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I-L-Glutamic Acid α-Benzyl Ester CAS 13030-09-6 (H-Glu-OBzl) i-Assay > 98.5% (HPLC) Umgangatho ophezulu woMfanekiso oFanelekileyo
  • I-L-Glutamic Acid α-Benzyl Ester CAS 13030-09-6 (H-Glu-OBzl) Uvavanyo > 98.5% (HPLC) Umgangatho ophezulu

I-L-Glutamic Acid α-Benzyl Ester CAS 13030-09-6 (H-Glu-OBzl) Uvavanyo > 98.5% (HPLC) Umgangatho ophezulu

Inkcazelo emfutshane:

Igama leKhemikhali: L-Glutamic Acid α-Benzyl Ester

Izithethantonye: H-Glu-OBzl;I-1-Benzyl L-Glutamate

CAS: 13030-09-6

Uvavanyo: >98.5% (HPLC)

Imbonakalo: Umgubo weCrystalline oMhlophe okanye oMhlophe

IiAmino Acids & Derivatives, Umgangatho ophezulu

Qhagamshelana: UGqr. Alvin Huang

Iselula/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com


Iinkcukacha zeMveliso

Iimveliso ezinxulumeneyo

Iithegi zeMveliso

Inkcazo:

I-Shanghai Ruifu Chemical Co., Ltd. ngumenzi ohamba phambili kunye nomthengisi we-L-Glutamic Acid α-Benzyl Ester (H-Glu-OBzl) (i-CAS: 13030-09-6) enomgangatho ophezulu.I-Ruifu Chemical ibonelela ngothotho lwee-amino acids kunye nezinto eziphuma kuzo.Sinokubonelela ngeenkonzo zehlabathi, ezincinci kunye nezixa ezininzi ezikhoyo.Ukuba ufuna i-L-Glutamic Acid α-Benzyl Ester,Please contact: alvin@ruifuchem.com

Iipropati zeMichiza:

Igama leMchiza I-L-Glutamic Acid α-Benzyl Ester
Izithethantonye H-Glu-OBzl;I-HL-Glu-OBzl;I-L-Glutamic Acid 1-Benzyl Ester;I-1-Benzyl L-Glutamate;I-L-Glutamic Acid alpha-Benzyl Ester;(S) -4-Amino-5- (Benzyloxy) -5-Oxopentanoic Acid
Ubume beStokhwe Ikhona evenkileni
Inombolo yeCAS 13030-09-6
Ifomula yeemolekyuli C12H15NO4
Ubunzima beMolekyuli 237.26
Indawo yokunyibilika 140.0 ~ 150.0℃
Ukuxinana 1.245±0.06 g/cm3
Inovakalelo Ukungeva kuMoya, Ukungenwa kukufuma, uBushushu
Ugcino Temp. Itywinwe kwindawo eyomileyo, iVenkile kwindawo yobushushu beGumbi
I-COA kunye ne-MSDS Iyafumaneka
Ukuhlelwa Amino Acids & Derivatives
Uphawu Ruifu Chemical

Iinkcukacha:

Izinto ImiGangatho yokuHlola Iziphumo
Imbonakalo Umgubo weCrystalline oMhlophe okanye oMhlophe Iyahambelana
Ilahleko ekomisweni <0.50% 0.24%
Indawo yokunyibilika 140.0 ~ 150.0℃ 146.0 ~ 150.0℃
Indlela yoVavanyo / yoHlahlelo >98.5% (HPLC) 98.84%
Ukujikeleziswa okuthe ngqo [α]20/D +10.0 ukuya +12.0 ° (C=1, 1mol/L HCl) Iyahambelana
I-Infrared Spectrum Iyahambelana neSakhiwo Iyahambelana
Proton NMR Spectrum Iyahambelana neSakhiwo Iyahambelana
Ukuqukumbela Le Mveliso ngokuHlolwa kweZivumelwano kunye noMgangatho woShishino
Usetyenziso oluphambili Ii-Amino Acids kunye nezinto eziphuma kuzo;AbaPhakathi bamayeza

Inkqubo yeMveliso:

1. L-Glutamic Acid, Sodium Hydroxide, Amanzi, Acetone, Boc-Anhydride
2. I-Boc-L-Glu-OH iphendule nge-Benzyl Bromide kunye ne-Triethylamine ukufumana i-Boc-Glu-OBzl
3. HCL/EA Khupha iBoc-, Lungisa i-PH, Fumana i-H-Glu-OBzl
4. Izinyibilikisi ezisetyenzisiweyo: DMF, Ethyl Acetate, Ethanol

Indlela yoHlahlelo:

1. Ubunyulu (HPLC)
1.1 Izixhobo
Ukusebenza okuphezulu kwechromatography yolwelo, umtshini we-UV3000.
Ibhalansi yohlalutyo lwe-elektroniki
1.2 IiReagents
I-Acetonitrile (ibakala lechromatographic), TFA (ibakala lechromatographic)
1.3 Iimeko zeChromatographic
1.3.1 Uluhlu: C18 ikholamu, 5 μl * 250 * 4.6 mm
1.3.2 Ubungakanani bewavenge: 220nm
Izinga lokuhamba: 1.0 mL / min
Umthamo wesitofu: 10 μL(yereferensi)
Ukunciphisa: i-acetonitrile
Ixesha lokubaleka: imizuzu engama-20
1.4 Ukulungiswa kwesigaba esiphathwayo
Isigaba se-Mobile A (0.1% i-Trifluoroacetic acid Amanzi): ngokuchanekileyo ukufunxa i-1.0 ml ye-TFA ehlanjululwe kwi-1000 ml ngamanzi, ukuxuba kunye ne-degas.
Isigaba seselula B (0.1% i-Trifluoroacetic acid Acetonitrile): ifunxa ngokuchanekileyo i-1.0 ml TFA, ihlanjululwe kwi-1000 ml nge-acetonitrile, i-mix kunye ne-degas.
1.5 Inkqubo yeGradient
Ixesha (umzu) A% B%
0:00 90 10
10.00 10 90
15.00 10 90
15.01 90 10
20.00 90 10
1.6 Ukulungiswa kwesisombululo sesampuli
Ukulinganisa i-0.1 g isampuli kwaye uyinyibilikise nge-acetonitrile kwaye uyihlambulule kwi-100ml.Vuthulula kakuhle ukusetyenziswa kwixesha elizayo, okanye ukugxininiswa okufanayo.Lungiselela iisampuli ezimbini ngokuhambelanayo.
1.7 Ukumiselwa kweSampuli
Hlalutya isampuli ngokwenkqubo yesampulu ilandelayo:
1) Ngaphezulu kwe-1 inaliti yesisombululo esingenanto
2) Isitofu esi-1 sesisombululo sesampulu 1#
3) Isitofu esi-1 sesisombululo sesampulu 2#
1.8.0 Izibalo
1.8.1 Indlela yokulinganisa indawo eyincopho yasetyenziswa ukubala ukusulungeka kwe-HPLC.
1.8.2 Ukutenxa kuthetha ukutenxa kococeko lweenaliti ezimbini aziyi kuba nkulu kune-1%
1.8.3 Ukuba iziphumo zazo zombini iinaliti ziyahlangabezana nemilinganiselo yokwamkelwa, thatha umyinge wobunyulu njengesiphumo sokugqibela.

Ubume bobumdaka:

                                                          

                         

Ukupakishwa kunye noGcino:

Iphakheji: Ibhotile eFluorinated, iAluminium foil bag, 25kg/Cardboard Drum, okanye ngokwemfuno yomthengi.

Imeko yoGcino:Gcina kwizikhongozeli ezivaliweyo kwindawo yokugcina impahla epholileyo, eyomileyo nengena umoya kude nezinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.

Ukupakishwa kunye noGcino:

Iphakheji: Ibhotile eFluorinated, iAluminium foil bag, 25kg/Cardboard Drum, okanye ngokwemfuno yomthengi.

Imeko yoGcino:Gcina kwizikhongozeli ezivaliweyo kwindawo yokugcina impahla epholileyo, eyomileyo nengena umoya kude nezinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.

Izinto eziluncedo:

Umthamo owaneleyo: Izixhobo ezaneleyo kunye namagcisa

Inkonzo yobuNgcali: Inkonzo enye yokuyeka ukuthenga

Ipakethe ye-OEM: Iphakheji yesiko kunye neleyibhile ekhoyo

Ukuhanjiswa ngokukhawuleza: Ukuba ngaphakathi kwesitokhwe, ukuhanjiswa kweentsuku ezintathu kuqinisekisiwe

Ubonelelo oluzinzileyo: Gcina isitokhwe esifanelekileyo

Inkxaso yobuGcisa: Isisombululo seTekhnoloji siyafumaneka

Inkonzo yesiNtu yoHlanganiso: Isuka kwiigram ukuya kwiikhilos

Umgangatho ophezulu: Kusekwe inkqubo epheleleyo yokuqinisekisa umgangatho

FAQ:

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Isicelo:

I-L-Glutamic Acid α-Benzyl Ester (H-Glu-OBzl) (i-CAS: 13030-09-6), i-Amino Acids kunye ne-Derivatives;AbaPhakathi bamayeza.

Bhala umyalezo wakho apha kwaye uwuthumele kuthi