L-Proline CAS 147-85-3 (H-Pro-OH) Assay 98.5 ~ 101.0% Warshada Tayada Sare
Shanghai Ruifu Kiimikada Co., Ltd. waa saaraha iyo soo saaraha ugu horreeya ee L-Proline (H-Pro-OH; Soo gaabinta Pro ama P) (CAS: 147-85-3) oo leh tayo sare leh, awoodda wax soo saarka 2000 Tons sannadkii.Sida mid ka mid ah alaab-qeybiyeyaasha amino acids-ka ugu weyn Shiinaha, Kiimikada Ruifu waxay siisa asiidhyada amino-ka ilaa heerarka caalamiga ah, sida AJI, USP, EP, JP iyo heerarka FCC.Waxaan bixin karnaa COA, gaarsiinta adduunka oo dhan, tiro yar iyo tiro badan oo la heli karo.Haddii aad xiisaynayso L-Proline,Please contact: alvin@ruifuchem.com
| Magaca Kiimikada | L-Proline |
| La mid ah | H-Pro-OH;L-(-)-Proline;L-Pro;La soo gaabiyey Pro ama P;Laevo-Proline;Proline;(-)-Proline;(S)-(-)-Proline;(S)-Proline;(S)-Pyrrolidine-2-Carboxylic Acid;(S)-2-Pyrrolidinecarboxylic acid;(-)-2-Pyrrolidinecarboxylic acid;L-Pyrrolidine-2-Carboxylic acid;L-a-Pyrrolidinecarboxylic acid;(S)-2-Carboxypyrrolidine |
| Heerka Saamiyada | Kaydka dhexdiisa, Awood Wax-soo-saar 2000 oo tan sannadkii |
| Lambarka CAS | 147-85-3 |
| Qaanuunka molecular | C5H9NO2 |
| Miisaanka Molecular | 115.13 |
| Meesha dhalaalaysa | 228 ℃ (dac.) ( shidan) |
| Cufnaanta | 1.35 |
| Xasaasi ah | Hygroscopic |
| Biyuhu milmayn | Ku milmay Biyaha, H2O: 50 mg/mL, Ku dhawaad daahfurnaan |
| Solubility | Si Xor Ah Ugu Soluble Glacial Acetic Acid, Ku Dhaafsan Kara EthanolDhaqan ahaan Aan lagu milmi karin Ether |
| Heerkulka Kaydinta | Lagu xidhay qalalan, ku kaydi heerkulka qolka |
| COA & MSDS | La heli karo |
| Kala soocidda | Amino Acids |
| Summada | Kiimikada Ruifu |
| Xeerarka Khatarta | Xi,Xn |
| Bayaanka Khatarta | R36/37/38 - Waxay ka xanaajisaa indhaha, habdhiska neefsiga iyo maqaarka. R22 - Waxyeelo leh haddii la liqo |
| Bayaanada Badbaadada | S24/25 - Iska ilaali taabashada maqaarka iyo indhaha. S36/37/39 - Xidho dhar ilaalin ku haboon, galoofyada iyo ilaalinta indhaha/wejiga. S26 - Haddii ay dhacdo in indhaha la taabto, isla markiiba ku raaci biyo badan oo raadso talo caafimaad. |
| WGK Germany | 3 |
| RTECS | TW3584000 |
| F | 3-10 |
| TSCA | Haa |
| Koodhka HS | 2933990099 |
| Walxaha | Heerarka Kormeerka | Natiijooyinka |
| Muuqashada | Crystals cad ama budada crystalline;Dhadhan yar oo macaan | waafaqsan |
| Aqoonsiga | Nuugista Infrared Spectrum | waafaqsan |
| Wareeg gaar ah [α]20/D | -84.5° ilaa -86.0° (Sample qalalan, C=4, H2O) | -85.51° |
| Xaaladda Xalka ( Gudbinta) | Cad iyo Midab la'aan ≥98.0% | 98.5% |
| Chloride (Cl) | ≤0.020% | <0.020% |
| Sulfate (SO4) | ≤0.020% | <0.020% |
| Ammonium (NH4) | ≤0.020% | <0.020% |
| Birta (Fe) | ≤10pm | <10pm |
| Biraha culus (Pb) | ≤10pm | <10pm |
| Arsenic (As2O3) | ≤1.0pm | <1.0pm |
| Amino Acids kale | Chromatographic ahaan lama ogaan karo | waafaqsan |
| Khasaare xagga qalajinta | ≤0.30% (105 ℃ ilaa 3 saacadood) | 0.16% |
| Hadhaaga dabka (Sulfated) | ≤0.10% | 0.07% |
| Qiimayn | 98.5 ilaa 101.0% (Titration, as Asal Qalalan) | 99.7% |
| Tijaabada pH | 5.9 ilaa 6.9 (1.0g ee 10ml ee H2O) | 6.2 |
| Walxaha Wanaagsan ee Ninhydrin | waafaqsan | waafaqsan |
| Asal ahaan | Ka Isha Aan Xayawaanka ahayn | waafaqsan |
| Xalalka Haraaga ah | waafaqsan | waafaqsan |
| Gabagabo | la kulmay AJI97;EP;USP;Tilmaamaha Tijaabada JP | |
| Isticmaalka Muhiimka ah | Amino Acids;Cuntada lagu daro;Daawooyinka;Kaabista Nafaqada | |
L-Proline (H-Pro-OH) (CAS: 147-85-3) AJI 97 Habka Imtixaanka
Aqoonsiga: Is barbar dhig nooca nuugista infrared-ka ee muunada iyo kan heerka caadiga ah ee habka saxanka bromide ee potassium.
Wareegga Gaarka ah [α] 20/D: Muunad qallalan, C=4, H2O
Xaaladda Xalka ( Gudbinta): 1.0g ee 10ml ee H2O, spectrophotometer, 430nm, 10mm dhumucda unugga.
Chloride (Cl): 0.7g, A-1, tixraac: 0.40ml ee 0.01mol/L HCl
Ammonium (NH4): B-1
Sulfate (SO4): 1.2g, (1), tixraac: 0.50ml ee 0.005mol/L H2SO4
Birta (Fe): 1.5g, tixraac: 1.5ml ee Iron Std.(0.01mg/ml)
Biraha culus (Pb): 2.0g, (1), tixraac: 2.0ml ee Pb Std.(0.01mg/ml)
Arsenic (As2O3): 2.0g, (1), tixraac: 2.0ml ee As2O3 Std.
Amino Acids kale: Tusaalaha Tijaabada: 30μg, B-6-a
Luminta qallajinta: at 105 ℃ 3 saacadood.
Qiimaynta: Muunad qallalan, 120mg, (1), 3ml of formic acid, 50ml of glacial acetic acid, 0.1mol/L HCLO4 1ml=11.513mg C5H9NO2
Tijaabada pH: 1.0g gudaha 10ml ee H2O
L-Proline (H-Pro-OH) (CAS: 147-85-3) Habka Imtixaanka USP35
Qeexitaan
Proline waxay ka kooban tahay NLT 98.5% iyo NMT 101.5% L-Proline (C5H9NO2), oo lagu xisaabiyo sal qallalan.
AQOONSIGA
A. NUUXDA INFRAREED <197K>
ASSAY
HABKA
Tusaale: 110 mg oo Proline ah
Madhan: Isku qas 3 ml oo ah aashitada formic iyo 50 ml oo ah glacial acetic acid.
Nidaamka Titrimetric
(Fiiri Titrimetry <541>)
Habka: Titration toos ah
Titrant: 0.1 N perchloric acid VS
Ogaanshaha barta dhamaadka: Potentiometric
Falanqaynta: Ku mil muunada 3 mL oo ah ashitada formic iyo 50ml ee glacial acetic acid.Titrate la Titrant.Samee go'aanka maran.
Xisaabi boqolkiiba Proline (C5H9NO2) ee muunada la qaaday:
Natiijadu = {[(VS-VB) x N x F]/W} x100
VS= mugga Titrant ee uu isticmaalo Tusaalaha (mL)
VB= mugga Titrant ee uu isticmaalo Bannaanka (mL)
N= Caadiga dhabta ah ee Titrant (mEq/ml)
F= Qodob u dhigma, 115.1 mg/mEq
W= Miisaanka Tusaalaha (mg)
Shuruudaha aqbalaadda: 98.5% ~ 101.5% ee salka qallalan
XANUUNKA
Hadhaaga dabka <281>: NMT 0.4%
Kloride iyo sulfate, Chloride <221>
Xalka caadiga ah: 0.50ml oo ah 0.020 N hydrochloric acid
Tusaalaha: 0.73g ee Proline
Shuruudaha aqbalaadda: NMT 0.05%
Kloride iyo sulfate, Sulfate <221>
Xalka caadiga ah: 0.10ml of 0.020 N sulfuric acid
Tusaalaha: 0.33g ee Proline
Shuruudaha aqbalaadda: NMT 0.03%
IRON <241>: NMT 30ppm
Biraha culus, Habka I <231>: NMT 15ppm
KALA XIRIIR
Xalka ku habboonaanta nidaamka: 0.4mg/mL midkiiba USP L-Proline RS iyo USP L-Threonine RS ee 0.1 N hydrochloric acid
Xalka caadiga ah: 0.05mg/mL ee USP L-Proline RS ee 0.1 N hydrochloric acid.[FIIRO GAAR AH-Xalkani waxa uu leeyahay fiirsi u dhigma 0.5% ee xalka Tusaalaha.]
Xalka muunada: 10mg/mL of Proline in 0.1 N hydrochloric acid
Nidaamka Chromatographic
(Fiiri Chromatography <621>, Chromatography-ka-dhuuban.)
Habka: TLC
Adsorbent: 0.25-mm lakabka silica jel chromatographic ah
Codsiga mugga: 5μL
Horumarinta habka dareeraha: khamriga Butyl, glacial acetic acid, iyo biyaha (3:1:1)
Daawada reagent: 2 mg/mL oo ninhydrin ah oo isku dhafka alkohol butyl ah iyo 2N acetic acid (95:5)
Ku habboonaanta nidaamka
Shuruudaha ku habboonaanta: chromatogram-ka xalka ku habboonaanta nidaamka wuxuu muujinayaa laba baro oo si cad u kala soocan.
Falanqaynta
Tusaalooyinka: Xalka ku habboonaanta nidaamka, xalalka caadiga ah, iyo xal muunad.
Ka dib markaad hawo-qaboojiso saxanka, ku buufi reagent buufin, oo kulayl inta u dhaxaysa 100 ° iyo 105 ° 15 min.Ku baadh saxanka hoostiisa iftiin cad.
Shuruudaha aqbalaadda: Meel kasta oo labaad ee xalka Tusaalaha kama weyna ama kama xoog badna meesha ugu muhiimsan ee xalinta caadiga ah.
Nijaasaha shaqsiga ah: NMT 0.5%
Wadarta wasakhda: NMT 2.0%
IMTIXAANO GAAR AH
Wareegga indhaha, wareeg gaar ah <781S>
Xalka muunada: 40 mg/mL oo biyo ah
Shuruudaha aqbalaadda: -84.3° ilaa -86.3°
LOSSON QALABKA <731>: Ku qalaji muunad 105 ℃ 3 saacadood: waxay luminaysaa NMT 0.4% miisaankeeda.
SHURUUD DHEERAAD AH
Baakadaha iyo Kaydinta: Ku kaydi weelasha si fiican u xidhan.
HEERARKA Tixraaca USP <11>
USP L-Proline RS
USP L-Threonine RS
Xidhmada: Dhalada fluorinated, 25kg/bac, 25kg/Cardboard Durbaan, ama si waafaqsan shuruudaha macmiilka.
Xaaladda Kaydinta:HygroscopicKu kaydi weelasha daboolan bakhaar qabow, engegan oo hawo leh oo ka fog walxaha aan ku habboonayn.Ka ilaali iftiinka iyo qoyaanka.Aan ku habboonayn walxaha oksaydhaynta ee xooggan.
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L-Proline (H-Pro-OH; La soo gaabiyey Pro ama P) (CAS: 147-85-3) waa amino acid dhexdhexaad ah.Inkasta oo proline loo kala saaro sida amino acid, waxay si adag u hadlaysaa imino acid, maadaama ay ka kooban tahay koox imino ah (carbon-nitrogen double bond).Silsiladdeeda dhinac ee pyrrolidine ee meertoga ah awgeed waxa loo kala saaray sidii amino acid aliphatic nonpolar.
Codsiga
Waxaa loo isticmaalaa cilmi-baarista biochemical, daawada nafaqo-xumada, yaraanta borotiinka, cudurrada caloosha iyo mindhicirka, gubasho iyo borotiinka ka dambeeya qaliinka.
1. Sida amino acid, waxay kabi kartaa nafaqooyinka waxayna u tahay walxo ceeriin oo faleebo amino acid ah.
2. Waxay wax ku ool u tahay dhiig-karka waxayna u tahay dhexdhexaadiye muhiim u ah isku-darka daawooyinka ka hortagga dhiig-karka ee safka hore sida captopril iyo enalapril.
3. Kaabista nafaqeynta, waxay hagaajin kartaa caabbinta unugyada waxayna kordhin kartaa heerka badbaadada ee callus.Dhadhannada qandhada sonkorta leh waxay dhacdaa falcelinta amino-carbonyl, waxay dhalin kartaa walxo dhadhan gaar ah.Shiinaha GB 2760-86 waxay bixisaa waxaa loo isticmaali karaa uunsi ahaan.
4. Waxay si wax ku ool ah u yareyn kartaa dhaawaca culeyska milixda ee qaabka mitochondrial ee dhirta bariiska dib loo soo celiyay.
5. L-Proline waa amino acid aan muhiim ahayn.Peptides waxay ku xidhan yihiin proline, taas oo ka dhigaysa dhisme faa'iido leh borotiinnada.Waxaa loo isticmaali karaa sida qayb ka mid ah warbaahinta dhaqanka unugga oo loogu talagalay soo saarista baayacmushtarka ee borotiinnada dib-u-daweynta iyo unugyada unugyada monoclonal.
6. L-Proline waxaa loo isticmaalaa sida kicinta asymmetric in synthesis organic iyo asymmetric aldol cyclization.Waa qayb firfircoon oo ka mid ah kolajka waxayna ku lug leedahay shaqada saxda ah ee kala-goysyada iyo seedaha.Waxay ka heshaa isticmaalka daawooyinka, codsiyada bayotechnoolajiyada sababtoo ah hantideeda osmoprotectant.
Shaqada:
1. L-Proline iyo soosaarayaasheeda waxaa inta badan loo isticmaalaa kicinta asymmetric ee falcelinta organic.Dhimista CBS iyo uumiga aldol ee proline katalysed ayaa ah tusaalayaal caan ah.
2. L-Proline waa osmoprotectant sidaas darteed waxaa loo isticmaalaa dawooyin badan, codsiyada biotechnological. Marka la sameeyo, borotiinada hodanka ku ah proline waxay isku daraan polyphenols si ay u soo saaraan caraf.
3. L-Proline waa mid ka mid ah asiidhyada amino ee muhiimka ah ee soo saara borotiinka aadanaha.Waxaa si weyn loogu isticmaalaa warshadaha cuntada iyo caafimaadka, waana dhexdhexaad muhiim u ah soo saarista ACE inhibitors sida Captopril iyo Enalapril.Sidoo kale waa mid ka mid ah walxaha muhiimka ah ee ku shubista amino acid.
4. L-Proline waxa loo isticmaalay caalam ahaan sida cuntada lagu daro, kicinta iyo alaabta ceeriin ee warshadaha kiimikada wanaagsan.
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