1-Methyl-3-Pyrrolidinol CAS 13220-33-2 daahirnimo>98.0% (GC)

Sharaxaad Gaaban:

Magaca Kiimikada: 1-Methyl-3-Pyrrolidinol

La mid ah: 3-Hydroxy-1-Methylpyrrolidine

CAS: 13220-33-2

Daahirsanaanta:>98.0% (GC)

Muuqaalka: Dareeraha Jaallaha fudud

Xiriirka: Dr. Alvin Huang

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Sharaxaad:

Kiimikada Ruifu waa soo saaraha ugu horreeya ee 1-Methyl-3-Pyrrolidinol (3-Hydroxy-1-Methylpyrrolidine) (CAS: 13220-33-2) oo leh tayo sare.Kiimikada Ruifu waxay bixin kartaa gaarsiinta adduunka oo dhan, qiimo tartan ah, adeeg aad u wanaagsan, tiro yar iyo tiro badan oo la heli karo.Iibso 1-Methyl-3-Pyrrolidinol,Please contact: alvin@ruifuchem.com

Guryaha Kiimikada:

Magaca Kiimikada	1-Methyl-3-Pyrrolidinol
La mid ah	N-Methyl-3-Pyrrolidinol;3-Hydroxy-1-Methylpyrrolidine;N-Methyl-Pyrrolidin-3-ol;N-Methyl-Pyrrolidinyl Khamriga;1-Methylpyrrolidin-3-ol
Heerka Saamiyada	Suuqa dhexdiisa, Wax-soo-saarka Ganacsiga
Lambarka CAS	13220-33-2
Qaanuunka molecular	C5H11NO
Miisaanka Molecular	101.15 g/mol
Barta Karsan	75 ℃/12 mmHg
Barta Fiishka	71℃
Cufnaanta	0.921 g/ml at 25 ℃ ( shid)
Tusmada N20/D	1.464 (iftiin)
Xasaasi ah	Xasaasiyadda hawada, Hygroscopic
Solubility	Ku milmay Biyaha, Ku milma Khamriga, Ether iyo Benzene
COA & MSDS	La heli karo
Tusaale	La heli karo
Asal ahaan	Shanghai, Shiinaha
Summada	Kiimikada Ruifu

Tilmaamaha:

Walxaha	Heerarka Kormeerka	Natiijooyinka
Muuqashada	Dareeraha Jaallaha fudud	Dareeraha Jaallaha fudud
Biyaha waxaa qoray Karl Fischer	<0.20%	0.15%
Daahirnimada / Habka Falanqaynta	>98.0% (GC)	98.57%
Cufnaanta (20 ℃)	0.920 ~ 0.923	U hogaansama
Tusmada N20/D	1.463 ~ 1.465	U hogaansama
Infrared Spectrum	Waafaqsan Qaab-dhismeedka	U hogaansama
1H NMR Spectrum	Waafaqsan Qaab-dhismeedka	U hogaansama
Gabagabo	Alaabta waa la tijaabiyay oo waafaqay tilmaamihii la bixiyay

Xidhmada/Kaydinta/Raridda:

Xidhmada:Dhalo, bacda bireed ee aluminium, 25kg/Drum kartoonada, ama sida waafaqsan shuruudaha macmiilka.

Xaaladda Kaydinta:Weelka si adag u xidh oo ku kaydi qabow, qalalan (2 ~ 8 ℃) iyo bakhaar hawo wanaagsan leh oo ka fog walxaha aan ku habboonayn.Ka ilaali iftiinka iyo qoyaanka.
Rarida:Ku gaarsii adduunka oo dhan hawo, by FedEx/DHL Express.Bixi keenid degdeg ah oo la isku halayn karo.

13220-33-2 - Jidka synthetic:

13220-33-2 - Habka diyaarinta:

Ku dar 1,2,4-Butanetriol iyo glacial acetic acid dheriga falcelinta, walaaq oo kulayl ku saabsan 100 ℃, ku dar gaaska hydrogen chloride qalalan, oo ka falceliya 90 ~ 110 ℃ 30h, marka qadar badan oo ah hydrogen chloride bilaabay ka muuqda gaaska dabada, meesha ugu dambeysa ee falcelinta ayaa la hubiyay waxaana la joojiyay hydrogen chloride.Qaboojinta ka dib, walxaha waa la sii daayay, lagu maydhay xal karbohaydrayt soodhiyam ah oo buuxa, waxaana lagu sarifay cadaadiska hoos u dhaca, iyo 120 ilaa 135 ℃.(12.6 ilaa 13. 3kPa) jajab, I .e., 1,4-Dichloro-2-Butanol walxaha saliidda ah, waxay soo saaraan 50% ~ 60%.
Baaskiilada xal aqueous ah 1,4-Dichloro-2-Butanol iyo Methylamine ayaa lagu daray dheriga baaskiil wadista, oo kuleyl ilaa 120 ℃.Kuleyl xiran hoostiisa, falcelinta ayaa la kiciyay 10h.qaboojinta ka dib, sodium hydroxide adag ayaa lagu daray, iyo cusbada aan organic ahayn ee degdegay ayaa la sifeeyay.Lakabka saliidda waa la kala soocay oo waxaa lagu sakhiray nadiifinta faakuumka, iyo jajabka 76-85 ℃.(2.1 kPa) ayaa la ururiyay si ay u noqoto badeecada la dhammeeyay.Soo saarista lakabka aqueous leh benzene sidoo kale waxay soo saartaa qayb ka mid ah 1-Methyl-3-Pyrrolidinol.Wax-soo-saarku wuxuu ahaa ilaa 60%.
3. Hababka muhiimka ah:
3.1 Habka falcelinta beddelka: xakamee wakhtiga falcelinta oo ogow meesha ugu dambaysa ee falcelinta
3.2 Nidaamka furfurista faakuumka ee 1,4-Dichloro-2-Butanol: xakamaynta heerka faakuumka distillation vacuum iyo heerkulka jajabka
3.3 Habka falcelinta wareegga wareegga: xakamaynta heerkulka falcelinta iyo waqtiga
3.4 1-Methyl-3-Pyrrolidinol habka distillation vacuum: xakamee heerka faakuumka distillation vacuum iyo heerkulka jajabka
4. Qodobbada xakamaynta tayada:
Goobta xakamaynta tayada 1: 1,2,4-Butanetriol heerka tayada alaabta ceeriin
Barta xakamaynta tayada 2: Heerka tayada xakamaynta dhexe ee falcelinta baaskiilka
Barta xakamaynta tayada 3: 1,4-Dichloro-2-Butanol heerka tayada dhexdhexaadka ah
Goobta xakamaynta tayada 4: 1-Methyl-3-Pyrrolidinol waxay dhammaatay heerka tayada alaabta

13220-33-2 - Habka Imtixaanka:

Nuxurka Qoyaanka: Qaado alaabtan oo tijaabi si waafaqsan habka go'aaminta qoyaanka (Habka koowaad A ee Lifaaqa Ⅷ M, Daabacaadda 2010 ee Jamhuuriyadda Dadka Shiinaha Pharmacopoeia).Qoyaanku waa inuusan ka badnaan 0.2%.
Cufnaanta Qaraabo: Cufnaanta qaraabada ee alaabtan (Lifaaqa VI A ee Qaybta II, daabacaadda 2010) waa 0.920 ~ 0.923
Tusmada dib-u-celinta: Tusaha dib-u-celinta ee alaabtan (Lifaaqa VI F ee Qaybta II ee daabacaadda 2010) waa 1.463 ~ 1.465
Go'aaminta nuxurka: Waxa ku jira 1-Methyl-3-Pyrrolidinol waa in aanay ka yarayn 98.0% chromatography gaaska (Lifaaqa Ⅴ E, Qaybta II, daabacaadda 2010).
Tiirka: Kaabadaha ku jira silica dhalaalay SPB-5, dhexroorka gudaha 0.32mm, dhererka 30m
T duritaanka: 300 ℃
FID: 320 ℃
Tiirka T: 80 ℃ 5 daqiiqo, ilaa 200 ℃ at 5℃/daqiiqo, ka dibna at 200 ℃ 7 daqiiqo
Qaade: Helium at 1 ml/min
Saamiga kala baxa: 100:1
Duritaan: 1 microlitir
Xalka tijaabada: milanka 200mg ee muunada marka la falanqaynayo 10ml oo methanol ah.Duri 1 microlitir.1μl ayaa lagu duray chromatograph gaaska si loo duubo chromatogramka.Waxa ku jira 1-Methyl-3-Pyrrolidinol waxaa lagu xisaabiyay habka caadiga ah ee aagga ugu sarreeya.

Faa'iidooyinka

Awood ku filan: Tas-hiilaad ku filan iyo farsamoyaqaanno

Adeegga Xirfadlaha: Adeegga iibsashada hal joogsi

Xidhmada OEM: Xidhmada gaarka ah iyo summada ayaa diyaar ah

Gaadhida Degdega ah: Haddii kaydku ku jiro, dammaanad bixinta saddex maalmood ah

Supply xasiloon: Hayso kayd macquul ah

Taageerada Farsamada: Xalka tignoolajiyada waa la heli karaa

Adeegga Isku-dhafka Gaarka ah: Wuxuu u dhexeeyaa garaam ilaa kiilo

Tayo Sare: Waxaa la sameeyay nidaam hubinta tayada dhamaystiran

FAQ:

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13220-33-2 - Khatarta iyo Badbaadada:

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13220-33-2 - Codsiga:

1-Methyl-3-Pyrrolidinol (3-Hydroxy-1-Methylpyrrolidine) (CAS: 13220-33-2) waxaa loo isticmaalaa sidii dhexdhexaad ah oo isku dhafan oo dabiici ah, oo loo isticmaalo dhexdhexaadinta dawooyinka ee warshadaha dawooyinka.