I-6-Bromopiperonal CAS 15930-53-7 Ubunyulu > 98.0% (GC) Umgangatho ophezulu
Ubonelelo loMvelisi ngoMgangatho oPhezulu, iMveliso yoRhwebo
Igama leKhemikhali: 6-Bromopiperonal CAS: 15930-53-7
| Igama leMchiza | 6-Bromopiperonal |
| Izithethantonye | I-6-Bromo-3,4-Methylenedioxybenzaldehyde;6-Bromo-1,3-Benzodioxole-5-Carboxaldehyde |
| Inombolo yeCAS | 15930-53-7 |
| Inombolo yeCAT | RF-PI1162 |
| Ubume beStokhwe | Kwi-Stock, iMveliso yoMveliso ukuya kwiiToni |
| Ifomula yeemolekyuli | C8H5BrO3 |
| Ubunzima beMolekyuli | 229.03 |
| Ukunyibilika | Inyibilika kwi-DMSO, iMethanol |
| Uphawu | Ruifu Chemical |
| Into | Iinkcukacha |
| Imbonakalo | Umgubo oMhlophe ukuya koMthubi oKhanyayo |
| Ubunyulu / Indlela yokuHlalutya | >98.0% (GC) |
| Indawo yokunyibilika | 127.0 ~ 132.0℃ |
| Iasidi yasimahla ngeTitration | ≤0.50% |
| Ukungcola ngokupheleleyo | <2.0% |
| Umgangatho woVavanyo | Umgangatho woShishino |
Uvavanyo ngeGas Chromatography AS2
Uhlobo lwekholamu: ZB-5MSi
I-solvent yesampuli: 5% kwi-DCM
Ubushushu be-injector: 300*C
Umthamo wokutofa: 1.0ul
Umlinganiselo wokwahlula: 250:1
Irhasi yokuthwala: iHelium
Ukuhamba kwekholamu: 1.3ml/min Constant
Imilinganiselo yekholamu: 30m x 0.25mm Ubukhulu befilimu 0.25um
Inkqubo yobushushu be-oven: Ubushushu bokuqalisa = 100 * C
Ixesha lokuqala lokubamba = 1.0min
Ireyithi yerempu = 25.0 * C / min
Ubushushu bokugqibela = 300*C
Ixesha lokugqibela lokubamba = 7.0min
Uhlobo lwe-Detector: I-ionization detector yomlilo
Ubushushu bomtshini: 300*C
Free acid titration.FA
Ubunzima malunga no.2.0-3.0g (ukuya kwiindawo ezi-4 zedesimali), chitha kwi-50ml MeOH.Titrate
nge-standardized 0.1 molar sodium hydroxide ukuya kwindawo yokuphela kwi-Metrohm 794
I-Titrino autotitrator isebenzisa i-pH electrode.Tshatisa imathiriyeli ngokuphindwe kabini.
Uvavanyo lwe-asidi yasimahla=V x M x 100/W
apho i-V=Volume ye-0.1M NaOH
W=Ubunzima besampulu kwiigram
M=Ubunzima bemolekyuli yeasidi yasimahla
Iphakheji: Ibhotile, ingxowa yefoyile yeAluminiyam, 25kg/Igubu lekhadibhodi, okanye ngokwemfuno yomthengi.
Imeko yoGcino:Gcina kwizikhongozeli ezivaliweyo kwindawo epholileyo neyomileyo;Khusela ukukhanya kunye nokufuma.
I-6-Bromopiperonal (i-CAS: i-15930-53-7) isetyenziswe njengento ebalulekileyo eluhlaza kunye nephakathi esetyenziswa kwi-organic synthesis, i-pharmaceuticals.I-6-Bromopiperonal isetyenziswe njengendawo ephakathi ekulungiseleleni i-GPR30-i-agonist ekhethiweyo ye-G-1.
