I-Boc-D-Trp-OH CAS 5241-64-5 Ubunyulu > 98.5% (HPLC) Factory
I-Shanghai Ruifu Chemical Co., Ltd. ngumenzi ohamba phambili we-N-Boc-D-Tryptophan (Boc-D-Trp-OH) (CAS: 5241-64-5).I-Ruifu Chemical ibonelela ngothotho lwee-amino acids kunye nezinto eziphuma kuzo.Sinokubonelela ngeenkonzo zehlabathi, ezincinci kunye nezixa ezininzi ezikhoyo.Thenga i-Boc-D-Trp-OH,Please contact: alvin@ruifuchem.com
Igama leMchiza | N-Boc-D-Tryptophan |
Izithethantonye | I-Boc-D-Trp-OH;N-Boc-D-Trp-OH;I-Boc-D-Tryptophan;Nα-Boc-D-Tryptophan;N-(tert-Butoxycarbonyl)-D-Tryptophan;N(alpha)-Boc-D-Tryptophan;N(alpha)-tert-Butoxycarbonyl-D-Tryptophan |
Ubume beStokhwe | Ikhona evenkileni |
Inombolo yeCAS | 5241-64-5 |
Ifomula yeemolekyuli | I-C16H20N2O4 |
Ubunzima beMolekyuli | 304.35 g/mol |
Indawo yokunyibilika | 130.0 ~ 136.0℃ |
Ukuxinana | 1.262 |
Inovakalelo | UkuKhanya okungevayo, ukungeva komoya |
Ukunyibilika kwiMethanol | Phantse Ukungafihli |
Ugcino Temp. | Indawo epholileyo neyomileyo (≤25℃) |
I-COA kunye ne-MSDS | Iyafumaneka |
Udidi | I-Boc-Amino Acids |
Uphawu | Ruifu Chemical |
Iingxelo zoKhuseleko | 24/25 - Gwema ukudibana nolusu kunye namehlo. | ||
WGK eJamani | 3 | Ikhowudi ye-HS | 2922491990 |
Izinto | ImiGangatho yokuHlola | Iziphumo |
Imbonakalo | Mhlophe ukuya kwi-Off-White Powder | Umgubo oMhlophe |
Indawo yokunyibilika | 130.0 ~ 136.0℃ | 130.2 ~ 133.0℃ |
Ukujikeleziswa okuthe ngqo [α]20/D | +20° ± 2.0° (C=2 kwi-AcOH) | +18,5 ° |
Ilahleko ekomisweni | <0.50% | 0.15% |
Intsalela kwi-Ignition | <0.10% | 0.08% |
Ubunyulu / Indlela yokuHlalutya | >98.5% (HPLC) | 99.29% |
Ukucoceka kwamehlo | <0.50% L-Enantiomer | 0.0365% |
300 MHz NMR Spectrum 1H | Iyahambelana neSakhiwo | Iyahambelana |
Uhlalutyo lwe-TLC | Indawo enye | Iyahambelana |
I-Infrared Spectrum | Iyahambelana neSakhiwo | Iyahambelana |
Ukuqukumbela | Le Mveliso ngokuHlolwa kweZivumelwano kunye noMgangatho woShishino | |
Usetyenziso oluphambili | I-Boc-Amino Acids;I-Peptide Synthesis;AbaPhakathi bamayeza |
Iphakheji: Ibhotile eFluorinated, iAluminium foil bag, 25kg/Cardboard Drum, okanye ngokwemfuno yomthengi.
Imeko yoGcino:Gcina kwizikhongozeli ezivaliweyo kwindawo epholileyo, eyomileyo (≤25℃) kunye nendawo yokugcina ingenisa umoya kude nezinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.
Ukuthenga njani?Nceda uqhagamshelaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Amava Eminyaka Eli-15?Sineminyaka engaphezu kwe-15 yamava ekwenziweni nasekuthumeleni kumazwe angaphandle uluhlu olubanzi oluphezulu lwamayeza aphakathi okanye amachiza alungileyo.
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I-N-Boc-D-Tryptophan (i-Boc-D-Trp-OH) (i-CAS: 5241-64-5), i-amino acids kunye ne-derivatives, i-peptide synthesis, i-organic synthesis intermediate, i-pharmaceutical intermediates, i-biochemical reagents.
I-Boc-D-Trp-OH yifom ye-N-Boc ekhuselweyo ye-D-Tryptophan.I-D-Tryptophan i-isomer engeyondalo ye-L-Tryptophan kwaye ihlelwa njenge-amino acid ebalulekileyo.I-D-Tryptophan iye yadityaniswa njengenxalenye yabachasi be-Oxytocin abanamandla abanyanga ukuzala kwangaphambi kwexesha.
Isingeniso esifutshane: I-Boc-D-Tryptophan ingasetyenziselwa njengendawo ephakathi kwi-pharmaceutical synthesis, njenge-tadalafil (tadalafil).i-tadalafil iphuhliswa yinkampani yeLilly yamayeza e-United States.ixhomekeke kwi-PDE-5 ukuphucula umphumo we-vasodilation we-NO ngokuvimbela ukubola kwe-cGMP, ukwenzela ukuba izigulane ze-ED zikwazi ukuphinda zikwazi ukubuyisela amandla e-penile erection, kwaye isetyenziselwa ikakhulu ukuphatha ukungasebenzi kwe-erectile yamadoda.Yayidweliswe eYurophu ngoFebruwari 2003 nase-United States ngoDisemba 2003. Lichiza elitsha lesithathu elivunywe yi-FDA kwi-ED.
Ukulungiselela: i-compound D-Tryptophan (50g, 0.245mol) ilinganiswe kwibhotile yomlomo emithathu, ixutywe ngomatshini, i-500ml yamanzi kunye ne-Triethylamine (74g, 0.731mol), (Boc) 2O (56g, 0.257mol) yongezwa.Ukusabela kwavuselelwa kwi-45 degrees Celsius iiyure ezili-12.Ekupheleni kokuphendula, isisombululo se-0.1% se-phosphoric acid songezwa kwi-dropwise, isixa esikhulu sokuqina senziwa, ixabiso le-PH lilungelelaniswe kwi-7, kwaye emva koko unyango lwenziwa.Ukuhluzwa, isiphumo esiqinileyo siyanyibilika nge-ethyl acetate, isisombululo esisiphumo sihlanjwa kube kanye ngamanzi, i-anhydrous sodium sulfate yomile, kwaye emva kokuhluzwa, isigaba se-organic sisongelwa ukulungisa i-compound ye-Boc-D-Tryptophan kwisixa se I-70.9g (0.233mol), kwaye isivuno se-Boc-D-Tryptophan sibalwa kwi-95.1%.