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Wararka

Habka Tijaabada (R)-(-)-3-Pyrrolidinol Hydrochloride CAS: 104706-47-0

Qalabka: Qalabka GC (Shimadzu GC-2010)

Tiirka: DB-17 Agilent 30mX0.53mmX1.0μm

Heerkulka foornada hore: 80 ℃

Waqtiga hore 2.0min

Qiyaasta 15 ℃/daq

Heerkulka foornada kama dambaysta ah: 250 ℃

Waqtiga ugu dambeeya 20min

Gaasta Nitrojiinka sidaha

Habka socodka joogtada ah

Socodka 5.0ml/min

Saamiga kala baxa 10:1

Heerkulka duritaanka: 250 ℃

Heerkulka qalabka: 300 ℃

Mugga cirbadeynta 1.0μL

Taxaddar in la sameeyo falanqaynta ka hor:

1. Tiirka xaalada 240 ℃ ugu yaraan 30 daqiiqo.

2. Ku dhaq saliingaha oo si fiican u nadiifi xuubka cirbadeynta si aad uga saarto wasakhda falanqaynta hore.

3. Ku dhaq, engeji oo ka buuxi milix weel lagu dhaqo saliingaha.

 

Diyaarinta qaska:

Ku diyaari 2% w/v xal sodium hydroxide biyaha.

Diyaarinta caadiga ah:

Ku miisaam qiyaastii 100mg of (R) -3-hydroxyprolidine hydrochloride heerka fijaan, ku dar 1mL oo qasin ah oo milmi.

Diyaarinta tijaabada:

Ku miisaam qiyaastii 100mg oo muunad tijaabo ah dhalo, ku dar 1mL oo dareere ah oo milmi.Ku diyaari nuqul

Habka:

Ku duri maran (diluent), diyaarinta caadiga ah iyo diyaarinta tijaabada adoo isticmaalaya xaaladaha ka sarreeya GC.Iska daa meelaha ugu sarreeya madhan awgeed.Waqtiga haynta ee ugu sarreysa sababtoo ah (R) -3-hydroxyprolidine waa qiyaastii 5.0min.

Fiiro gaar ah:

U soo sheeg natiijada celcelis ahaan


Waqtiga boostada: Nov-13-2021