N,N-Diisopropylethylamine CAS 7087-68-5 (DIPEA) Ucoceko > 99.0% (GC)
I-Ruifu Chemical ngumenzi ohamba phambili we-N, N-Diisopropylethylamine (DIPEA; i-Hunig's Base) (i-CAS: 7087-68-5) enomgangatho ophezulu.I-Ruifu Chemical inokubonelela ngenkonzo yehlabathi jikelele, ixabiso elikhuphisanayo, inkonzo egqwesileyo, encinci kunye nezixa ezininzi ezikhoyo.Thenga i-N,N-Diisopropylethylamine,Please contact: alvin@ruifuchem.com
Igama leMchiza | N,N-Diisopropylethylamine |
Izithethantonye | I-DIPEA;I-DIEA;N-Ethyldisopropylamine;Isiseko sikaHunig;Isiseko sikaHuenig;I-Reagent kaHunig;N-Ethyl-N,N-Diisopropylamine |
Ubume beStokhwe | Kwi-Stock, iMveliso yoRhwebo |
Inombolo yeCAS | 7087-68-5 |
Ifomula yeemolekyuli | C8H19N |
Ubunzima beMolekyuli | 129.25 g/mol |
Indawo yokunyibilika | -45℃ |
Indawo yokubilisa | 127.0 ~ 128.0℃ |
Indawo yokuflasha | 12℃ |
Ukuxinana | 0.742 g/mL ku-25℃(lit.) |
Refractive Index n20/D | 1.41 |
Inovakalelo | Ubuthathaka bomoya |
Ukunyibilika kwamanzi | Ayinyibilikiyo emanzini |
Ukunyibilika | Inyibilika kuTywala |
I-COA kunye ne-MSDS | Iyafumaneka |
Isampulu | Iyafumaneka |
Imvelaphi | Shanghai, China |
Uphawu | Ruifu Chemical |
Izinto | ImiGangatho yokuHlola | Iziphumo |
Imbonakalo | Ulwelo oluNgaMabala oluNgaMabala | Ulwelo oluNgaMabala oluNgaMabala |
Ubunyulu / Indlela yokuHlalutya | >99.0% (GC) | 99.69% |
Diisopropylamine | <0.50% | 0.12% |
Amanzi nguKarl Fischer | <0.20% | 0.10% |
Indawo yokubilisa | 127.0 ~ 128.0℃ | 127.2℃ |
Refractive Index n20/D | 1.412~1.415 | Iyahambelana |
Ubuninzi (20℃) | 0.742~0.760 g/ml | Iyahambelana |
I-Infrared Spectrum | Ngokungqinelana noLwakhiwo | Iyahambelana |
Ukuqukumbela | Imveliso ivavanyiwe kwaye ihambelana neenkcukacha ezinikiweyo |
Umqulu:Ibhotile eneFluorinated, 25kg/Drum, 50kg/Drum, 200kg/Drum, okanye ngokwemfuno yomthengi.
Ugcino:Gcina isikhongozeli sivalwe ngokuqinileyo kwaye usigcine kwindawo epholileyo, eyomileyo (2-8℃) kunye nendawo yokugcina impahla engena moya ikude kwizinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.Ayihambelani ne-acids, i-acid chlorides, i-anhydrides ye-asidi, i-carbon dioxide, ubhedu, ubhedu, i-rubber, i-oxidizing agents, i-nitrate, i-peroxides, i-aldehydes kunye neentsimbi.
Ukuhambisa ngenqanawe:Zisa kwihlabathi liphela ngomoya, ngeFedEx / DHL Express.Ukubonelela ngokukhawuleza nangokuthembekileyo.
Iipropati: Le mveliso kufuneka ibe lulwelo olungenambala olucacileyo.
2. Ukumiselwa komxholo: ngokwe-gas chromatography (i-Chinese Pharmacopoeia 2010 edition Isihlomelo VI E) ukuzimisela.
Uhlobo lwekholomu: SE-54 30m×0.25mm×0.5μm;Isixhobo se-FID;
Ubushushu bokuqala: 80 ℃, umzuzu omnye wokuqala, izinga lokufudumeza 5 ℃ / ngomzuzu, ubushushu bokugqibela: 200 ℃, ixesha lokugqibela: imizuzu eyi-10
Ubushushu bomtshini: 230℃;Iqondo lobushushu lokutofa: 200℃;
Isantya sokuhamba kwe-N2: 20ml-30ml / min;
Isantya sokuhamba kwe-H2: 20ml-30ml / min;
Izinga lokuhamba komoya: 200ml-300ml / min;
Umlinganiselo wokwahlula: 50:1;
Umthamo we-Injection: 0.2μl;
Uvakalelo lweAmplifayi (URANGE) : 10*9.
Iziphumo: Ngokwendlela yokulinganisa indawo, umxholo akufanele ube ngaphantsi kwe-99.0%, kwaye umxholo weDiisopropylamine akufanele ube ngaphezu kwe-0.5%.
3. Ukuzimisela komxholo wamanzi: ngokwendlela yokumisela umswakama (indlela ye-KF) ukumisela, umxholo wamanzi wale mveliso kufuneka ube ngaphantsi kwe-0.2%.
4. Ugcino: Gcina kwindawo epholileyo neyomileyo kude nokukhanya (2-8℃).
5. Ixesha lokuhlolwa kwakhona: unyaka omnye
Ukuthenga njani?Nceda uqhagamshelaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
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I-R20/21/22 - Iyingozi ngokuphefumla, xa udibana nolusu naxa uginyiwe.
I-R10 -Inokutsha
R41 - Umngcipheko womonakalo omkhulu emehlweni
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S36/37/39 - Nxiba iimpahla ezifanelekileyo zokukhusela, iiglavu kunye nokukhusela amehlo / ubuso.
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I-S61-Kuphephe ukukhululwa kokusingqongileyo.Jonga kwimiyalelo ekhethekileyo / kumaphepha edatha yokhuseleko.
S16 - Gcina kude kwimithombo yomlilo.
S27 - Khulula ngoko nangoko zonke iimpahla ezingcolisekileyo.
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Ii-ID ze-UN UN 2734 8/PG 2
WGK eJamani 2
FLUKA BRAND F IIKHOWUDI 9-34
TSCA Ewe
Ikhowudi yeHS 2942000000
Inqaku Lengozi Linokutsha kakhulu/I-Corrosion/Iyingozi
Udidi 3 lweengozi
Ukupakisha Iqela II
Ubuthi LD50 ngomlomo kuMvundla: > 200 - 500 mg/kg
I-N, N-Diisopropylethylamine (i-CAS: 7087-68-5) ikwabizwa ngokuba yi-Hunig's base kwaye ifinyeziwe njenge-DIPEA okanye i-DIEA, I-sterically ithintelwe i-amine kunye ne-organic compound.Ulwelo olungenambala lwathiywa njengesiseko sikaHung ngoSiegfried Hunig, usokhemesti waseJamani.Kwimichiza yezinto eziphilayo, i-N, N-Diisopropylethylamine isetyenziswa njengesiseko.Ekubeni iziko le-nitrogen lodwa liqela le-ethyl kunye namaqela amabini e-isopropyl, Inokubophelela kwiiprotons.I-compound, ngoko ke, isiseko esifana ne-2,2,6,6-tetramethylpiperidine, kodwa i-nucleophile embi, umxube wezakhiwo ezenza ukuba zixabiseke njenge-reagent ye-organic.
I-N, N-Diisopropylethylamine (DIPEA; i-Hunig's Base) (i-CAS: 7087-68-5) ibonisa ukusabela kobundlobongela kunye nokutsha kunye ne-nitrate, i-oxidizing agents, kunye ne-peroxides.Isenokusabela ngokugqithisileyo kwaye inokwenzeka ukuba itshice ngeehalogens kunye neeasidi ezomeleleyo.Kwimeko-bume yealkaline, ikhompawundi kunokwenzeka ukuba isabele ngobundlobongela.Ukongeza, i-compound inokwenza iimveliso ezinetyhefu ezifana ne-n-nitrosamines xa idibene ne-nitrous acid kunye ne-oxygen, i-nitrosating agents, kunye ne-nitrate.Ngaphantsi kweemeko eziqhelekileyo (ubushushu kunye noxinzelelo), i-DIPEA izinzile kakhulu.Nangona kunjalo, iyanyibilika kwiintlobo ezininzi ze-organic solvents.
I-N, N-Diisopropylethylamine (DIPEA; i-Hunig's Base) (i-CAS: i-7087-68-5) isetyenziswe njengesiseko kwi-palladium (0) i-alkoxycarbonylation ye-catalysed of allyl acetates kunye ne-phosphates.Isetyenziswe njenge-neutraizer ye-asidi ye-phosphoric eveliswayo.Ngokucacileyo, i-alkyl ester ayikwazi ukuveliswa ngaphandle kwe-DIPEA.Xa idityaniswe ne-boryl triflates, i-N, N-Diisopropylethylamine isetyenziswe kwi-enolate synthesis ye-ketone ukuze isetyenziswe kwiimpendulo ezichanekileyo ze-cross-adol.I-DIPEA isetyenziswa njenge-proton scavenger kwi-organic synthesis.Ekubeni i-compound iyi-amine ethintelwe ngokungqongqo, ayinayo i-quaternization;ngoko ke, ukwenza ukhetho olugqibeleleyo lwesiseko sokusetyenziswa kunye nee-alkylating agents ezisebenzayo kakhulu.I-DIPEA iluncedo ngokukodwa njengesiseko ekukhuselweni kwee-alcohol njenge-ethers ezifakwe endaweni yokukhusela i-chemistry yeqela.Kwi-synthesis ye-peptides, i-compound isetyenziselwa ukudibanisa i-amino acids.Ubume be-steric kunye nesiseko se-DIPEA ngexesha lokuphendula ukudibanisa kuchaphazela iqondo lokugijima.
I-N, N-Diisopropylethylamine sisibulali-zinambuzane esibalulekileyo kunye nesiphakathi soxubo, esingasetyenziselwa ukudibanisa i-anesthetics kunye ne-herbicides, kwaye inokusetyenziswa njenge-amine ethintelwe ngokungqongqo ukuba ithathe inxaxheba kwiimpendulo ezahlukeneyo ze-catalytic.Uphando lwe-Biochemical.I-organic synthesis intermediates ebalulekileyo, esetyenziswa kakhulu kumayeza, i-pesticide intermediate synthesis, ingasetyenziselwa njenge-solvent, i-agent ye-condensation, i-catalyst, i-amino acid peptide synthesis, njl.