6-Aminohexanoic Acid CAS 60-32-2 (ε-aminocaproic Acid) Assay 98.5~100.5% Warshada

6-Aminohexanoic Acid (ε-aminocaproic Acid) (CAS: 60-32-2) Habka Imtixaanka AJI97
Aminocaproic acid, marka lagu xisaabiyo ku salaysan anhydrous, waxa uu ka kooban yahay aan ka yarayn 98.5 boqolkiiba oo aan ka badnayn 100.5 boqolkiiba Aminocaproic Acid (C6H13NO2).
Sharaxaad: Kiristaalo cad ama budo crystalline, dhadhan qadhaadh ah.
Si xor ah ugu milmay biyaha iyo glacial acetic acid, wax yar ku milmay methanol, ficil ahaan aan lagu milmi karin ethanol.
Solubility (H2O, g/100g): Si xor ah ugu milmay biyaha
Aqoonsiga: Is barbar dhig nooca nuugista infrared-ka ee muunada iyo kan heerka caadiga ah ee habka saxanka bromide ee potassium.
Tilmaamaha:
Xaaladda Xalka ( Gudbinta): 0.5g gudaha 10ml ee H2O, spectrophotometer, 430nm, dhumucda unugga 10mm.
Chloride (Cl): 0.7g, A-1, tixraac: 0.40ml ee 0.01mol/L HCl
Ammonium (NH4): B-1
Sulfate (SO4): 1.2g, (1), tixraac: 0.50ml ee 0.005mol/L H2SO4
Birta (Fe): 0.5g, tixraac: 1.5ml ee Iron Std.(0.01mg/ml)
Biraha culus (Pb): 2.0g, (1), pH=7, tixraac: 2.0ml ee Pb Std.(0.01mg/ml)
Arsenic (As2O3): 2.0g, (1), tixraac: 2.0ml ee As2O3 Std.
Amino Acids kale: Tijaabada tijaabada: 100μg, B-1-a, xakamaynta;ε-Acp 0.6μg
Biyaha: 500mg, methanol: ethyleneglycol (1:2) ee habka Karl Fischer, A, 15 daqiiqo.
Hadhaaga dabka (Sulfated): AJI Test 13
Qiimaynta: Muunad lagu xisaabay ku salaysan anhydrous, 130mg, (1), 3ml of formic acid, 50ml of glacial acetic acid, 0.1mol/L HCLO4 1ml=13.117mg C6H13NO2
pH: 1.0g gudaha 10ml ee H2O
Xadka kaydinta lagu taliyay iyo xaalada: weelasha adag ee la ilaaliyo ee heerkulka qolka la kantaroolay (2 sano).

6-Aminohexanoic Acid (ε-Aminocaproic Acid) (CAS: 60-32-2) Habka Tijaabada USP35
Aminocaproic acid waxa uu ka kooban yahay wax aan ka yarayn 98.5 boqolkiiba kana badnayn 101.5 boqolkiiba C6H13NO2, oo lagu xisaabiyo ku salaysan anhydrous.
Baakadaha iyo kaydinta-Ku xafid weel cidhiidhi ah.Ku kaydi heerkulka qolka.
Heerarka Tixraaca USP <11>-
USP Aminocaproic Acid RS
Aqoonsiga, Nuugista Infrared <197K>.
Biyaha, Habka I <921>: aan ka badnayn 0.5%.
Hadhaaga dabka <281>: aan ka badnayn 0.1%.
Biraha culus, Habka II <231>: 0.002%.
Imtixaan-
Xalka A-Ku wareeji 0.55 g sodium 1-heptanesulfonate ilaa 1000-mL weel mug leh, ku milmi oo ku qas biyo mugga, oo isku qas.
Marxaladda wareegta-Ku wareeji 10 g oo ah fosfat potassium monobasic ilaa 1000-mL beaker, ku milmi 300 ml oo Xalka A, ku dar 250 ml oo methanol ah, oo ay ku xigto 300 ml oo kale oo Xalka A ah, oo isku walaaq.Ku hagaaji isku dhafka fosfooraska acid pH ah 2.2.Ku wareeji isku dhafka oo dhan ilaa 1000-mL weel mug leh, ku milo Solution A si mugga, iyo qas.Shaandhayso iyo degas.Samee hagaajin haddii loo baahdo (eeg Habboonaanta Nidaamka ee hoos timaada Chromatography <621>).
Xalka caadiga ah ee gudaha-Ku diyaari xal methionine ah oo biyo ah oo ka kooban 1.25 mg halkii ml.
Diyaargarowga caadiga ah-Ku milmaan tirada saxda ah ee USP Aminocaproic Acid RS ee biyaha si aad u hesho xal kayd ah oo la og yahay oo ah 12.5 mg halkii ml.Ku wareeji 5.0 mL ee xalalka kaydka ilaa 100-mL weel mug leh, ku dar 2.0 mL ee xalka caadiga ah ee gudaha, ku qas biyo mugga, oo qas.
Diyaarinta Assay-Ku wareeji tiro sax ah oo la miisaamay oo ah 1.25 g oo Aminocaproic Acid ilaa 100-mL weel mug leh, ku milmi oo ku milmaan biyo ilaa mug, oo qas.Ku wareeji 5.0 mL ee xalkan ilaa 100-mL weel mug leh, ku dar 2.0mL ee xalinta heerka gudaha, ku milo biyo ilaa mug, oo qas.
Nadaamka Chromatographic (eeg Chromatography <621>)-Kromaatograph-ka dareeraha ah waxa uu ku qalabaysan yahay 210-nm qalabka wax baadha iyo tiir 4.6-mm × 15-cm ah oo ka kooban baakad L1 waxaana lagu hayaa 30°.Heerka socodka waa qiyaastii 0.7 mL daqiiqadii.Chromatograph ee heerka diyaarinta, oo diwaangeli jawaabaha ugu sarreeya sida lagu faray Habka: waqtiyada haynta qaraabo waxay ku dhow yihiin 0.76 ee aminocaproic acid iyo 1.0 ee methionine;xallinta, R, inta u dhaxaysa aminocaproic acid iyo methionine waa mid aan ka yarayn 2.0;iyo weecasho heerka qaraabo ah ee cirbadaha soo noqnoqda kama badna 2.0%.
Habka-Si gooni ah u duri mugga siman (qiyaastii 20 µL) ee diyaarinta Heerka iyo diyaarinta Assay chromatograph-ka, una ogolow diyaarinta Assay in ay sare u kacdo wax aan ka yarayn laba jeer wakhtiga haynta aminocaproic acid.Qor chromatogram-yada, oo cabbir dhammaan jawaabaha ugu sarreeya.Xisaabi tirada, g, ee C6H13NO2 ee qaybta Aminocaproic Acid ee ay qaadatay qaacidada:
2C (RU / RS)
taas oo C ay tahay fiirsashada, mg per mL, ee USP Aminocaproic Acid RS ee diyaarinta Standard;iyo RU iyo RS waa saamiga jawaabta aminocaproic acid ee jawaabta ugu sarreysa ee gudaha ee laga helay diyaarinta Assay iyo diyaarinta Heerka, siday u kala horreeyaan.