(Boc)2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity >99.0% (HPLC) Factory Protecting Reagent

Tlhaloso e Khutšoanyane:

Lebitso la lik'hemik'hale: Di-tert-Butyl Iminodicarboxylate

Mantsoe a tšoanang: (Boc)2NH;N-Boc-tert-Butylcarbamate

CAS: 51779-32-9

Bohloeki: >99.0% (HPLC)

Ponahalo: Phofo e tšoeu ea Crystalline

Ho sireletsa li-reagents, boleng bo holimo

Ikopanye le: Dr. Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

Re romelle lengolo-tsoibila

Lintlha tsa Sehlahisoa

Lihlahisoa tse Amanang

Li-tag tsa Sehlahisoa

Tlhaloso:

Shanghai Ruifu Chemical Co., Ltd. ke moetsi ea ka sehloohong oa Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9) e nang le boleng bo phahameng.Ruifu Chemical e fana ka letoto la li-reagents tse sireletsang le li-reagents tse kopanyang.Re ka fana ka litšebeletso tsa lefats'e ka bophara, theko ea tlhōlisano, palo e nyenyane le e ngata e fumanehang.Reka Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com

Lintho tsa Lik'hemik'hale:

Lebitso la Lik'hemik'hale	Di-tert-Butyl Iminodicarboxylate
Litlhaloso tse tšoanang	(Boc)2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic Acid Di-tert-Butyl Ester;Bis(tert-Butoxycarbonyl)ammonia
Boemo ba Setoko	E teng thepeng e teng ka lebenkeleng
Nomoro ea CAS	51779-32-9
Foromo ea limolek'hule	C10H19NO4
Boima ba Molek'hule	217.27 g/mol
Melting Point	114.0 ~ 120.0℃
Botenya	1.037±0.06 g/cm3
E hloahloa	Ha e Mamele Moeeng, Ha e Mamele Khanya
Ho qhibiliha ha Metsi	Ha e qhibilihe ka Metsing
Solubility	Chloroform, Methanol
Mocheso oa polokelo.	Sebaka se pholileng le se omileng (2~8℃)
COA & MSDS	E fumaneha
Sehlopha	Ho sireletsa li-reagents
Brand	Ruifu Chemical

Litlhaloso:

Lintho	Maemo a Tlhahlobo	Liphetho
Ponahalo	Phofo e Tšoeu ea Crystalline	E lumellana
Melting Point	114.0 ~ 120.0℃	118.8 ~ 119.3 ℃
Tahlehelo ka ho Omisa	<0.50%	0.10%
Mokhoa oa Bohloeki / Analysis	>99.0% (HPLC)	99.6%
Infrared Spectrum	E Ikamahanya le Sebopeho	E lumellana
Sekhahla sa NMR	E Ikamahanya le Sebopeho	E lumellana
Qetello	Sehlahisoa se lekoa 'me se lumellana le litlhaloso tse fanoeng

Teko ea Bohloeki:

Kholomo ea Chromatographic: SE-54 30m×0.25mm×0.5μm;
Mofuputsi: FID
Mocheso oa pele: 100 ℃
Nako ea pele: 1min
Sekhahla sa mocheso: 20 ℃/min
Mocheso oa ho qetela: 190 ℃
Qetellong: 10min
Mocheso oa ente: 160 ℃
Mocheso oa detector: 200 ℃
Karolelano ea ho arohana: 50: 1;
Boholo ba mohlala: 0,2μl;
Mokelikeli: methanol
Sephetho: Bohloeki bo ne bo le boholo ho feta 99.0% ka mokhoa o tloaelehileng oa sebaka.

Sephutheloana/Bobolokelo/Ho tsamaisa ka sekepe:

Sephutheloana:Botlolo, Aluminium foil bag, 25kg/Cardboard Drum, kapa ho ea ka tlhokahalo ea moreki.
Boemo ba polokelo:Boloka ka lijaneng tse tiisitsoeng sebakeng sa polokelo se pholileng le se omileng (2~8℃) hole le lintho tse sa lumellaneng.Sireletsa leseli le mongobo.
Ho tsamaisa ka sekepe:Fana ka lefatše ka FedEx / DHL Express.Fana ka thomello e potlakileng le e tšepahalang.

Melemo:

Bokhoni bo lekaneng: Lisebelisoa le litsebi tse lekaneng

Tšebeletso ea profeshenale: Tšebeletso e le 'ngoe ea ho reka

Sephutheloana sa OEM: Sephutheloana sa tloaelo le leibole lia fumaneha

Tlhahiso e potlakileng: Haeba e le ka har'a setoko, ho netefalitsoe hore ho tsamaisoa matsatsi a mararo

Thepa e tsitsitseng: Boloka thepa e lekaneng

Tšehetso ea Theknoloji: Tharollo ea theknoloji e teng

Tšebeletso e Tloaelehileng ea ho Kopanya: Ho tloha ho ligrama ho isa ho lik'hilograma

Boleng bo Phahameng: Ho thehile tsamaiso e felletseng ea netefatso ea boleng

LBH:

Mokhoa oa ho Reka?Ka kopo ikopanyeDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

Phihlelo ea Lilemo Tse 15?Re na le boiphihlelo ba lilemo tse fetang 15 ho etsa le ho romella kantle ho naha mefuta e mengata e fapaneng ea li-intermediate tsa boleng bo holimo tsa meriana kapa lik'hemik'hale tse ntle.

Limmaraka tse ka Sehloohong?Rekisetsa 'maraka oa lapeng, Amerika Leboea, Europe, India, Korea, Japane, Australia, joalo-joalo.

Melemo?Boleng bo phahameng, theko e theko e tlaase, lits'ebeletso tsa litsebi le ts'ehetso ea tekheniki, phano e potlakileng.

BolengTiisetso?Tsamaiso e thata ea taolo ea boleng.Lisebelisoa tsa profeshenale bakeng sa tlhahlobo li kenyelletsa NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, joalo-joalo.

Mehlala?Lihlahisoa tse ngata li fana ka mehlala ea mahala bakeng sa tlhahlobo ea boleng, litšenyehelo tsa ho tsamaisa thepa li lokela ho lefshoa ke bareki.

Feme Audit?Ho amoheloa ha fektheri.Ke kopa o etse kopano esale pele.

MOQ?Ha ho MOQ.Taelo e nyenyane e amoheleha.

Nako ea thomello? Haeba ka har'a setoko, ho netefalitsoe hore ho tsamaisoa ka matsatsi a mararo.

Lipalangoang?Ka Express (FedEx, DHL), ka Moea, ka Leoatle.

Litokomane?Ka mor'a tšebeletso ea thekiso: COA, MOA, ROS, MSDS, joalo-joalo e ka fanoa.

Custom Synthesis?E ka fana ka lits'ebeletso tsa tloaelo tsa ho kopanya ho lekana hantle litlhoko tsa hau tsa lipatlisiso.

Litefiso Melao?Invoice ea Proforma e tla romelloa pele kamora netefatso ea odara, e kenyellelitseng tlhahisoleseling ea rona ea banka.Tefo ka T/T (Telex Transfer), PayPal, Western Union, joalo-joalo.

51779-32-9 - Kotsi le Tšireletseho:

Matshwao a Kotsi Xi - E tenang
Likhoutu tsa Kotsi 36/37/38 - Ho hlohlona mahlong, tsamaiso ea ho hema le letlalo.
Tlhaloso ea Tšireletseho S26 - Ha u kopana le mahlo, hlatsoa hang-hang ka metsi a mangata 'me u batle keletso ea bongaka.
S37/39 - Apara liatlana tse loketseng le tšireletso ea mahlo / sefahleho
WGK Jeremane 3
HS Code 29241990
Hazard Note Irritant

Kopo:

Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Kopo ea Di-tert-Butyl Iminodicarboxylate ke setsi sa meriana, se ka lokisoang ka bohato bo le bong ba formamide le Boc2O.
Motsoako ona o sebelisoa e le reagent bakeng sa ho lokisa li-amine tsa mantlha tse tsoang ho alkyl halides.E ile ea tuma e le mokhoa o mong ho fapana le motsoako oa Gabriel bakeng sa phetoho e tšoanang.Li-amine li ka boela tsa lokisoa ho tsoa ho lino tse tahang ka ho felloa ke metsi 'meleng ho sebelisa karabelo ea Mitsunobu.Ts'ebetsong e tloaelehileng, reagent e senyeha ho fana ka letsoai la potasiamo, e leng N-alkylated.Lihlopha tse sireletsang tsa Boc hamorao li tlosoa tlas'a maemo a acidic.
Di-tert-Butyl Iminodicarboxylate ke sehlopha se sirelelitsoeng sa amine se sebelisetsoang ho lokisa li-spirocycle tse thibetsoeng e le bahanyetsi ba CCR1.
Ho lokisetsa tharollo ea DMAP (0.61g, 5.0mmol) ho MeCN (15ml) butle-butle e kenyelletsoa tharollo ea formamide (2.5g,56mmol) le Boc2O (24).g, 110mol) ho MeCN (15ml).Ka mor'a ho susumetsa mocheso oa kamore bakeng sa 4h, tharollo e mosehla e ne e pholile ho 0 ° C, 'me N,N-diethylenediamine (6.97g, 60mmol) e ile ea eketsoa butle-butle ho 0 ℃.Motsoako o hlahisoang o ile oa tsosoa mocheso oa kamore bakeng sa 12h mme o tlhotliloeng ka silika e tšesaane;motsoako o hlahisoang o ne o tlhotliloeng ka mocheso oa kamore.Joale solvent e fetoha mouoane tlas'a khatello e fokotsehileng.Sehlahisoa se sa tsoakoang se ile sa hloekisoa ka silica gel chromatography mme sa hlakisoa ka EtOAc/hexane (1:5) ho fumana sehlahisoa sa sehlooho, se tiileng se tšoeu (10.99g, 92%).