fa'ailoga | Ruifu Chemical |
Aitema | Tulaga Fa'atonu | I'uga |
Fa'aaliga | Pa'u Pa'epa'e po'o le Pa'epa'e Pa'epa'e | Fa'atatau |
Ma'imau ile Fa'amago | <0.50% | 0.24% |
Lisi Lisi | 140.0~150.0 ℃ | 146.0~150.0 ℃ |
Su'ega / Su'esu'ega Metotia | >98.5% (HPLC) | 98.84% |
Ta'amilosaga Fa'apitoa [α]20/D | +10.0 i le +12.0° (C=1, 1mol/L HCl) | Fa'atatau |
Alaleo Infrared | E tusa ma le Fauga | Fa'atatau |
Proton NMR Alaleo | E tusa ma le Fauga | Fa'atatau |
Fa'ai'uga | Lenei Oloa e ala ile Asiasiga E tusa ai ma le Enterprise Standard | |
Fa'aoga Autu | Amino acids ma mea e maua mai ai;Vailaau Fa'atekonolosi |
1. L-Glutamic Acid, Sodium Hydroxide, Suavai, Acetone, Boc-Anhydride
2. Boc-L-Glu-OH fa'atasi ma Benzyl Bromide ma Triethylamine e maua ai Boc-Glu-OBzl
3. HCL/EA Aveese Boc-, Fetuuna'i le PH, Maua H-Glu-OBzl
4. Solvents Faʻaaogaina: DMF, Ethyl Acetate, Ethanol
1. Mama (HPLC)
1.1 Meafaigaluega
Ole chromatography vai maualuga, UV3000 detector.
Paleni au'ili'ili faaeletonika
1.2 Reagents
Acetonitrile (vaega chromatographic), TFA (vaega chromatographic)
1.3 Tulaga Chromatographic
1.3.1 Koluma: koluma C18, 5 μl * 250 * 4.6 mm
1.3.2 Sailiga umi galu: 220nm
Fuafuaga tafe: 1.0 mL/min
Volume tui: 10 μL (mo faʻamatalaga)
Fa'asusu: acetonitrile
Taimi ta'avale: 20 minute
1.4 Sauniuniga vaega feaveai
Vaega feavea'i A (0.1% Trifluoroacetic acid Suavai): sa'o mitiia 1.0 ml TFA diluted i le 1000 ml i le vai, fefiloi ma degas.
Vaega feaveaʻi B (0.1% Trifluoroacetic acid Acetonitrile): faʻafefe saʻo le 1.0 ml TFA, faʻafefe i le 1000 ml ma le acetonitrile, faʻafefiloi ma degas.
1.5 Polokalama Gradient
Taimi (min) A% B%
0:00 90 10
10.00 10 90
15.00 10 90
15.01 90 10
20.00 90 10
1.6 Sauniuniga o fofo faataitai
Fua le 0.1 g faʻataʻitaʻiga ma faʻamavae i le acetonitrile ma faʻafefe i le 100ml.Lulu lelei mo le faʻaaogaina i le lumanaʻi, poʻo le faʻaoga tutusa.Saunia ni faataitaiga se lua e tutusa.
1.7 Fa'ata'ita'iga Filifiliga
Iloilo le fa'ata'ita'iga e tusa ai ma faiga fa'ata'ita'iga nei:
1) E sili atu i le 1 tui ole fofo avanoa
2) 1 tui ole fofo faataitai 1#
3) 1 tui ole fofo faataitai 2#
1.8.0 Fa'atatau
1.8.1 O le pito i luga o le eria normalization metotia na faʻaaogaina e fuafua ai le mama o le HPLC.
1.8.2 Ole eseesega ole fa'atatau ole mama ole nila e lua e le tatau ona sili atu ile 1%
1.8.3 Afai o taunuuga o tui uma e lua e fetaui ma tulaga taliaina, ave le averesi mama o le taunuuga mulimuli.
afifi: Fa'ato'aga Fa'alili, Ato pepa alumini, 25kg/Cardboard Drum, pe tusa ai ma mana'oga o tagata fa'atau.
Tulaga teuina:Teu i totonu o koneteina fa'amaufa'ailoga i fale teuoloa malulu, mago ma fa'a'avevela mai mea e le fetaui.Puipui mai le malamalama ma le susu.
afifi: Fa'ato'aga Fa'alili, Ato pepa alumini, 25kg/Cardboard Drum, pe tusa ai ma mana'oga o tagata fa'atau.
Tulaga teuina:Teu i totonu o koneteina fa'amaufa'ailoga i fale teuoloa malulu, mago ma fa'a'avevela mai mea e le fetaui.Puipui mai le malamalama ma le susu.
Fa'afefea ona Fa'atau?Fa'amolemole fa'afeso'ota'iDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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L-Glutamic Acid α-Benzyl Ester (H-Glu-OBzl) (CAS: 13030-09-6), Amino Acids and Derivatives;Vailaau Fa'atekonolosi.
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