(Boc)2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity >99.0% (HPLC) Factory Protecting Reagent

Tsanangudzo Pfupi

Kemikari Zita: Di-tert-Butyl Iminodicarboxylate

Anoreva zvakafanana: (Boc)2NH;N-Boc-tert-Butylcarbamate

CAS: 51779-32-9

Kuchena:> 99.0% (HPLC)

Kuonekwa: White Crystalline Powder

Kudzivirira Reagents, High Quality

Bata: Dr. Alvin Huang

Nharembozha/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

Tumira email kwatiri

Product Detail

Product Tags

Tsanangudzo:

Shanghai Ruifu Chemical Co., Ltd. ndiyo inotungamira kugadzira Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9) ine mhando yepamusoro.Ruifu Chemical inopa akateedzana ekudzivirira reagents uye coupling reagents.Isu tinokwanisa kupa kutakura kwepasirese, mutengo wemakwikwi, madiki uye akawanda akawanda aripo.Tenga Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com

Chemical Properties:

Chemical Name	Di-tert-Butyl Iminodicarboxylate
Mashoko anoreva zvakafanana	(Boc)2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic Acid Di-tert-Butyl Ester;Bis(tert-Butoxycarbonyl)ammonia
Stock Status	Mudura
Nhamba yeCAS	51779-32-9
Molecular Formula	C10H19NO4
Molecular Weight	217.27 g/mol
Melting Point	114.0~120.0℃
Density	1.037±0.06 g/cm3
Sensitive	Air Sensitive, Chiedza Chinonzwa
Mvura Solubility	Insoluble muMvura
Solubility	Chloroform, Methanol
Storage Temp.	Nzvimbo Inotonhorera & Yakaoma (2~8℃)
COA & MSDS	Available
Category	Kudzivirira Reagents
Brand	Ruifu Chemical

Zvinotsanangurwa:

Items	Kuongorora Maitiro	Results
Chitarisiko	White Crystalline Powder	Zvinoenderana
Melting Point	114.0~120.0℃	118.8~119.3℃
Kurasika paKuomesa	<0.50%	0.10%
Kuchena / Analysis Method	>99.0% (HPLC)	99.6%
Infrared Spectrum	Inopindirana neChimiro	Zvinoenderana
NMR Spectrum	Inopindirana neChimiro	Zvinoenderana
Mhedziso	Chigadzirwa chacho chakaedzwa uye chinoenderana nezvakapihwa

Purity Test:

Chromatographic column: SE-54 30m×0.25mm×0.5μm;
Detector: FID
Yekutanga tembiricha: 100 ℃
Nguva yekutanga: 1 min
Kupisa mwero: 20 ℃/min
Pakupedzisira tembiricha: 190 ℃
Pakupedzisira: 10min
Jekiseni tembiricha: 160 ℃
Tembiricha ye detector: 200 ℃
Kupatsanura ratio: 50:1;
Saizi yemuenzaniso: 0.2μl;
Diluent: methanol
Mhedzisiro: Kuchena kwaive kwakakura kupfuura 99.0% nenharaunda normalization nzira.

Pakeji/Kuchengeta/Shipping:

Package:Bhodhoro, Aluminium foil bag, 25kg/Cardboard Drum, kana zvinoenderana nezvinodiwa nemutengi.
Storage Condition:Chengetedza mumidziyo yakavharwa panzvimbo inotonhorera uye yakaoma (2~8℃) yekuchengetera kure nezvinhu zvisingaenderane.Dzivirira kubva kuchiedza uye unyoro.
KutumiraKuendesa kupasirese neFedEx / DHL Express.Ipa kutumirwa nekukurumidza uye kwakavimbika.

Zvakanakira:

Yakakwana Capacity: Inokwana zvivakwa uye matekiniki

Professional Service: Imwe inomira kutenga sevhisi

OEM Package: Tsika pasuru uye label iripo

Fast Delivery: Kana iri mukati me stock, mazuva matatu ekutumira anovimbiswa

Yakagadzika Supply: Chengetedza zvine musoro stock

Tsigiro yehunyanzvi: Tekinoroji mhinduro iripo

Tsika Synthesis Service: Kubva pamagiramu kusvika makirogiramu

Hunhu Hwepamusoro: Yakagadzira yakakwana yemhando yekusimbisa system

FAQ:

Kutenga sei?Please contactDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

Makore 15 Oupenyu?Tine makore anopfuura 15 ane ruzivo mukugadzira uye kutumira kunze kwemhando dzakasiyana-siyana dzepamusoro dzemishonga yepakati kana makemikari akanaka.

Main Markets?Tengesa kumusika wepamba, North America, Europe, India, Korea, Japan, Australia, nezvimwe.

Zvakanakira?Hunhu hwepamusoro, mutengo unokwanisika, masevhisi ehunyanzvi uye rutsigiro rwehunyanzvi, kuendesa nekukurumidza.

HunhuSimbiso?Strict quality control system.Midziyo yehunyanzvi yekuongorora inosanganisira NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, nezvimwe.

Samples?Zvigadzirwa zvakawanda zvinopa mahara emahara ekuongorora kwemhando, mutengo wekutumira unofanirwa kubhadharwa nevatengi.

Factory Audit?Factory audit inogamuchirwa.Ndapota itai nguva isati yasvika.

MOQ?Hapana MOQ.Kurongeka kudiki kunogamuchirwa.

Delivery Nguva? Kana mukati me stock, mazuva matatu kutumirwa anovimbiswa.

Transportation?Ne Express (FedEx, DHL), neMhepo, neGungwa.

Zvinyorwa?Mushure mekutengesa sevhisi: COA, MOA, ROS, MSDS, nezvimwe zvinogona kupihwa.

Custom Synthesis?Inogona kupa echinyakare synthesis masevhisi kuti aenderane nezvinodiwa zvako zvekutsvagisa.

Payment Terms?Proforma invoice inozotumirwa kutanga mushure mekusimbisa kurongeka, yakavharirwa ruzivo rwedu rwebhangi.Kubhadhara neT/T (Telex Transfer), PayPal, Western Union, nezvimwe.

51779-32-9 - Njodzi uye Kuchengeteka:

Hazard Symbols Xi - Irritant
Njodzi Makodhi 36/37/38 - Kushungurudza maziso, kufema system uye ganda.
Tsanangudzo Yekuchengetedza S26 - Kana wasangana nemaziso, sukurudza nekukurumidza nemvura yakawanda uye tsvaga mazano ekurapwa.
S37/39 - Pfeka magirovhosi akakodzera uye dziviriro yeziso / kumeso
WGK Germany 3
HS Code 29241990
Hazard Note Irritant

Application:

Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Kushandisa Di-tert-Butyl Iminodicarboxylate imishonga yepakati, iyo inogona kugadzirwa nedanho rimwechete rekuita kweformamide neBoc2O.
Mushonga wacho unoshandiswa seajenti yekugadzirira kwekutanga amines kubva kualkyl halides.Yakave yakakurumbira seimwe nzira yeGabriel synthesis yekutendeuka kumwe chete.Amines inogonawo kugadzirwa kubva kudoro nekupererwa nemvura uchishandisa Mitsunobu reaction.Mukushandiswa kwechinyakare iyo reagent inoderedzwa kupa iyo potassium munyu, iyo N-alkylated.Mapoka ekudzivirira eBoc anozobviswa pasi pemamiriro ane acidic.
Di-tert-Butyl Iminodicarboxylate iboka rakachengetedzwa reamine rinoshandiswa kugadzirira conformationally conformationally contrained spirocycles seCCR1 vanopikisa.
Kugadzirira mhinduro yeDMAP (0.61g, 5.0mmol) muMeCN (15ml) inowedzerwa zvishoma nezvishoma kune mhinduro ye formamide (2.5g,56mmol) uye Boc2O (24).g, 110mol) muMeCN (15ml).Mushure mekusimudzira pakamuri yekushisa kwe4h, mhinduro yero yakanyoroveswa kusvika ku0 ° C, uye N, N-diethylenediamine (6.97g, 60mmol) yakawedzerwa zvishoma nezvishoma pa 0 ℃.Iko kusanganiswa kwakagadzirwa kwakakonzerwa nekupisa kwekamuri kwe 12h uye kusefa kuburikidza nekatete silica pad;musanganiswa unoguma wakanatswa pane tembiricha yekamuri.The solvent inobva yanyungudutswa pasi pekumanikidzwa kwakaderedzwa.Chigadzirwa chisina kuchena chakacheneswa ne silica gel chromatography uye yakaburitswa neEtOAc/hexane (1:5) kuwana zita rezita, iro rakasimba chena (10.99g, 92%).