Boc-His(Dnp)-OH·IPA CAS 25024-53-7 Ubunyulu > 98.5% (HPLC)
I-Shanghai Ruifu Chemical Co., Ltd. ngumenzi ohamba phambili we-Boc-His (Dnp)-OH · IPA (CAS: 25024-53-7) kunye nomgangatho ophezulu.I-Ruifu Chemical ibonelela ngothotho lwee-amino acids kunye nezinto eziphuma kuzo.Sinokubonelela ngeenkonzo zehlabathi, ezincinci kunye nezixa ezininzi ezikhoyo.Thenga i-Boc-Yakhe(Dnp)-OH·IPA,Please contact: alvin@ruifuchem.com
Igama leMchiza | Boc-Wakhe(Dnp)-OH·IPA |
Izithethantonye | Boc-L-His(Dnp)-OH·IPA;Nα-Boc-Nim-2,4-Dinitrophenyl-L-Histidine·Isopropanol;I-Boc-Nim-2,4-Dinitrophenyl-L-Histidine;N-Boc-1-(2,4-Dinitrophenyl)-L-Histidine;N-(tert-Butoxycarbonyl)-1-(2,4-Dinitrophenyl)-L-Histidine |
Ubume beStokhwe | Ikhona evenkileni |
Inombolo yeCAS | 25024-53-7 |
Ifomula yeemolekyuli | C17H19N5O8·C3H8O |
Ubunzima beMolekyuli | 481.50 g/mol |
Indawo yokunyibilika | 98.0 ~ 100.0℃ |
Ukuxinana | 1.49 |
Inovakalelo | Ukukhanya okunovelwano |
Ukunyibilika kwamanzi | Inyibilika kancinane emanzini |
Ugcino Temp. | Indawo epholileyo neyomileyo (≤8℃) |
I-COA kunye ne-MSDS | Iyafumaneka |
Udidi | I-Boc-Amino Acids |
Uphawu | Ruifu Chemical |
Izinto | ImiGangatho yokuHlola | Iziphumo |
Imbonakalo | Umgubo oMthubi oKhanya | Iyahambelana |
Indawo yokunyibilika | 98.0 ~ 100.0℃ | 98.0 ~ 100.0℃ |
Ukujikeleziswa okuthe ngqo [α]20/D | +63.0 ± 3.0° (C=1 kwi-EtOAc) | + 63,8 ° |
Ubunyulu / Indlela yokuHlalutya | >98.5% (HPLC) | 99.37% |
300 MHz NMR Spectrum 1H | Iyahambelana neSakhiwo | Iyahambelana |
Uhlalutyo lwe-TLC | Indawo enye | Iyahambelana |
IR Spectrum | Ngokungqinelana noMgangatho | Iyahambelana |
Ukuqukumbela | Le Mveliso ngokuHlolwa kweZivumelwano kunye noMgangatho woShishino | |
Usetyenziso oluphambili | I-Boc-Amino Acids;I-Peptide Synthesis;AbaPhakathi bamayeza |
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Imeko yoGcino:Ukukhanya Kunovelwano, gcina ebumnyameni.Gcina kwizikhongozeli ezitywiniweyo kwindawo yokugcina impahla epholileyo, eyomileyo (≤8℃) kude nezinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.
Ukuthenga njani?Nceda uqhagamshelaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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Inkcazelo yoKhuseleko
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WGK eJamani 3
FLUKA BRAND F IIKHOWUDI 8
TSCA Ewe
I-Boc-His(Dnp)-OH·IPA (CAS: 25024-53-7), iqela le-Dnp lizinzile kwi-HF kunye ne-TFMSA.I-amino acids kunye ne-derivatives, i-peptide synthesis, i-pharmaceutical intermediates, i-biochemical reagents.Njengemveliso eqhelekileyo ye-L-Histidine, i-Boc-His(Dnp)-OH·IPA ifumene ingqwalasela engakumbi kwinkalo yoshishino lwamachiza kunye neekhemikhali.
Ukulungiselela Ukusebenzisa i-2,4-Dinitrophenyl-L-Histidine njengento yokuqala, i-compound ekujoliswe kuyo i-N- (tert-Butoxycarbonyl) -1- (2, 4-Dinitrophenyl) -L-Histidine ilungiswe yi-amino yokukhusela i-amino reaction kunye ne-dikitert-butyl. dicarbonate.Umzobo we-1 umsebenzi wokulinga we-synthesis reaction formula ye-N- (tert-Butoxycarbonyl) -1- (2, 4-Dinitrophenyl) -L-Histidine: 2,4-Dinitrophenyl-L-Histidine ichithwa kwi-100mL yesisombululo se-sodium hydroxide yamanzi. , I-200mL ye-tetrahydrofuran kunye ne-250g ye-dirt-butyl dicarbonate yongezwa ngokulandelelana, ixabiso le-pH lilawulwa kwi-8-9, kwaye emva kwe-12h yokuphendula, i-ethyl acetate ikhutshwe kabini, i-500mL ngexesha ngalinye;I-HCI isetyenziselwa ukwenza i-acidify isigaba samanzi kwixabiso le-pH ye-1-2, kwaye i-ethyl acetate isetyenziselwa ukukhupha imveliso ngamaxesha e-3, i-500mL ngexesha ngalinye.Iingqimba ze-ester zidibene kwaye zihlanjwe kabini nge-brine egcweleyo, i-200 ml.Yomisa nge-anhydrous sodium sulfate ye-12h, ihluzo, igxininise kwaye i-crystallize, kwaye yome kwi-40-50 ℃ ukufumana i-N- (tert-Butoxycarbonyl) -1- (2, 4-Dinitrophenyl) -L-Histidine.