HBTU CAS 94790-37-1 Peptide Coupling Reagent Purity >99.0% (HPLC) Feme
Shanghai Ruifu Chemical Co., Ltd. ke moetsi ea ka sehloohong oa HBTU (CAS: 94790-37-1) e nang le boleng bo phahameng.Ruifu Chemical e fana ka letoto la li-reagents tse sireletsang le li-reagents tse kopanyang.Ruifu e ka fana ka lits'ebeletso tsa lefats'e ka bophara, theko ea tlholisano, palo e nyane le e ngata e fumanehang.Reka HBTU,Please contact: alvin@ruifuchem.com
Lebitso la Lik'hemik'hale | HBTU |
Litlhaloso tse tšoanang | 1- [Bis (dimethylamino) methylene] -1H-benzotriazolium 3-Oxide Hexafluorophosphate;N,N,N′,N′-Tetramethyl-O-(1H-Benzotriazol-1-yl)uronium Hexafluorophosphate;O-Benzotriazole-N, N, N', N'-Tetramethyluronium-Hexafluorophosphate;O-(1H-Benzotriazol-1-yl) -N,N,N',N'-Tetramethyluronium Hexafluorophosphate;2-(1H-Benzotriazole-1-yl) -1,1,3,3-Tetramethyluronium Hexafluorophosphate |
Boemo ba Setoko | Ho Stock, Commercial Scale |
Nomoro ea CAS | 94790-37-1 |
Foromo ea limolek'hule | Setšoantšo sa C11H16F6N5OP |
Boima ba Molek'hule | 379.25 g/mol |
Melting Point | ≥200 ℃ |
Botenya | 1.5095 |
E hloahloa | E na le Kutloelo-bohloko ho Khanya, Ha e na Mongobo |
Ho qhibiliha ha Metsi | Ha e Monyehe ka Metsing |
Solubility | E qhibiliha ka Acetonitrile.E qhibiliha hanyenyane ka Acetone, Ethanol |
Mocheso oa polokelo. | Sebaka se pholileng le se omileng (2~8℃) |
COA & MSDS | E fumaneha |
Sehlopha | Coupling Reagents |
Brand | Ruifu Chemical |
Lintho | Maemo a Tlhahlobo | Liphetho |
Ponahalo | Phofo e Tšoeu ea Crystalline | E lumellana |
Melting Point | ≥200 ℃ | 205.6 ℃ |
Tahlehelo ka ho Omisa | <0.50% | 0.11% |
Mokhoa oa Bohloeki / Analysis | >99.0% (HPLC) | 99.9% |
Infrared Spectrum | E Ikamahanya le Sebopeho | E lumellana |
NMR Spectrum 1H | E Ikamahanya le Sebopeho | E lumellana |
Fluorine NMR Spectrum | E Ikamahanya le Sebopeho | E lumellana |
Teko ea Solubility ho Acetonitrile | 1g ho 10ml Acetonitrile Hlakile Tharollo | Feta |
Qetello | Sehlahisoa se lekoa 'me se lumellana le litlhaloso |
Sephutheloana:Botlolo, Aluminium foil bag, 25kg/Cardboard Drum, kapa ho ea ka tlhokahalo ea moreki.
Boemo ba polokelo:Boloka ka lijaneng tse tiisitsoeng sebakeng sa polokelo se pholileng le se omileng (2~8℃) hole le lintho tse sa lumellaneng.Sireletsa leseli le mongobo.
Ho tsamaisa ka sekepe:Fana ka lefatše ka FedEx / DHL Express.Fana ka thomello e potlakileng le e tšepahalang.
1. Thepa: Sehlahisoa sena e lokela ho ba phofo e tšoeu ea kristale.
2. Boikemisetso ba litaba: ho latela ts'ebetso e phahameng ea mokelikeli chromatography (Chinese Pharmacopoeia 2010 edition Appendix VI D) boikemisetso.
Maemo a Chromatographic: The octadecylsilane bonded silica gel e ne e sebelisoa e le ho tlatsa, (250 * 4.6mm * 5.0μm);Acetonitrile: metsi = 15: 85 (pH e fetotsoe ke acetic acid = 2.5) e le mohato oa selefouno;Nako ea ho lemoha e ne e le 258nm.Sekhahla sa phallo: 0.5ml / min;Palo ea lipoleiti tsa theory ho latela HBTU
Tlhōrō e kholo e lokela ho baloa eseng ka tlase ho 2000.
Mokhoa oa ho etsa qeto: Nka tekanyo e nepahetseng ea sehlahisoa sena, etsa tharollo ea mohato oa mohala o nang le HBTU 20μg ka 1ml, e le tharollo ea teko.10 μL ea tharollo ea teko e ile ea kenngoa ka har'a chromatograph 'me habeli nako ea ho boloka karolo ea mantlha e ile ea tlalehoa.
Liphello: Ho ea ka mokhoa oa tloaelo oa sebaka, litaba tsa HBTU ha lia lokela ho ba ka tlase ho 99.0%.
3. Sebaka sa ho qhibiliha: ho ea ka mokhoa oa ho etsa qeto ea ho qhibiliha (Sehlomathiso VIIC sa khatiso ea Chinese Pharmacopoeia 2010), tekanyo ea ho futhumatsa ke 3 ℃ / min.
Sebaka se qhibilihang sa sehlahisoa sena ha se ka tlase ho 200.0 ℃.
4. Ho lahleheloa ke ho omisa: nka sehlahisoa sena ho 80 ℃ 'me u omelle tlas'a khatello e fokotsehileng bakeng sa lihora tsa 4 ho boima bo sa feleng,' me tahlehelo ea boima ha ea lokela ho feta 0.50%.
5. Ho hlaka ha tharollo: nka 1g ea sehlahisoa sena, eketsa 10ml ea acetonitrile, sisinya hantle, tharollo e lokela ho ba e hlakileng le e hlakileng.
6. Polokelo: Boloka sebakeng se lefifi le se phodileng se omileng (2~8℃).
7. Nako ea ho hlahloba: selemo se le seng.
Mokhoa oa ho Reka?Ka kopo ikopanyeDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Phihlelo ea Lilemo Tse 15?Re na le boiphihlelo ba lilemo tse fetang 15 ho etsa le ho romella kantle ho naha mefuta e mengata e fapaneng ea li-intermediate tsa boleng bo holimo tsa meriana kapa lik'hemik'hale tse ntle.
Limmaraka tse ka Sehloohong?Rekisetsa 'maraka oa lapeng, Amerika Leboea, Europe, India, Korea, Japane, Australia, joalo-joalo.
Melemo?Boleng bo phahameng, theko e theko e tlaase, lits'ebeletso tsa litsebi le ts'ehetso ea tekheniki, phano e potlakileng.
BolengTiisetso?Tsamaiso e thata ea taolo ea boleng.Lisebelisoa tsa profeshenale bakeng sa tlhahlobo li kenyelletsa NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, joalo-joalo.
Mehlala?Lihlahisoa tse ngata li fana ka mehlala ea mahala bakeng sa tlhahlobo ea boleng, litšenyehelo tsa ho tsamaisa thepa li lokela ho lefshoa ke bareki.
Feme Audit?Ho amoheloa ha fektheri.Ke kopa o etse kopano esale pele.
MOQ?Ha ho MOQ.Taelo e nyenyane e amoheleha.
Nako ea thomello? Haeba ka har'a setoko, ho netefalitsoe hore ho tsamaisoa ka matsatsi a mararo.
Lipalangoang?Ka Express (FedEx, DHL), ka Moea, ka Leoatle.
Litokomane?Ka mor'a tšebeletso ea thekiso: COA, MOA, ROS, MSDS, joalo-joalo e ka fanoa.
Custom Synthesis?E ka fana ka lits'ebeletso tsa tloaelo tsa ho kopanya ho lekana hantle litlhoko tsa hau tsa lipatlisiso.
Litefiso Melao?Invoice ea Proforma e tla romelloa pele kamora netefatso ea odara, e kenyellelitseng tlhahisoleseling ea rona ea banka.Tefo ka T/T (Telex Transfer), PayPal, Western Union, joalo-joalo.
Likhoutu tsa Kotsi
R36/37/38 - Ho hlohlona mahlong, tsamaiso ya moya le letlalo.
R20/21/22 - E kotsi ka ho hema, ho kopana le letlalo le haeba e koetsoe.
R42/43 - E ka baka maikutlo ka ho hema le ho ama letlalo.
Tlhaloso ea Tšireletseho
S26 - Ha u kopana le mahlo, hlatsoa hang-hang ka metsi a mangata 'me u batle keletso ea bongaka.
S36/37/39 - Apara liaparo tse loketseng tse sireletsang, liatlana le tšireletso ea mahlo / sefahleho.
S36 - Apara liaparo tse loketseng tsa tšireletso.
S22 - U se ke ua hema lerole.
WGK Jeremane 3
FLUKA BRAND F CODES 8-10-21
HS Code 2933990099
Hazard Note Irritant
Chefo LD50 ka molomo ho Mmutla: > 2000 mg/kg
HBTU (CAS: 94790-37-1) ke reagent ea ho kopanya e sebelisoang ka peptide synthesis.HBTU e bonts'itsoe hore e hatella racemization ka katleho.
HBTU ke coupling reagent e atisang ho sebelisoa ho solid phase peptide synthesis.HBTU e boetse e sebelisitsoe ho protocol e tloaelehileng ea Fmoc-based solid-phase peptide synthesis (SPPS).
HBTU, ka mor'a hore e hlahisoe ka 1978, moemeli oa HBTU o bontša botumo ba k'hemistri le tšebeliso ea indasteri ka lebaka la thepa ea eona e bonolo ea ho sebetsa.ho feta moo, e boetse e bontša ho hanyetsa khahlanong le racemization.tšekamelo e tlase ea racemization ke tlhokahalo ea mantlha bakeng sa peptide synthesis.haholo-holo bakeng sa motsoako o tiileng oa karolo ea peptide, chai e ngata e nang le nako e khuts'oane ea karabelo e bohlokoa ho etsa hore motsoako oa li-peptide tse kholo o khonehe.
Liphuputso tsa morao-rao li bontša hore kristale hammoho le sebopeho sa tharollo ea moemeli ona oa ho kopanya ke guanidinium N-oxide eseng motsoako oa uronium;Coupling reagent bakeng sa peptide synthesis;melemo ke: lebelo le tlase haholo, maemo a bonolo a karabelo, nako e khuts'oane haholo ea karabelo, le chai e ngata.
Peptide synthesis e ne e itšetlehile haholo ka li-reagents tse sebetsang hantle le tse sireletsehileng.HBTU e ile ea pakoa hore e fetola li-carboxylic acid hore e be azides ka katleho le ka mokhoa o sebetsang.ts'ebetso ena e ka sebelisoa ho mefuta e mengata ea li-carboxylic acid ho kenyelletsa le li-amino acid tse sirelelitsoeng.Ho feta moo, HBTU e ne e le ea bohlokoa haholo ho kopantseng pitsa e le 'ngoe ea dipeptidyl urea esters, urea le carbamates ho tsoa ho acid.melemo ea HBTU e kenyelelitse lintlha tse latelang: 1) e sa phatlohang 'me ka hona e loketse haholoanyane bakeng sa motsoako oa peptide ea tharollo / e tiileng.2) solubility e phahameng le botsitso ho li-solvents tsa khale.3) e khonahala bakeng sa tlhahlobo ea karabelo ea colorimetric.