β-Phenylethylamine (PEA) CAS 64-04-0 Assay > 99.0% (GC) Factory High Purity

4 Test nzira
4.1 Chitarisiko
Kuongorora kwekuona.
4.2 Kuchena Kutsunga
4.2.1 Reagents uye zvinhu
a) Nitrogen: kuchena hakusi pasi pe99.9%, mushure mekucheneswa kurapwa
b) Hydrogen: kuchena hakusi pasi pe99.9%, mushure mekucheneswa kurapwa
C) Mhepo: mushure mekunatswa kurapwa
4.2.2 Zvishandiso nemidziyo
a) Gasi chromatograph: kunzwa uye kugadzikana kunosangana nezvinodiwa zveGB/T9722;
Detector: hydrogen flame ionization detector;
Koramu yeruvara ndeye SE-54 ine dhayamita ye30m*0.32mm*0.4μm.
b) Kugadziriswa kwedata: N2000 makemikari workstation, uchishandisa nharaunda normalization nzira kuverenga muzana yezvigadzirwa.
c) 10μm sampler.
4.2.3 Mamiriro ekushanda kwegasi chromatography
a) Gasification tembiricha: 250 ℃;
b) Kuona tembiricha: 220 ℃;
c) Column tembiricha: 160 ℃;
d) Mutakuri gasi kumanikidzwa: 0.06MPa;
e) Hydrogen pressure: 0.1MPa;
f) Kudzvinyirirwa kwemhepo: 0.2MPa;
g) Muenzaniso jekiseni vhoriyamu: 0.2ul;
h) Nguva yekuchengeta: 2.693
Izvo zviri pamusoro ndizvo zvinowanzoitika mamiriro ekushanda, vashandisi vanogona kugadzirisa kwakakodzera zvinoenderana nehunhu hwechiridzwa, kuitira kuti vawane yakanakisa kupatsanura mhedzisiro.
4.2.4 Kuyera nzira
Pasi pemamiriro epamusoro echromatographic, 0.2ul sampuli dzakatorwa ne 10ul sampler mushure mekunge chiridzwa chagadziriswa, uye chromatographic diagram yakawanikwa.Kuchena kwe β-phenylethylamine kwakayerwa nenharaunda normalization nzira.
4.2.5 Musiyano unobvumidzwa
Musiyano uripo pakati pezviyero zviviri zvakaenzana hazvipfuuri 0.25%, uye kukosha kwemasvomhu kunotorwa semugumisiro wekuyera.
4.3 Sarudzo yemvumo yemukati yemukati
Maererano neJJF1070.
5 Testing Regulations
5.1 β-Phenethylamine inofanira kuongororwa nedhipatimendi rekuongorora unhu hwefekitari, uye yakanamatirwa kune chitupa chisati chaendeswa.
5.2 Zvigadzirwa zvekettle imwe chete zvichashandiswa sebatch, uye batch yega yega yezvigadzirwa haingapfuuri tani imwe.
5.3 Sampling Method
Sample maererano neGB/T 6680-2003, huwandu hwese hwemuenzaniso hausi pasi pe50g.
5.4 Panguva yekuongorora, kana chero chinhu chisina kukodzera, chinotenderwa kuenzanisa pasuru mbiri yechigadzirwa kuti itariswezve.Kana kuchine imwe index isina kukodzera mumhedzisiro yekuongororazve, batch yezvigadzirwa ichatongwa seisina kukodzera.
Label, kurongedza, chekufambisa uye kuchengetedza
6.1 Label
Zvakajeka zvigadzirwa mamaki achadhindwa kana kunamirwa pamidziyo yekurongedza, kusanganisira zita rechigadzirwa, kuchena, giredhi remhando, kugadzirwa kwechigadzirwa nhamba yakajairika, zuva rekugadzira, nhamba yejeti, huremu hwakakura uye huremu hwemukati hwezvigadzirwa.Iyo dhizaini yekuchengetedza ichave inoenderana neGB/T191.
6.2 Packaging
Plastic drum packing
6.3 Kufambisa
Chigadzirwa chacho chinogona kutakurwa nenzira dzakajairika, izvo zvinofanirwa kudzivirira kunaya kwemvura, tembiricha yakakwira uye fireworks, uye haifanirwe kusanganiswa nezvinhu zvinoparadza uye zvinhu zvinoburitsa gasi rinoparadza kana mhute.
6.4 Kuchengeta
Zvigadzirwa zvichachengetwa munzvimbo inotonhorera, yakaoma uye hazvizochengetwe nezvinhu zvinoora uye zvinhu zvinoburitsa gasi rinoparadza kana mhute.