Fmoc-Cl CAS 28920-43-6 9-Fluorenylmethyl Chloroformate Purity >99.0% (HPLC) Factory Protecting Reagent
I-Shanghai Ruifu Chemical Co., Ltd. ngumenzi ohamba phambili we-9-Fluorenylmethyl Chloroformate (Fmoc-Cl; Fmoc Chloride) (CAS: 28920-43-6) kunye nomgangatho ophezulu.I-Ruifu Chemical ibonelela ngothotho lwee-reagents ezikhuselayo kunye ne-coupling reagents.Sinokubonelela ngenkonzo yehlabathi jikelele, ixabiso elikhuphisanayo, ubungakanani obuncinci kunye nobuninzi obukhoyo.Thenga iFmoc-Cl,Please contact: alvin@ruifuchem.com
Igama leMchiza | I-9-Fluorenylmethyl Chloroformate |
Izithethantonye | Fmoc-Cl;Fmoc Chloride;(9-Fluorenylmethyl) Chloroformate;I-Chloroformic Acid 9-Fluorenylmethyl Ester;(9H-Fluoren-9-ylmethoxy)carbonyl Chloride;I-9H-Fluoren-9-ylmethyl Chloroformate |
Ubume beStokhwe | KwiStokhwe, Umthamo weMveliso kwiiToni ngeNyanga |
Inombolo yeCAS | 28920-43-6 |
Ifomula yeemolekyuli | C15H11ClO2 |
Ubunzima beMolekyuli | 258.70 g/mol |
Indawo yokunyibilika | 60.0~65.0℃(lit.) |
Ukuxinana | 1.288 g/cm3 |
Inovakalelo | Ubunobuzaza bokufuma, Bunobuzaza bubushushu |
Ukunyibilika | Inyibilika kwi-acetone |
Ugcino Temp. | Indawo epholileyo neyomileyo (2~8℃) |
I-COA kunye ne-MSDS | Iyafumaneka |
Udidi | Ukukhusela iiReagents |
Uphawu | Ruifu Chemical |
Izinto | ImiGangatho yokuHlola | Iziphumo |
Imbonakalo | Umgubo weCrystalline oMhlophe ukuya koMthubi | Iyahambelana |
Indawo yokunyibilika | 60.0 ~ 65.0℃ | 62.6 ~ 63.0℃ |
Ilahleko ekomisweni | <0.50% | 0.19% |
Ukucaca kwesisombululo | I-0.5 gram kwi-10ml Isisombululo esicacileyo se-Acetone | Iyahambelana |
Ubunyulu / Indlela yokuHlalutya | >99.0% (HPLC) | 99.4% |
IR Spectrum | Ngokungqinelana noMgangatho | Iyahambelana |
Ubuninzi beSpectrum | Ngokungqinelana noMgangatho | Iyahambelana |
NMR Spectrum | Ngokungqinelana noMgangatho | Iyahambelana |
Ukuqukumbela | Imveliso ivavanyiwe kwaye iyahambelana neenkcukacha |
Imeko yeChromatographic
Uluhlu: I-Diamonsil C18 (250*4.6mm 5μm)
Isigaba esiphathwayo: I-Acetonitrile: amanzi (PH=3.0 trifluoroacetic acid isisombululo se-aqueous)=80:20
Ukubonwa kobude: 254nm
Ubushushu bekholamu: 25℃
Izinga lokuhamba: 1.0ml / min
Inombolo yepleyiti yethiyori: Ngokweyona ncopho iphambili yokubala kwe-Fmoc-Cl akufuneki ibe ngaphantsi kwama-2000.
Indlela yokuzimisela
Isisombululo se-Acetonitrile esiqulethe i-Fmoc-Cl 20μg nge-1ml yalungiswa njengesisombululo sovavanyo.Isisombululo sovavanyo i-10μl safakwa kwichromatograph, kwaye ichromatogram yarekhodwa de ixesha lokugcinwa kwencopho yecandelo eliphambili laliphindwe kabini.
Iziphumo: Umxholo we-Fmoc-Cl wawungekho ngaphantsi kwe-99.0% ngendlela yokulinganisa indawo
Indawo yokunyibilikisa: Isixhobo se-WRS-2A sokunyibilika: izinga lokushisa: 1.5/min.Indawo yokunyibilika yale mveliso kufuneka ibe yi-60.0 ~ 63.0℃
Ilahleko ekomisweni: Thatha le mveliso kwi-40 ℃ i-vacuum drying ukuya kubunzima obuqhubekayo, ukunciphisa ubunzima akufanele kudlule i-0.5%
Ixesha lokuhlolwa kwakhona: unyaka omnye
Umqulu:Ibhotile, ingxowa yefoyile yeAluminiyam, 25kg/Igubu lekhadibhodi, okanye ngokwemfuno yomthengi.
Ingqalelo:Ukugcinwa kwexesha elide kwiqondo lobushushu begumbi kuya kuthotywa ukubola.Kulula ukufunxa ukufuma kunye nokubola emanzini.
Imeko yoGcino:Gcina kwizikhongozeli ezivaliweyo kwindawo yokugcina impahla epholileyo neyomileyo (2~8℃) kude nezinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.
Ukuhambisa ngenqanawe:Zisa kwihlabathi liphela ngeFedEx / DHL Express.Ukubonelela ngokukhawuleza nangokuthembekileyo.
Ukuthenga njani?Nceda uqhagamshelaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Amava Eminyaka Eli-15?Sineminyaka engaphezu kwe-15 yamava ekwenziweni nasekuthumeleni kumazwe angaphandle uluhlu olubanzi oluphezulu lwamayeza aphakathi okanye amachiza alungileyo.
Iimarike eziphambili?Thengisa kwimarike yasekhaya, eMntla Melika, eYurophu, eIndiya, eKorea, eJapan, eOstreliya, njl.
Iingenelo?Umgangatho ophezulu, ixabiso elifikelelekayo, iinkonzo zengcali kunye nenkxaso yobugcisa, ukuhanjiswa ngokukhawuleza.
UmgangathoIsiqinisekiso?Inkqubo yokulawula umgangatho ongqongqo.Izixhobo zobuchwephesha zokuhlalutya ziquka i-NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, njl.
Iisampulu?Uninzi lweemveliso zibonelela ngeesampulu zasimahla zokuvavanya umgangatho, iindleko zokuthumela kufuneka zihlawulwe ngabathengi.
Factory Audit?Uphicotho-zincwadi lwasefektri wamkelekile.Nceda wenze idinga kwangaphambili.
MOQ?Akukho MOQ.Umyalelo omncinci wamkelekile.
Ixesha lokuzisa? Ukuba ngaphakathi kwesitokhwe, ukuhanjiswa kweentsuku ezintathu kuqinisekisiwe.
Ezothutho?Nge-Express (FedEx, DHL), ngoMoya, ngoLwandle.
Amaxwebhu?Emva kwenkonzo yokuthengisa: I-COA, i-MOA, i-ROS, i-MSDS, njl.
Udibaniso lweSiko?Inokubonelela ngeenkonzo zesiko lokudibanisa ukuze zilungele iimfuno zakho zophando.
Immimiselo yokuhlawula?I-invoyisi yeProforma iya kuthunyelwa kuqala emva kokuqinisekiswa kwe-odolo, efakwe kwiinkcukacha zethu zebhanki.Intlawulo nge-T / T (i-Telex Transfer), i-PayPal, i-Western Union, njl.
Iikhowudi zoMngcipheko
I-R34 - Ibangela ukutsha
I-R20/21/22 - Iyingozi ngokuphefumla, xa udibana nolusu naxa uginyiwe.
Inkcazelo yoKhuseleko
S26 - Xa udibana namehlo, hlambulula ngokukhawuleza ngamanzi amaninzi kwaye ufune iingcebiso zonyango.
S36/37/39 - Nxiba iimpahla ezifanelekileyo zokukhusela, iiglavu kunye nokukhusela amehlo / ubuso.
S45 - Kwimeko yengozi okanye ukuba uziva ungaphilanga, funa ingcebiso kagqirha ngokukhawuleza (bonisa ileyibhile nanini na kunokwenzeka.)
S27 - Khulula ngoko nangoko zonke iimpahla ezingcolisekileyo.
Ii-ID ze-UN UN 3261 8/PG 2
WGK eJamani 3
I-RTECS LQ6250000
FLUKA BRAND F IIKHOWUDI 10-21
Inombolo ye-TSCA
Udidi lweengozi 6.1
Ukupakisha Iqela II
I-9-Fluorenylmethyl Chloroformate (i-Fmoc-Cl; i-Fmoc Chloride) (i-CAS: i-28920-43-6) isetyenziselwa ngokukodwa i-polypeptide synthesis yesigaba esiqinileyo, ingasetyenziselwa njenge-N-protecting reagent ye-oligonucleotide kunye ne-peptide syntheses.I-Fmoc-Cl inokusebenza njenge-reagent yokuqaliswa kweqela le-Fmoc-amino-protecting, elizinzile malunga ne-acids kodwa licolwa ngokulula phantsi kweemeko ezingeyo-hydrolytic ezisisiseko.
Isetyenziselwa i-organic synthesis (iqela elikhusela i-amino acid).I-amino acid derivative reagent, ukufumanisa i-fluorescence, inokubona ngokufanelekileyo iimveliso zokusabela nge-HPLC, kodwa iya kuvelisa ukungcola kwe-dipeptide kunye ne-tripeptide, kwaye i-reagent ayilula ukuyigcina.
I-Fmoc-Cl isetyenziselwa ukulungisa i-N-Fmoc amino acids kwi-slide-phase polypeptide synthesis.Ama-reagents akhuselayo e-amino ukwenzela ukuhlanganiswa kwe-bicyclic proline analogs;I-amino acid derivative reagents, engasetyenziselwa i-HPLC kunye nohlalutyo lwe-capillary electrophoresis, ukhuseleko lwe-N kwi-polypeptides kunye ne-oligonucleotide synthesis
I-Fmoc-Cl yi-reagent ekhuselayo yee-amine eziphambili kunye nesekondari kwaye inovakalelo kwiziseko.Ngokuqhelekileyo isetyenziselwa ukuhlanganiswa kweepolypeptides okanye i-derivatization phambi kwe-amino kunye ne-amino acid uhlalutyo lwe-HPLC kunye nokufunyanwa kwe-fluorescence.
Ukhuseleko: Ityhefu.Idatha yokuguqulwa kwengxelo.Eyothusayo.Xa ishushu ukuze ibole ikhupha imiphunga eyityhefu yeCl-.
Ukugcinwa kwexesha elide kwiqondo lobushushu begumbi kuya kuthotywa ukubola.Kulula ukufunxa ukufuma kunye nokubola emanzini.
Inyibilika kwizinyibilikisi eziphilayo ezifana ne-CH2Cl2, THF kunye ne-dioxane.Inokusabela ngotywala, i-ammonia okanye i-amine, okanye amanzi.