Qalabka: Qalabka GC (Shimadzu GC-2010)
Tiirka: DB-17 Agilent 30mX0.53mmX1.0μm
Heerkulka foornada hore: 80 ℃
Waqtiga hore 2.0min
Qiyaasta 15 ℃/daq
Heerkulka foornada kama dambaysta ah: 250 ℃
Waqtiga ugu dambeeya 20min
Gaasta Nitrojiinka sidaha
Habka socodka joogtada ah
Socodka 5.0ml/min
Saamiga kala baxa 10:1
Heerkulka duritaanka: 250 ℃
Heerkulka qalabka: 300 ℃
Mugga cirbadeynta 1.0μL
Taxaddar in la sameeyo falanqaynta ka hor:
1. Tiirka xaalada 240 ℃ ugu yaraan 30 daqiiqo.
2. Ku dhaq saliingaha oo si fiican u nadiifi xuubka cirbadeynta si aad uga saarto wasakhda falanqaynta hore.
3. Ku dhaq, engeji oo ka buuxi milix weel lagu dhaqo saliingaha.
Diyaarinta qaska:
Ku diyaari 2% w/v xal sodium hydroxide biyaha.
Diyaarinta caadiga ah:
Ku miisaam qiyaastii 100mg of (R) -3-hydroxyprolidine hydrochloride heerka fijaan, ku dar 1mL oo qasin ah oo milmi.
Diyaarinta tijaabada:
Ku miisaam qiyaastii 100mg oo muunad tijaabo ah dhalo, ku dar 1mL oo dareere ah oo milmi.Ku diyaari nuqul
Habka:
Ku duri maran (diluent), diyaarinta caadiga ah iyo diyaarinta tijaabada adoo isticmaalaya xaaladaha ka sarreeya GC.Iska daa meelaha ugu sarreeya madhan awgeed.Waqtiga haynta ee ugu sarreysa sababtoo ah (R) -3-hydroxyprolidine waa qiyaastii 5.0min.
Fiiro gaar ah:
U soo sheeg natiijada celcelis ahaan
Waqtiga boostada: Nov-13-2021