Isixhobo: isixhobo seGC (Shimadzu GC-2010)
Uluhlu: DB-17 Agilent 30mX0.53mmX1.0μm
Ubushushu bokuqala be-oveni: 80℃
Ixesha lokuqala 2.0min
Ireyithi ye-15℃/min
Ubushushu bokugqibela be-oveni: 250 ℃
Ixesha lokugqibela 20min
Irhasi yokuthwala iNitrojeni
Imowudi Ukuhamba rhoqo
Ukuhamba 5.0mL / min
Ukwahlula umlinganiselo 10:1
Ubushushu be-injector: 250℃
Ubushushu besixhobo: 300℃
Umthamo wokutofa 1.0μL
Amanyathelo okufuneka athathwe ngaphambi kohlalutyo:
1. Ikholam yemeko kwi-240℃ ubuncinci bemizuzu engama-30.
2. Hlamba isirinji kwaye ucoce i-injector liner ngokufanelekileyo ukususa ukungcola kohlalutyo lwangaphambili.
3. Hlamba, womise kwaye ugcwalise i-diluent kwiibhotile zesirinji.
Amalungiselelo okunciphisa:
Lungiselela i-2% w / v isisombululo se-sodium hydroxide emanzini.
Ulungiselelo olusemgangathweni:
Ubunzima malunga ne-100mg ye (R) -3-hydroxyprrolidine hydrochloride umgangatho kwi-vial, yongeza i-1mL ye-diluent kwaye udibanise.
Ukulungiselela uvavanyo:
Ubunzima malunga ne-100mg yesampuli yovavanyo kwi-vial, yongeza i-1mL ye-diluent kwaye unyibilikise.Lungiselela kabini.
Inkqubo:
Ukutofa okungenanto (i-diluent), ukulungiswa okusemgangathweni kunye nokulungiswa kovavanyo usebenzisa iimeko ezingaphezulu kwe-GC.Ukungahoyi iincopho ngenxa yokungenanto.Ixesha lokugcinwa kwencopho ngenxa (R) -3-hydroxyprrolidine malunga ne-5.0min.
Phawula:
Xela iziphumo njenge-avareji
Ixesha lokuposa: Nov-13-2021