L-(+)-Lysine Monohydrochloride CAS 657-27-2 (H-Lys-OH·HCl) Qiimaynta 98.5 ~ 101.0% Warshada Tayada Sare
Shanghai Ruifu Chemical Co., Ltd. waa soo saaraha ugu horreeya iyo alaab-qeybiyaha L- (+) - Lysine Monohydrochloride (H-Lys-OH · HCl) (CAS: 657-27-2) oo leh tayo sare leh, awood wax soo saar 1000 Tons per sanad.Sida mid ka mid ah alaab-qeybiyeyaasha amino acids-ka ugu weyn Shiinaha, Kiimikada Ruifu waxay siisa asiidhyada amino-ka ilaa heerarka caalamiga ah, sida AJI, USP, EP, JP iyo heerarka FCC.Waxaan bixin karnaa COA, gaarsiinta adduunka oo dhan, tiro yar iyo tiro badan oo la heli karo.Haddii aad xiisaynayso L-(+)-Lysine Monohydrochloride,Please contact: alvin@ruifuchem.com
| Magaca Kiimikada | L-(+)-Lysine Monohydrochloride |
| La mid ah | H-Lys-OH·HCl;L-Lysine Monohydrochloride;L-Lysine Hydrochloride;L-Lysine HCl;Laevo-Lysine Hydrochloride;Lysine Hydrochloride;Lysine monohydrochloride;(S)-2,6-Diaminohexanoic Acid Monohydrochloride |
| Heerka Saamiyada | Kaydka dhexdiisa, Awood Wax-soo-saar 1000 Tan sannadkii |
| Lambarka CAS | 657-27-2 |
| Qaanuunka molecular | C6H14N2O2·HCl |
| Miisaanka Molecular | 182.65 |
| Meesha dhalaalaysa | 263 ℃ (dac.) |
| Cufnaanta | 1.28 g/cm3 (20 ℃) |
| Biyuhu milmayn | Ku milmay Biyaha, Ku dhawaad Hufnaan |
| Solubility | Si Xor Ah Ugu milmay Biyaha iyo Ashitada Formic.Wax yar oo ku milma Ethanol.Dhaqan ahaan Aan La Dhaafin karin Ether |
| Heerkulka Kaydinta | Lagu xidhay qalalan, ku kaydi heerkulka qolka |
| COA & MSDS | La heli karo |
| Kala soocidda | Amino Acid iyo Darevatives |
| Summada | Kiimikada Ruifu |
| Xeerarka Khatarta | 34 - Sababaha gubashada |
| Sharaxaada Badbaadada | S24/25 - Iska ilaali taabashada maqaarka iyo indhaha. |
| Aqoonsiga UN-ka | UN 1789 8/PG 3 |
| WGK Germany | 2 |
| Koodhka HS | 2922419000 |
| Walxaha | Heerarka Kormeerka | Natiijooyinka |
| Muuqashada | Crystals cad ama budada crystalline | waafaqsan |
| Aqoonsiga | Nuugista Infrared Spectrum | waafaqsan |
| Wareeg gaar ah [α]20/D | +20.4° ilaa +21.4°(C=8 gudaha 6N HCl) | +20.8° |
| Xaaladda Xalka ( Gudbinta) | Cad iyo Midab la'aan ≥98.0% | 98.8% |
| Chloride (Cl) | 19.0 ilaa 19.6% | 19.15% |
| Sulfate (SO4) | ≤0.020% | <0.020% |
| Ammonium (NH4) | ≤0.020% | <0.020% |
| Birta (Fe) | ≤10pm | <10pm |
| Biraha culus (Pb) | ≤10pm | <10pm |
| Arsenic (As2O3) | ≤1.0pm | <1.0pm |
| Amino Acids kale | ≤0.50% (TLC) | waafaqsan |
| Khasaare xagga qalajinta | ≤0.40% (105 ℃ ilaa 3 saacadood) | 0.25% |
| Hadhaaga dabka (Sulfated) | ≤0.10% | 0.06% |
| Qiimayn | 98.5 ilaa 101.5% (sida Asal qallalan) | 99.7% |
| Waxyaalaha wasakhaysan ee Dabiiciga ah | Buuxi Shuruudaha | waafaqsan |
| Tijaabada pH | 5.0 ilaa 6.0 (1.0g ee 10ml ee H2O) | 5.2 |
| Xalalka Haraaga ah | waafaqsan | waafaqsan |
| Gabagabo | La kulmay heerka AJI97;USP;JP | |
| Nolosha shelf | 24 bilood laga bilaabo taariikhda wax soo saarka haddii si sax ah loo kaydiyo | |
| Isticmaalka Muhiimka ah | Amino Acids;Cuntada lagu daro / Quudinta;Daawooyinka;Kobciyaha Nafaqada;iwm. | |
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) AJI 97 Habka Tijaabada
Aqoonsiga: Is barbar dhig nooca nuugista infrared-ka ee muunada iyo kan heerka caadiga ah ee habka saxanka bromide ee potassium.
Wareegga Gaarka ah [α]20/D: Muunad la qallajiyey, C=8, 6mol/L HCl
Xaaladda Xalka ( Gudbinta): 1.0g gudaha 10ml ee H2O spectrophotometer, 430nm, dhumucda unugyada 10nm.
Chloride (Cl): Muunad qallalan, 370mg, B-1
Ammonium (NH4): B-1
Sulfate (SO4): 1.2g, (1), tixraac: 0.50ml ee 0.005mol/L H2SO4
Birta (Fe): 1.5g, (1), tixraac: 1.5ml ee Iron Std.(0.01mg/ml)
Biraha culus (Pb): 2.0g, (4), tixraac: 2.0ml ee Pb Std.(0.01mg/ml)
Arsenic (As2O3): 2.0g, (1), tixraac: 2.0ml ee As2O3 Std.
Amino Acids kale: Tusaalaha Tijaabada: 50μg, S-6-a, xakamaynta: L-Lys HCl 0.25μg
Luminta qallajinta: at 105 ℃ 3 saacadood.
Qiimaynta: Muunad qallalan, 110mg, (3), 2ml oo ah aashitada formic, 0.1mol/L HCLO4 1ml=9.133mg C6H14N2O2·HCl
Tijaabada pH: 1.0g gudaha 10ml ee H2O
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) Habka Tijaabada USP35
Qeexitaan
Lysine Hydrochloride waxay ka kooban tahay NLT 98.5% iyo NMT 101.5% ee L-Lysine Hydrochloride (C6H14N2O2·HCl), oo lagu xisaabiyo sal qallalan.
AQOONSIGA
A. NUUXDA INFRAREED <197K>
ASSAY
HABKA
Tusaale: 90 mg oo ah Lysine Hydrochloride
Madhan: Isku qas 3 ml oo ah aashitada formic iyo 50 ml oo ah glacial acetic acid.
Nidaamka Titrimetric
(Fiiri Titrimetry <541>)
Habka: Titration toos ah
Titrant: 0.1 N perchloric acid VS
Ogaanshaha barta dhamaadka: Potentiometric
Falanqaynta: Ku mil muunada 3 mL oo ah ashitada formic iyo 50ml ee glacial acetic acid.Ku dar 10 ml oo ah mercuric acetate TS, oo titrate ku dar Titrant.Samee go'aanka maran.
Xisaabi boqolkiiba Lysine Hydrochloride (C6H14N2O2·HCl) ee muunadda la qaaday:
Natiijadu = {[(VS-VB) xNxF]/W} x100
VS= Mugga titrant ee uu isticmaalo Tusaalaha (mL)
VB= Mugga titrant ee uu isticmaalo Bannaanka (mL)
N= Caadiga dhabta ah ee Titrant (mEq/ml)
F= qodob u dhigma, 91.33 mg/mEq
W= Miisaanka Tusaalaha (mg)
Shuruudaha aqbalaadda: 98.5% ~ 101.5% ee salka qallalan
QAYBO KALE
WAXYAABAHA KOLORIDKA
Tusaale: 350 mg oo ah Lysine Hydrochloride
maran: 140 ml oo biyo ah
Nidaamka Titrimetric
(Fiiri Titrimetry <541>)
Habka: Titration toos ah
Titrant: 0.1 N nitrate silver VS
Ogaanshaha barta dhamaadka: Muuqaal
Falanqaynta: Ku beddel muunadda dhalada foornada, oo ku dar 140 ml oo biyo ah iyo 1 ml oo dichlorofluorescein TS ah.Ku xidh Titrant-ka ilaa chloride-ka qalinka ahi uu soo wareego oo isku darku uu helo midab casaan ah oo daciif ah.Samee go'aanka maran.
Xisaabi boqolleyda chloride (Cl) ee ku jira Tusaalaha la qaaday:
Natiijadu = {[(VS − VB) × N × F]/W} × 100
VS = Mugga titrant ee uu isticmaalo Tusaalaha (mL)
VB = Mugga titrant ee uu isticmaalo Bannaanka (mL)
N = Caadiga dhabta ah ee Titrant (mEq/ml)
F = qodob u dhigma, 35.45 mg/mEq
W = Tusaalaha miisaanka (mg)
Shuruudaha aqbalaadda: 19.0% ~ 19.6%
XANUUNKA
Hadhaaga dabka <281>: NMT 0.1%
Kloride iyo sulfate, Sulfate <221>
Xalka caadiga ah: 0.10ml of 0.020 N sulfuric acid
Tusaalaha: 0.33g of Lysine Hydrochloride
Shuruudaha aqbalaadda: NMT 0.03%
IRON <241>: NMT 30ppm
Tirtir waxyaabaha soo socda:
Biraha culus, Habka I <231>: NMT 15ppm
KALA XIRIIR
Xalka caadiga ah: 0.05 mg/mL ee USP L-Lysine Hydrochloride RS ee biyaha.[FIIRO GAAR AH-Xalkani waxa uu leeyahay fiirsi u dhigma 0.5% ee xalka Tusaalaha.]
Xalka muunada: 10mg/ml ee Lysine Hydrochloride ee biyaha
Xalka ku habboonaanta nidaamka: 0.4 mg/mL midkiiba USP L-Lysine Hydrochloride RS iyo USP Arginine Hydrochloride RS
Nadaamka Chromatographic (Eeg Chromatography <621>, Chromatography ee khafiifka ah.)
Habka: TLC
Adsorbent: 0.25-mm lakabka silica jel chromatographic ah
Codsiga mugga: 5μL
Horumarinta habka dareeraha: isopropyl khamriga iyo ammonium hydroxide (7: 3)
Daawada reagent: 0.2 g oo ninhydrin ah oo isku dar ah alkolada butyl iyo 2N acetic acid (95:5)
Ku habboonaanta nidaamka
Shuruudaha ku habboonaanta: chromatogram-ka xalka ku habboonaanta nidaamka wuxuu muujinayaa laba baro oo si cad u kala soocan.
Falanqaynta
Tusaalooyinka: Xalka caadiga ah, Xalka ku habboonaanta nidaamka, iyo Tusaalaha xalka.
Qalaji saxanka inta u dhaxaysa 100 ° iyo 105° ilaa ammonia ay gebi ahaanba baaba'do.Ku buufin reagent buufin, oo kuleyl u dhexeeya 100 ° iyo 105 ° 15 daqiiqo.Ku baadh saxanka hoostiisa iftiin cad.
Shuruudaha aqbalaadda: Meel kasta oo labaad ee xalka Tusaalaha kama weyna ama kama xoog badna meesha ugu muhiimsan ee xalinta caadiga ah.
Nijaasaha shaqsiga ah: NMT 0.5%
Wadarta wasakhda: NMT 2.0%
IMTIXAANO GAAR AH
Wareegga indhaha, wareeg gaar ah <781S>
Xalka muunada: 80 mg/ml ee 6 N hydrochloric acid
Shuruudaha aqbalaadda: +20.4° ilaa +21.4°
LOSSON QALABKA <731>: Ku qalaji muunad 105 ℃ 3 saacadood: waxay luminaysaa NMT 0.4% miisaankeeda.
SHURUUD DHEERAAD AH
Baakadaha iyo Kaydinta: Ku kaydi weelasha si fiican u xidhan.
HEERARKA Tixraaca USP <11>
USP Arginine Hydrochloride RS
USP L-Lysine Hydrochloride RS
L-(+)-Lysine Monohydrochloride (CAS: 657-27-2) JP17 Habka Tijaabada
L-Lysine Hydrochloride, marka la qalajiyo, waxay ka kooban tahay wax aan ka yarayn 98.5% ee L-lysine hydrochloride (C6H14N2O2.HCl).
DescriptionL-Lysine Hydrochloride waxay u dhacdaa sida budo cad.Waxay leedahay dhadhan sifadeed.
Waxay si xor ah ugu milmay biyaha iyo aashitada formic, iyo ficil ahaan aan lagu milmi karin ethanol (95).
Waxay muujinaysaa polymorphism crystal.
Aqoonsiga (1) Go'aami qaabka nuugista infrared ee L-Lysine Hydrochloride, oo hore loo qalajiyey, sida lagu faray habka potassium bromide disk ee hoos yimaada Spectrophotometry Infrared <2.25>, oo barbar dhig spectrum iyo Spectrum tixraaca: labadaba spectra waxay muujinayaan xoojinta nuugista ee isku midka ah tirooyinka mawjadaha isku midka ah.Haddii wax farqi ahi u dhexeeyo spectra, ku mil L-Lysine Hydrochloride biyaha, uumi-baxa biyaha si ay u engegaan 60 ℃, oo ku celi tijaabada hadhaaga.
(2) Xalka L-Lysine Hydrochloride (1kii 10) ayaa ka jawaabaya Tijaabada tayada <1.09> ee chloride.
Wareegga indhaha <2.49>[α]20/D: +19.0 - +21.5° (ka dib qalajinta, 2 g, 6 mol/L hydrochloric acid TS, 25 mL, 100 mm)
pH <2.54> Ku mil 1.0 g oo L-Lysine Hydrochloride ah 10 ml oo biyo ah: pH ee xalkani waxa uu u dhexeeyaa 5.0 iyo 6.0.
Nadiif (1) Cadnaanta iyo midabka xalka-Ku mil 1.0 g oo L-Lysine Hydrochloride ah 10 ml oo biyo ah: xalku waa cad yahay oo aan midab lahayn.
(2) Sulfate <1.14>-Ku samee tijaabada 0.6 g oo ah L-Lysine Hydrochloride.Ku diyaari xalka xakamaynta 0.35 mL ee 0.005 mol/L sulfuric acid VS (aan ka badnayn 0.028%).
(3) Ammonium <1.02>-Ku samee tijaabada 0.25 g oo ah L-Lysine Hydrochloride.Ku diyaari xalinta xakamaynta 5.0 mL ee Heerka Ammonium Solution (aan ka badnayn 0.02%).
(4) Biraha culus <1.07>- Ku wad 2.0 g oo ah L-Lysine Hydrochloride sida waafaqsan Habka 1, oo samee tijaabada.Ku diyaari xalka xakamaynta 2.0 mL ee Xalinta Lead Heerka (aan ka badnayn 10 ppm).
(5) Arsenic <1.11>-Ku diyaari xalka tijaabada 1.0 g ee L-Lysine Hydrochloride sida waafaqsan Habka 1, oo samee tijaabada (aan ka badnayn 2 ppm).
(6) Walxaha laxidhiidha-Ku mil 0.10 g ee L-Lysine Hydrochloride 25 ml oo biyo ah, una isticmaal xalkan sida xal muunad ah.Beet 1 ml oo muunada muunada ah, ku dar biyo si aad u samayso 50 ml oo sax ah, pipet 5 mL ee xalkan, ku dar biyo si aad u samayso 20 ml oo sax ah, una isticmaal xalkan sida xalka caadiga ah.Ku samee tijaabada xalalkan sida lagu faray Chromatography-ka khafiifka ah <2.03>.Bar 5μL mid kasta oo ka mid ah muunadda muunada iyo xalalka caadiga ah ee saxan jel silica ah oo loogu talagalay chromatography-daaha khafiifka ah.Ku samee saxanka isku dar ah 1-propanol iyo biyaha ammonia (28) (67:33) ilaa fogaan dhan 10 cm, oo ku qalaji saxanka 100 ℃ 30 daqiiqo.Si siman ugu buufi saxanka adigoo isticmaalaya xal ninhydrin ah oo ku jira acetone (1kii 50) kuna kulayl 80 ℃ 5 daqiiqo: dhibco kale oo aan ahayn meesha ugu muhiimsan ee xalinta muunada ma aha kuwo ka xoog badan barta xalka caadiga ah.
Luminta qalajinta <2.41> In aan ka badnayn 1.0% (1 g, 105 ℃, 3 saacadood).
Hadhaaga dabka <2.44> In aan ka badnayn 0.1% (1 g).
Assay Si sax ah u miisaan qiyaastii 0.1 g oo ah L-Lysine Hydrochloride, oo hore loo qalajiyey, ku milmi 2 mL oo ah ashitada formic, ku dar 15 mL oo ah 0.1 mol/L perchloric acid VS, kuleyli biyaha qubeyska 30 daqiiqo.Ka dib qaboojinta, ku dar 45 mL oo acetic acid (100), iyo titrate <2.50> xad-dhaafka ah perchloric acid oo leh 0.1 mol/L sodium acetate VS (titration potentiometric).Samee go'aan maran, oo samee sixid kasta oo lagama maarmaan ah.
ml kasta oo ah 0.1 mol/L perchloric acid VS ＝9.132 mg ee C6H14N2O2.HCl
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L-(+)-Lysine Monohydrochloride (H-Lys-OH·HCl) (CAS: 657-27-2) waxaa si weyn loogu isticmaalaa kaabayaasha nafaqeynta ee warshadaha cuntada iyo cabitaanka.Waxa kale oo loo isticmaali karaa quudinta xoolaha sida isha L-Lysine.L-Lysine Monohydrochloride waxaa loo isticmaali karaa noocyo kala duwan oo warshado ah oo ay ku jiraan: wax soo saarka cuntada, cabitaanka, daawooyinka, beeraha / quudinta xoolaha, iyo warshado kale oo kala duwan.
Hawlaha Alaabta & Codsiyada:
1. Lysine HCL waa xoojiye nafaqeynta quudinta, kaas oo leh hawlaha kor u qaadida rabitaanka cuntada xoolaha iyo digaaga, hagaajinta caabbinta cudurada, kor u qaadida bogsashada nabarrada, hagaajinta tayada hilibka, kor u qaadida dheecaanka caloosha, iyo synthesize dareemayaasha maskaxda, unugyada jeermiska, borotiinada iyo hemoglobin lagama maarmaan ah. walxo.Guud ahaan qadarka lagu daray quudinta waa 0.1-0.2%.
2. Lysine HCL waa amino acid lagama maarmaanka u ah jidhka bini'aadamka, taas oo kor u qaadi karta shaqada hematopoietic, kor u qaadida dheecaanka casiirka gastric, kordhinta isticmaalka borotiinka, kordhiso caabbinta cudurada, ilaalinta dheelitirka dheef-shiid kiimikaadka, waxayna gacan ka geysataa horumarinta buug-yareedka kiimikada ee carruurta horumarka jireed iyo maskaxeed.Shiinaha ayaa dhigaya in bur, buskud iyo rooti loo isticmaali karo in lagu farsameeyo baasto la isticmaalo 1 ilaa 2g/kg;0.3 ilaa 0.8g/kg ee cabitaanka cabitaanka.
3. Lysine HCL waa mid ka mid ah asiidhyada amino ee ugu muhiimsan, iyo warshadaha amino acid hadda waxay noqdeen warshad miisaan iyo muhiimad la taaban karo leh.Lysine waxaa inta badan loo isticmaalaa cuntada, daawada iyo quudinta.
Shaqada:
1. Heerka cuntada: xoojiye nafaqeynta, oo loo isticmaalo xawaash ee majones, caanaha, cuntada baasto degdeg ah
2. Darajada daawada: diyaarinta isku shubista amino acid, hagaajinta waxtarka daawooyinka
3. Heerka quudinta: samee dheelitirnaanta nafaqada digaaga, wanaaji tayada hilibka iyo wax soo saarka
L-(+)-Lysine Monohydrochloride waxaa inta badan soo saara halsano iyadoo la isticmaalayo nuucyada corynebacteria, gaar ahaan Corynebacterium glutamicum, kaas oo ka kooban hannaan dhowr tallaabo ah oo ay ku jiraan halsano, kala soocidda unugga by centrifugation ama ultrafiltration, kala soocida alaabta iyo nadiifinta, uumiga iyo qalajinta.Sababtoo ah L-Lysine muhiimad weyn, dadaalka ayaa si joogto ah loo sameeyaa si loo hagaajiyo hababka halsano, oo ka kooban culeyska iyo horumarinta habka iyo sidoo kale hagaajinta warbaahinta iyo habka hoose ayaa loo isticmaalaa wax soo saarka L-lysine iyo kuwa kale ee L-amino acids, ka shaqaynta isku dhafka haanta ama kiishadaha hawada.
