(Boc) 2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity>99.0% (HPLC) Warshada Ilaalinta Reagent
Shanghai Ruifu Chemical Co., Ltd. waa saaraha ugu horreeya ee Di-tert-Butyl Iminodicarboxylate ((Boc) 2NH) (CAS: 51779-32-9) oo leh tayo sare leh.Kiimikada Ruifu waxay keentaa reagen-ilaalin taxane ah iyo reagen-yaasha isku xidha.Waxaan bixin karnaa gaarsiinta adduunka oo dhan, qiimo tartan ah, tiro yar iyo tiro badan oo la heli karo.Iibso Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com
Magaca Kiimikada | Di-tert-Butyl Iminodicarboxylate |
La mid ah | (Boc)2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic acid Di-tert-Butyl Ester;Bis (tert-Butoxycarbonyl) ammonia |
Heerka Saamiyada | In Stock |
Lambarka CAS | 51779-32-9 |
Qaanuunka molecular | C10H19NO4 |
Miisaanka Molecular | 217.27 g/mol |
Meesha dhalaalaysa | 114.0 ~ 120.0 ℃ |
Cufnaanta | 1.037± 0.06 g/cm3 |
Xasaasi ah | Xasaasiyadda Hawada, Xasaasiyadda Fudud |
Biyuhu milmayn | Aan ku milmin Biyaha |
Solubility | Chloroform, methanol |
Heerkulka Kaydinta | Meel Qabow & Qallalan (2 ~ 8 ℃) |
COA & MSDS | La heli karo |
Qaybta | Ilaalinta Reagents |
Summada | Kiimikada Ruifu |
Walxaha | Heerarka Kormeerka | Natiijooyinka |
Muuqashada | Budada Crystalline White | U hogaansama |
Meesha dhalaalaysa | 114.0 ~ 120.0 ℃ | 118.8 ~ 119.3 ℃ |
Khasaare xagga qalajinta | <0.50% | 0.10% |
Daahirnimada / Habka Falanqaynta | >99.0% (HPLC) | 99.6% |
Infrared Spectrum | Waafaqsan Qaab-dhismeedka | U hogaansama |
NMR Spectrum | Waafaqsan Qaab-dhismeedka | U hogaansama |
Gabagabo | Alaabta waa la tijaabiyay oo waafaqay tilmaamihii la bixiyay |
Tiirka Chromatographic: SE-54 30m×0.25mm×0.5μm;
Baaraha: FID
Heerkulka hore: 100 ℃
Muddada hore: 1 daqiiqo
Heerka kulaylka: 20 ℃ / daq
Heerkulka kama dambaysta ah: 190 ℃
Dhamaadka: 10min
Heerkulka cirbadeynta: 160 ℃
Heerkulka qalabka wax lagu baadho: 200 ℃
Saamiga kala qaybsan: 50:1;
Cabbirka Tusaalaha: 0.2μl;
Dheecaan: methanol
Natiijadu: Nadiifintu waxay ka badnayd 99.0% habka caadiga ah ee aagga.
Xidhmada:Dhalo, bacda bireed ee aluminium, 25kg/Drum kartoonada, ama sida waafaqsan shuruudaha macmiilka.
Xaaladda Kaydinta:Ku kaydi weelasha xidhan meel qabow oo engegan (2 ~ 8℃) bakhaar ka fog walxaha aan ku haboonayn.Ka ilaali iftiinka iyo qoyaanka.
Rarida:Gaarsiiya adduunka oo dhan FedEx/DHL Express.Bixi keenid degdeg ah oo la isku halayn karo.
Sidee loo Iibsadaa?Fadlan la xidhiidhDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Khibrad 15 Sano ah?Waxaan leenahay in ka badan 15 sano oo waayo-aragnimo ah oo ku saabsan soo saarista iyo dhoofinta ee tiro balaadhan oo ah dhexdhexaad ah daawooyinka tayada sare leh ama kiimikooyinka ganaax.
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Faa'iidooyinka?Tayada sare, qiimo jaban, adeegyo xirfadeed iyo taageero farsamo, gaarsiin degdeg ah.
TayadaHubinta?Nidaamka xakamaynta tayada adag.Qalabka xirfadlayaasha ah ee falanqaynta waxaa ka mid ah NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Imtixaanka xadka Microbial, iwm.
Tusaalooyinka?Badeecadaha intooda badani waxay bixiyaan muunado bilaash ah oo loogu talagalay qiimeynta tayada, kharashka dhoofinta waa in ay bixiyaan macaamiisha.
Hantidhawrka Warshada?Hantidhawrka warshada soo dhawoow.Fadlan horay u sii ballan.
MOQ?Ma jiro MOQ.Dalabka yar waa la aqbali karaa.
Waqtiga dirida? Haddii ay ku jirto kaydka, dammaanad bixinta saddex maalmood ah.
Gaadiidka?By Express (FedEx, DHL), hawada, badda.
Dukumentiyada?Adeegga iibka kadib: COA, MOA, ROS, MSDS, iwm waa la bixin karaa.
Isku-dhafka gaarka ah?Waxay ku siin kartaa adeegyada isku-dhafka gaarka ah si ay ugu habboonaato baahiyahaaga cilmi-baarista.
Shuruudaha Lacag-bixinta?Qaansheegga Proforma ayaa marka hore la soo diri doonaa ka dib marka la xaqiijiyo dalabka, oo lagu soo lifaaqay macluumaadka bangigayaga.Lacag bixinta T/T (Telex Transfer), PayPal, Western Union, iwm.
Calaamadaha halista Xi - xanaaq badan
Xeerarka halista 36/37/38 - Ka xanaajiya indhaha, habdhiska neefsiga iyo maqaarka.
Sharaxaada Badbaadada S26 - Haddii ay dhacdo in indhaha la taabto, isla markiiba ku raaci biyo badan oo raadso talo caafimaad.
S37/39 - Xidho galoofyada ku haboon iyo ilaalinta indhaha/wejiga
WGK Germany 3
HS code 29241990
Xusuusin Khatarta Irritant
Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Codsiga Di-tert-Butyl Iminodicarboxylate waa dhexdhexaadiye dawooyin ah, kaas oo lagu diyaarin karo falcelin hal-tallaabo ah oo ah formamide iyo Boc2O.
Xarunta waxa loo isticmaalaa sidii reagement ahaan diyaarinta aminyada aasaasiga ah ee ka imanaya alkyl halides.Waxa loo caan baxay beddelka isku-dhafka Jibriil ee isla beddelidda.Amines waxaa sidoo kale laga diyaarin karaa khamriga iyadoo fuuqbaxa la isticmaalayo falcelinta Mitsunobu.Hirgelinta caadiga ah reagent waa la damiyaa si loo siiyo milixda potassium, taas oo ah N-alkylated.Kooxaha ilaalinta Boc ayaa markaa ka dib laga saaray xaaladaha acidic.
Di-tert-Butyl Iminodicarboxylate waa koox aamin ah oo la ilaaliyo oo loo isticmaalo in lagu diyaariyo spirocycles xaddidan sida CCR1 antagonists.
Diyaarinta xalka DMAP (0.61g, 5.0mmol) ee MeCN (15ml) ayaa si tartiib ah loogu daraa xalka foramide (2.5g,56mmol) iyo Boc2O (24)g, 110mol) gudaha MeCN (15ml).Ka dib markii lagu walaaqay heerkulka qolka 4h, xal jaalaha ah ayaa la qaboojiyey ilaa 0 ° C, N, N-diethylenediamine (6.97g, 60mmol) ayaa si tartiib ah loogu daray 0 ℃.Isku darka natiijada waxaa lagu walaaqay heerkulka qolka 12h waxaana lagu sifeeyaa suuf khafiif ah oo silica ah;isku darka ka dhashay waxaa lagu sifeeyay heerkulka qolka.Walxaha ayaa markaa ku soo baxa cadaadis yar.Alaabada cayriin waxaa lagu sifeeyay silica gel chromatography waxaana lagu nadiifiyay EtOAc/hexane (1: 5) si loo helo badeecada lahaanshaha, taas oo ah cad cad (10.99g, 92%).