I-Z-Thr-OMe CAS 57224-63-2 ZL-Threonine Methyl Ester Purity ≥98.0% (HPLC)
I-Shanghai Ruifu Chemical Co., Ltd. ngumenzi ohamba phambili we-ZL-Threonine Methyl Ester (Z-Thr-OMe) (CAS: 57224-63-2) enomgangatho ophezulu.I-Ruifu Chemical inokubonelela ngenkonzo yehlabathi jikelele, ixabiso elikhuphisanayo, inkonzo egqwesileyo, encinci kunye nezixa ezininzi ezikhoyo.Thenga i-Z-Thr-OMe,Please contact: alvin@ruifuchem.com
Igama leMchiza | ZL-Threonine Methyl Ester |
Izithethantonye | Z-Thr-OMe;ZL-Thr-OMe;I-N-Benzyloxycarbonyl-L-Threonine Methyl Ester;N-Carbobenzyloxy-L-Threonine Methyl Ester;ZL-Threonine Methyl Ester;N-Cbz-L-Threonine Methyl Ester |
Ubume beStokhwe | Ikhona evenkileni |
Inombolo yeCAS | 57224-63-2 |
Ifomula yeemolekyuli | C13H17NO5 |
Ubunzima beMolekyuli | 267.28 g/mol |
Indawo yokunyibilika | 88.0~93.0℃ |
Inovakalelo | Ubuthathaka bomoya |
Ukunyibilika kwamanzi | Ingxubevange Emanzini |
Ugcino Temp. | Indawo epholileyo neyomileyo (2~8℃) |
Ukuhambisa ngenqanawe | Okuqhelekileyo |
I-COA kunye ne-MSDS | Iyafumaneka |
Uphawu | Ruifu Chemical |
Iingxelo zoKhuseleko | 24/25 - Gwema ukudibana nolusu kunye namehlo. |
WGK eJamani | 3 |
Izinto | ImiGangatho yokuHlola | Iziphumo |
Imbonakalo | Umgubo oMhlophe | Umgubo oMhlophe |
Indawo yokunyibilika | 88.0~93.0℃ | 89.0~90.1℃ |
Ukujikeleziswa okuthe ngqo | -18.0°±2.0° (C=1 kwi-MeOH) | -18.9 ° |
Amanzi nguKarl Fischer | <0.50% | 0.26% |
Ubunyulu / Indlela yokuHlalutya | ≥98.0% (HPLC) | 99.13% |
I-Infrared Spectrum | Ngokungqinelana noLwakhiwo | Iyahambelana |
I-1 H NMR Spectrum | Ngokungqinelana noLwakhiwo | Iyahambelana |
Ukuqukumbela | Imveliso ivavanyiwe kwaye iyahambelana neenkcukacha ezinikiweyo |
Umqulu:Ibhotile, ingxowa yefoyile yeAluminiyam, 25kg/Igubu lekhadibhodi, okanye ngokwemfuno yomthengi.
Imeko yoGcino:Gcina isikhongozeli sivalwe ngokuqinileyo kwaye usigcine kwindawo epholileyo, eyomileyo (2~8℃) kunye nendawo yokugcina impahla engena moya ikude kwizinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.
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Ukuthenga njani?Nceda uqhagamshelaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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I-ZL-Threonine Methyl Ester (Z-Thr-OMe) (i-CAS: 57224-63-2) ingasetyenziselwa njenge-intermediates kwi-organic synthesis kunye ne-pharmaceutical intermediates, esetyenziswa kwi-peptide synthesis.
Yongeza i-70g L-threonine kunye ne-ML methanol kwi-1.1000ml i-flask enentamo ezintathu, lawula ubushushu obungaphantsi kwe-0℃, i-64 ml ye-thionyl chloride yongezwa nge-dropwise.Emva kokugqitywa kwesongezo, umxube wawushushu ukuze uhlaziye i-reflux iiyure ze-4.Idistillation phantsi koxinzelelo oluncitshisiweyo ukuya komile kwi-55℃.Unike i-100g ye-L-threonine methyl ester hydrochloride njengeoli.Ukusabela okulandelayo kubalwe ngesivuno se-100%;2. Kwi-beaker ye-2L, yongeza i-100g ye-L-threonine methyl ester hydrochloride, i-600ml yamanzi, kwaye ulungelelanise i-pH ye-sodium bicarbonate kwi-alkaline, i-z-cl G yongezwa nge-dropwise kwaye i-pH yahlengahlengiswa kwi-8-9 kunye ne-2MOC / l sodium hydroxide yokusabela.Ekupheleni kwempendulo, yongeza i-ethyl acetate 1L ukuyikhupha, yithathe, ihlambe ngamanzi angama-500ml, ihlambe nge-500ml ye-saturated brine, yomise nge-100g anhydrous sodium sulfate, ihluze ngokufunxa, idistilled phantsi koxinzelelo olucuthiweyo de ibe yinto eqinile. i-precipitates, yongeza i-petroleum ether 600Ml crystallization, i-Suction filtration, ukomisa ukufumana i-N-benzyloxycarbonyl-l-threonine methyl ester 140g, isivuno se-89.1%.