1-Methyl-3-Pyrrolidinol CAS 13220-33-2 Purity > 98.0% (GC) Setšoantšo se Featured

1-Methyl-3-Pyrrolidinol CAS 13220-33-2 Bohloeki >98.0% (GC)

Tlhaloso e Khutšoanyane:

Lebitso la lik'hemik'hale: 1-Methyl-3-Pyrrolidinol

Synonyms: 3-Hydroxy-1-Methylpyrrolidine

CAS: 13220-33-2

Bohloeki: >98.0% (GC)

Ponahalo: Mokelikeli o Bosehla o Khanyang

Ikopanye le: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

Re romelle lengolo-tsoibila

Lintlha tsa Sehlahisoa

Lihlahisoa tse Amanang

Li-tag tsa Sehlahisoa

Tlhaloso:

Ruifu Chemical ke moetsi ea ka sehloohong oa 1-Methyl-3-Pyrrolidinol (3-Hydroxy-1-Methylpyrrolidine) (CAS: 13220-33-2) e nang le boleng bo phahameng.Ruifu Chemical e ka fana ka lits'ebeletso tsa lefats'e ka bophara, theko ea tlholisano, litšebeletso tse ntle haholo, tse nyane le tse ngata tse fumanehang.Reka 1-Methyl-3-Pyrrolidinol,Please contact: alvin@ruifuchem.com

Lintho tsa Lik'hemik'hale:

Lebitso la Lik'hemik'hale	1-Methyl-3-Pyrrolidinol
Litlhaloso tse tšoanang	N-Methyl-3-Pyrrolidinol;3-Hydroxy-1-Methylpyrrolidine;N-Methyl-Pyrrolidin-3-ol;N-Methyl-Pyrrolidinyl Alcohol;1-Methylpyrrolidin-3-ol
Boemo ba Setoko	Ka Stock, Tlhahiso ea Khoebo
Nomoro ea CAS	13220-33-2
Foromo ea limolek'hule	C5H11NO
Boima ba Molek'hule	101.15 g/mol
Ntlha e belang	75℃/12 mmHg
Flash point	71℃
Botenya	0.921 g/mL ho 25℃ (lit.)
Refractive Index n20/D	1.464(lit.)
E hloahloa	Ha e na Moeeng, ea Hygroscopic
Solubility	E qhibiliha ka Metsing, E qhibiliha ka Joala, Ether le Benzene
COA & MSDS	E fumaneha
Mohlala	E fumaneha
Tšimoloho	Shanghai, China
Brand	Ruifu Chemical

Litlhaloso:

Lintho	Maemo a Tlhahlobo	Liphetho
Ponahalo	Mokelikeli o Mosehla o Khanyang	Mokelikeli o Mosehla o Khanyang
Metsi ka Karl Fischer	<0.20%	0.15%
Mokhoa oa Bohloeki / Analysis	>98.0% (GC)	98.57%
Boima ba 'mele (20 ℃)	0.920~0.923	E lumellana
Refractive Index n20/D	1.463~1.465	E lumellana
Infrared Spectrum	E tsamaellanang le Sebopeho	E lumellana
1H NMR Spectrum	E tsamaellanang le Sebopeho	E lumellana
Qetello	Sehlahisoa se lekoa 'me se lumellana le litlhaloso tse fanoeng

Sephutheloana/Bobolokelo/Ho tsamaisa ka sekepe:

Sephutheloana:Botlolo, Aluminium foil bag, 25kg/Cardboard Drum, kapa ho ea ka tlhokahalo ea moreki.

Boemo ba polokelo:Boloka setshelo se kwetswe ka thata mme o se boloke sebakeng se phodileng, se omeletseng (2~8℃) le se nang le moya o hlwekileng hole le dintho tse sa dumellaneng.Sireletsa leseli le mongobo.
Ho tsamaisa ka sekepe:Tsamaisa lefatšeng ka bophara ka sefofane, ka FedEx / DHL Express.Fana ka thomello e potlakileng le e tšepahalang.

13220-33-2 - Tsela ea Synthetic:

13220-33-2 - Mokhoa oa ho itokisa:

Kenya 1,2,4-Butanetriol le glacial acetic acid pitseng ea karabelo, hlohlelletsa le mocheso hoo e ka bang 100 ℃, eketsa khase e omileng ea hydrogen chloride, 'me u arabe ka 90 ~ 110 ℃ bakeng sa 30h, ha palo e kholo ea hydrogen chloride e qala ho ho hlaha ka khase ea mohatla, ntlha ea ho qetela ea karabelo e ile ea hlahlojoa 'me hydrogen chloride ea emisoa.Kamora ho pholile, thepa e ile ea ntšoa, ea hlatsuoa ka tharollo ea sodium carbonate e tletseng, 'me ea kenngoa ka tlas'a khatello e fokotsehileng, le 120 ho 135 ℃.(12.6 ho 13. 3kPa) karoloana, ke hore, 1,4-Dichloro-2-Butanol oli ea taba, e fana ka 50% ~ 60%.
Cyclization tharollo ea metsi ea 1,4-Dichloro-2-Butanol le Methylamine e ile ea kenngoa pitseng ea cyclization, 'me ea futhumatsoa ho 120 ℃.Tlas'a ho futhumatsa ho koetsoeng, 'me karabelo e ile ea tsosoa bakeng sa 10h.Ka mor'a ho pholile, ho ne ho eketsoa sodium hydroxide e tiileng, 'me letsoai la inorganic le neng le le metsi le ne le sefuoa.Lera la oli le ile la aroloa 'me la kenngoa ka har'a vacuum distillation, le karolo ea 76-85 ℃.(2.1 kPa) e ile ea bokelloa hore e be sehlahisoa se felileng.Ho ntšoa ha lera la metsi le benzene ho boetse ho fana ka karolo ea 1-Methyl-3-Pyrrolidinol.Kotulo e ne e ka ba 60%.
3. Mekhoa ea bohlokoa:
3.1 Ts'ebetso ea karabelo e fetotsoeng: laola nako ea karabelo 'me u bone pheletso ea karabelo
3.2 Vacuum distillation process ea 1,4-Dichloro-2-Butanol: laola vacuum degree ea vacuum distillation le mocheso oa karoloana.
3.3 Ts'ebetso ea cyclization: laola mocheso oa karabelo le nako
3.4 1-Methyl-3-Pyrrolidinol vacuum distillation process: laola vacuum degree ea vacuum distillation le karoloana ea mocheso
4. Lintlha tsa taolo ea boleng:
Ntlha ea 1 ea taolo ea boleng: 1,2,4-Butanetriol maemo a boleng ba thepa e tala
Ntlha ea 2 ea taolo ea boleng: Tekanyetso ea boleng bo bohareng bakeng sa karabelo ea cyclization
Ntlha ea 3 ea taolo ea boleng: 1,4-Dichloro-2-Butanol maemo a mahareng a boleng
Ntlha ea 4 ea taolo ea boleng: 1-Methyl-3-Pyrrolidinol e felile boleng ba boleng ba sehlahisoa

13220-33-2 - Mokhoa oa Teko:

Mongobo: Nka sehlahisoa sena 'me u se hlahlobe ho latela mokhoa oa ho lekanya mongobo (Mokhoa oa Pele oa A oa Sehlomathiso Ⅷ M, Khatiso ea 2010 ea People's Republic of China Pharmacopoeia).Mongobo ha oa lokela ho feta 0.2%.
Relative Density: Tekanyo e lekanyelitsoeng ea sehlahisoa sena (Sehlomathiso VI A sa Karolo ea II, khatiso ea 2010) ke 0.920~0.923
Refractive Index: Lenane la refractive la sehlahisoa sena (Sehlomathiso VI F sa Karolo ea II ea khatiso ea 2010) ke 1.463 ~ 1.465
Boikemisetso ba Litaba: Likahare tsa 1-Methyl-3-Pyrrolidinol ha lia lokela ho ba ka tlase ho 98.0% ka chromatography ea khase (Sehlomathiso Ⅴ E, Karolo ea II, khatiso ea 2010).
Kholomo: Capillary ka silika e qhibilihisitsoeng SPB-5, bophara ba ka hare 0.32mm, bolelele ba 30m
T Ente: 300 ℃
FID: 320 ℃
T Column: 80 ℃ bakeng sa metsotso ea 5, ho 200 ℃ ho 5 ℃ / min, ebe ho 200 ℃ bakeng sa 7 min.
Sesebelisoa: Helium ho 1 ml / min
Karo-karolelano ea ho arohana: 100: 1
Ente: 1 microliter
Tharollo ea teko: qhala 200mg ea sampuli tlas'a tlhahlobo ho 10ml ea methanol.Enta 1 microliter.1μl e ile ea kenngoa ka har'a chromatograph ea khase ho hatisa chromatogram.Litaba tsa 1-Methyl-3-Pyrrolidinol li ne li baloa ka mokhoa oa ho tloaeleha sebakeng se phahameng.

Melemo:

Bokhoni bo lekaneng: Lisebelisoa le litsebi tse lekaneng

Tšebeletso ea profeshenale: Tšebeletso e le 'ngoe ea ho reka

Sephutheloana sa OEM: Sephutheloana sa tloaelo le leibole lia fumaneha

Tlhahiso e potlakileng: Haeba e le ka har'a setoko, ho netefalitsoe hore ho tsamaisoa matsatsi a mararo

Thepa e tsitsitseng: Boloka thepa e lekaneng

Tšehetso ea Theknoloji: Tharollo ea theknoloji e teng

Tšebeletso e Tloaelehileng ea ho Kopanya: Ho tloha ho ligrama ho isa ho lik'hilograma

Boleng bo Phahameng: Ho thehile tsamaiso e felletseng ea netefatso ea boleng

LBH:

Mokhoa oa ho Reka?Ka kopo ikopanyeDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

Phihlelo ea Lilemo Tse 15?Re na le boiphihlelo ba lilemo tse fetang 15 ho etsa le ho romella kantle ho naha mefuta e mengata e fapaneng ea li-intermediate tsa boleng bo holimo tsa meriana kapa lik'hemik'hale tse ntle.

Limmaraka tse ka Sehloohong?Rekisetsa 'maraka oa lapeng, Amerika Leboea, Europe, India, Korea, Japane, Australia, joalo-joalo.

Melemo?Boleng bo phahameng, theko e theko e tlaase, lits'ebeletso tsa litsebi le ts'ehetso ea tekheniki, phano e potlakileng.

BolengTiisetso?Tsamaiso e thata ea taolo ea boleng.Lisebelisoa tsa profeshenale bakeng sa tlhahlobo li kenyelletsa NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, joalo-joalo.

Mehlala?Lihlahisoa tse ngata li fana ka mehlala ea mahala bakeng sa tlhahlobo ea boleng, litšenyehelo tsa ho tsamaisa thepa li lokela ho lefshoa ke bareki.

Feme Audit?Ho amoheloa ha fektheri.Ke kopa o etse kopano esale pele.

MOQ?Ha ho MOQ.Taelo e nyenyane e amoheleha.

Nako ea thomello? Haeba ka har'a setoko, ho netefalitsoe hore ho tsamaisoa ka matsatsi a mararo.

Lipalangoang?Ka Express (FedEx, DHL), ka Moea, ka Leoatle.

Litokomane?Ka mor'a tšebeletso ea thekiso: COA, MOA, ROS, MSDS, joalo-joalo e ka fanoa.

Custom Synthesis?E ka fana ka lits'ebeletso tsa tloaelo tsa ho kopanya ho lekana hantle litlhoko tsa hau tsa lipatlisiso.

Litefiso Melao?Invoice ea Proforma e tla romelloa pele kamora netefatso ea odara, e kenyellelitseng tlhahisoleseling ea rona ea banka.Tefo ka T/T (Telex Transfer), PayPal, Western Union, joalo-joalo.

13220-33-2 - Kotsi le Tšireletseho:

Matshwao a Kotsi Xi - E tenang
Likhoutu tsa Kotsi
36/37/38 - Ho halefisa mahlo, tsamaiso ea ho hema le letlalo.
Tlhaloso ea Tšireletseho
S26 - Ha u kopana le mahlo, hlatsoa hang-hang ka metsi a mangata 'me u batle keletso ea bongaka.
S36/37/39 - Apara liaparo tse loketseng tse sireletsang, liatlana le tšireletso ea mahlo / sefahleho.
WGK Jeremane 3
HS Code 2933990099

13220-33-2 - Kopo:

1-Methyl-3-Pyrrolidinol (3-Hydroxy-1-Methylpyrrolidine) (CAS: 13220-33-2) e sebelisoa e le motsoako oa organic synthesis bohareng, o sebelisoang e le setsi sa meriana lefapheng la meriana.