Inosine CAS 58-63-9 Assay 98.0 ~ 102.0% Warshada Tayada Sare

Inosine (CAS: 58-63-9) Habka Imtixaanka ChP2020
Inosin - QEEXAAD
Waxa ku jira C10H12N4O5 waa inay ahaataa inta u dhaxaysa 98.0% iyo 102.0% ee lagu xisaabiyo alaabta la qalajiyey.
Inosine - Sifo Alaabtani waa budada crystalline cad;Aan ur lahayn.Alaabtani wax yar bay ku milmi kartaa biyaha, kuma milmi karaan ethanol, waxayna ku milmi kartaa acid hydrochloric iyo milanka sodium hydroxide.
Inosin - AQOONSI
1. Qaado qiyaasta saxda ah ee 0.01% xalalka alaabtan, ku dar mugga siman ee 3, 5-dihydroxytoluene (qaado 3, 5-dihydroxytoluene iyo ferric chloride 0.lg, ku dar acid hydrochloric si aad u sameyso 100ml), si fiican isku qas, ka dib. kuleylinta biyaha qubeyska ilaa 10 daqiiqo, midab cagaaran ayaa la arkay.
2. chromatogram-ka lagu duubay sheyga go'aaminta nuxurka, wakhtiga haynta ee ugu sarraysa ee xalka tijaabada waa in uu ahaado mid la jaan qaada wakhtiga haynta ee ugu sarreysa xalka tixraaca.
3. Muuqaalka nuugista infrared ee alaabtan waa in ay la socotaa kan kantaroolka (Spectrum set 605).
Inosin - Falanqaynta
Gudbinta Xalka
Qaado 0.5g oo badeecadan ah, ku dar 50ml oo biyo ah si aad u milmaan, marka loo eego spectrophotometry UV-visible (Sharciga Guud 0401), go'aami gudbinta 430nm dhererka hirarka, aan ka yarayn 98.0%.(Dirridda)
Walxaha laxidhiidha
Qaado alaabtan, ku dar biyo si aad u milmaan oo u milo si aad u samayso xal ka kooban 0.5mg halkii 1ml sida xal tijaabo ah;Qaado 1ml cabbirka saxda ah, ku rid weel 100ml ah oo cabbir ah, ku qas biyo ilaa cabbirka, si loo xakameeyo.Marka loo eego xaaladaha chromatographic ee hoos yimaada shayga go'aaminta nuxurka, 20 u1 ee xalka tijaabada iyo xalinta xakamaynta ayaa siday u kala horreeyaan loo duraa chromatograph-ka dareeraha ah, iyo chromatogram-ka waxaa loo diiwaangeliyaa 2 jeer wakhtiga haynta ee ugu sarreysa.Haddii ay jiraan meelaha ugu sarreeya ee wasakhda ah ee chromatogram-ka ee xalka tijaabada, wadarta meel kasta oo ugu sarreysa wasakhdu waa in aanay ka badnaan aagga ugu sarreeya ee xalka xakamaynta (1.0%).
Khasaare xagga qalajinta
Qaado alaabtan, engegan ilaa miisaan joogto ah 105 ° C, miisaan lumis waa inuusan dhaafin 1.0% (Xeerka Guud 0831).
Hadhaaga dabka (Sulfated)
Aan ka badnayn 0.1% (duritaan), ama aan ka badnayn 0.2% (isticmaalka afka) (Xeerka guud 0841).
Biraha culus
Qaado badeecadan 1.0g, kormeer sida uu qabo sharciga (Mabaadi'da Guud 0821 sharciga labaad), ka kooban biraha culus waa in aanay ka badan 10 qaybood halkii milyan.
Sunta aan caadiga ahayn
Qaado alaabtan, ku dar duritaanka sodium chloride si aad u milmaan oo u milo xalka ay ku jirto inosine 10mg halkii 1ml, hubi sida waafaqsan sharciga (Xeerka Guud ee 1141), waa in uu u hoggaansamaa qodobada.(Dirridda)
Inosine - go'aaminta nuxurka
Lagu cabbiray Waxqabadka Sare ee Chromatography (Guud 0512).
Xaaladaha Chromatographic iyo ku habboonaanta nidaamka tijaabada jel silica oo ku xidhan siddeed iyo toban alkyl silane ayaa loo adeegsaday buuxin ahaan;Methanol-water (10:90) ayaa loo isticmaalay sidii wejiga guurguura;Dhererka hirarka ogaanshaha wuxuu ahaa 248nm.Qaado qiyaastii 10mg oo tixraac ah inosin, ku dar 1 mol/L hydrochloric acid (1ml), kulayl biyaha qubeyska 80 ℃ 10 daqiiqo, ha qaboojiso, ku dar 1ml of 1 mol/L sodium hydroxide xal, ku dar biyo 50ml 20u1 duritaanka chromatograph dareere dareere ah, hagaajin nidaamka chromatographic, heerka kala soocidda ugu sarreysa inosine iyo ugu sarreysa nijaasta ku xiga waa in ay buuxiyaan shuruudaha, tirada saxan teori marka loo eego xisaabinta peak inosine aan ka yarayn 2000.
Qiimayn
Qaado qadar ku habboon alaabtan, si sax ah u miisaan, ku dar biyo si ay u milaan oo qiyaas ahaan u milo si aad u samayso xal ka kooban 20ug halkii lml, rux, oo u isticmaal sidii xal tijaabo ah, A 20ul cirbadeynta dareeraha chromatograph si sax ah ayaa loo qiyaasay chromatogramka ayaa la duubay.Qadarka saxda ah ee tixraaca inosine-ka ayaa si sax ah loo miisaamay waxaana lagu go'aamiyay hab la mid ah, iyo aagga ugu sarreeya waxaa loo xisaabiyay habka caadiga ah ee dibadda.
Inosine - Qaybta
Dheef-shiid kiimikaadka unugyada hagaajinta daawooyinka.
Inosin - Kaydinta
Gaashaanka khafiifka ah, kaydinta daboolan.
Dawada