TCFH CAS 94790-35-9 Ubunyulu > 99.0% (HPLC) Factory Coupling Reagents
I-Shanghai Ruifu Chemical Co., Ltd. ngumenzi ohamba phambili we-TCFH (i-CAS: 94790-35-9) enomgangatho ophezulu.I-Ruifu Chemical ibonelela ngothotho lwee-reagents ezikhuselayo kunye ne-coupling reagents.I-Ruifu inokubonelela ngenkonzo yehlabathi jikelele, ixabiso elikhuphisanayo, amanani amancinci kunye nesixa esikhulu esikhoyo.Thenga iTCFH,Please contact: alvin@ruifuchem.com
Igama leMchiza | N,N,N',N'-Tetramethylchloroformamidinium Hexafluorophosphate |
Izithethantonye | TCFH;I-Chloro-N,N,N',N'-Tetramethylformamidinium Hexafluorophosphate;N- [Chloro (dimethylamino) methylene]-N-Methyl-Methanaminium Hexafluorophosphate;Tetramethylchloroformamidinium Hexafluorophosphate |
Ubume beStokhwe | Kwi-Stock, iMveliso yeMisa |
Inombolo yeCAS | 94790-35-9 |
Ifomula yeemolekyuli | I-C5H12ClF6N2P |
Ubunzima beMolekyuli | 280.58 g/mol |
Indawo yokunyibilika | 99.0 ~ 108.0℃ |
Ukuxinana | 1.58 |
Inovakalelo | Ubunobuzaza bokufuma, Bunobuzaza bubushushu |
Ugcino Temp. | Indawo epholileyo neyomileyo (2~8℃) |
I-COA kunye ne-MSDS | Iyafumaneka |
Udidi | Coupling Reagents |
Uphawu | Ruifu Chemical |
Izinto | ImiGangatho yokuHlola | Iziphumo |
Imbonakalo | Mhlophe ukuya kuMhlophe oMhlophe wePowder | Iyahambelana |
Indawo yokunyibilika | 99.0 ~ 108.0℃ | 102.4~103.6℃ |
Ilahleko ekomisweni | <0.50% | 0.15% |
Ubunyulu / Indlela yokuHlalutya | >99.0% (HPLC) | 99.9% |
I-Infrared Spectrum | Iyahambelana neSakhiwo | Iyahambelana |
Proton NMR Spectrum | Iyahambelana neSakhiwo | Iyahambelana |
Ukuqukumbela | Imveliso ivavanyiwe kwaye iyahambelana neenkcukacha ezinikiweyo |
Umqulu:Ibhotile, ingxowa yefoyile yeAluminiyam, 25kg/Igubu lekhadibhodi, okanye ngokwemfuno yomthengi.
Imeko yoGcino:Gcina kwizikhongozeli ezivaliweyo kwindawo yokugcina impahla epholileyo neyomileyo (2~8℃) kude nezinto ezingahambelaniyo.Khusela ukukhanya kunye nokufuma.
Ukuhambisa ngenqanawe:Zisa kwihlabathi liphela ngeFedEx / DHL Express.Ukubonelela ngokukhawuleza nangokuthembekileyo.
Ukuthenga njani?Nceda uqhagamshelaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Amava Eminyaka Eli-15?Sineminyaka engaphezu kwe-15 yamava ekwenziweni nasekuthumeleni kumazwe angaphandle uluhlu olubanzi oluphezulu lwamayeza aphakathi okanye amachiza alungileyo.
Iimarike eziphambili?Thengisa kwimarike yasekhaya, eMntla Melika, eYurophu, eIndiya, eKorea, eJapan, eOstreliya, njl.
Iingenelo?Umgangatho ophezulu, ixabiso elifikelelekayo, iinkonzo zengcali kunye nenkxaso yobugcisa, ukuhanjiswa ngokukhawuleza.
UmgangathoIsiqinisekiso?Inkqubo yokulawula umgangatho ongqongqo.Izixhobo zobuchwephesha zokuhlalutya ziquka i-NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, njl.
Iisampulu?Uninzi lweemveliso zibonelela ngeesampulu zasimahla zokuvavanya umgangatho, iindleko zokuthumela kufuneka zihlawulwe ngabathengi.
Factory Audit?Uphicotho-zincwadi lwasefektri wamkelekile.Nceda wenze idinga kwangaphambili.
MOQ?Akukho MOQ.Umyalelo omncinci wamkelekile.
Ixesha lokuzisa? Ukuba ngaphakathi kwesitokhwe, ukuhanjiswa kweentsuku ezintathu kuqinisekisiwe.
Ezothutho?Nge-Express (FedEx, DHL), ngoMoya, ngoLwandle.
Amaxwebhu?Emva kwenkonzo yokuthengisa: I-COA, i-MOA, i-ROS, i-MSDS, njl.
Udibaniso lweSiko?Inokubonelela ngeenkonzo zesiko lokudibanisa ukuze zilungele iimfuno zakho zophando.
Immimiselo yokuhlawula?I-invoyisi yeProforma iya kuthunyelwa kuqala emva kokuqinisekiswa kwe-odolo, efakwe kwiinkcukacha zethu zebhanki.Intlawulo nge-T / T (i-Telex Transfer), i-PayPal, i-Western Union, njl.
Iikhowudi zoMngcipheko
R36/37/38 - Ukucaphukisa emehlweni, inkqubo yokuphefumla kunye nolusu.
R40 - Ubungqina obuncinci besiphumo somhlaza
Inkcazelo yoKhuseleko
S26 - Xa udibana namehlo, hlambulula ngokukhawuleza ngamanzi amaninzi kwaye ufune iingcebiso zonyango.
S36 - Nxiba iimpahla ezifanelekileyo zokukhusela.
S22 - Musa ukuphefumla uthuli.
WGK eJamani 3
FLUKA BRAND F IIKHOWUDI 3-10-21
N, N, N', N'-Tetramethylchloroformamidinium Hexafluorophosphate (TCFH) (CAS: 94790-35-9), ukudibanisa i-reagent ye-peptide synthesis kunye nokuqala izinto zokulungiselela ezinye ii-reagents zokudibanisa.I-TCFH yinto efanelekileyo yokudibanisa i-peptide synthesis ye-non-hygroscopic.Njengesixhobo sokusebenza ngokubanzi sekhemistri yesigaba esiluqilima, i-TCFH ikhuthaza ikakhulu ukusekwa kwe-carboxylic acid amine derivatives kune-amide kwinkqubo yokudibanisa amino acid.Iluncedo kakhulu ekudityanisweni kwe-amino acids ethintelwe kakhulu, kwaye ineempawu zenkqubo elula nelula yokudibanisa kunye nobomi obude beshelufu.
I-TCFH yindawo ekhuselekileyo, efikelelekayo ye-reagent ye-ester kunye ne-amide synthesis enzima.
I-TCFH njenge-reagent ineenzuzo ezininzi ngaphandle koqoqosho:
-Ngenxa yokudibanisa amandla aphezulu, inokuthi isetyenziswe kwiimpendulo ezenziwe ngaphambili kuphela ngokusebenzisa i-carbodiimide-mediated couplings, ukwandisa ngale ndlela isicelo sayo sokwenziwa kwe-esters, i-diacyl amides kunye ne-acylation ye-amines engasebenziyo.
– Liqinile, lizinze ngokufanelekileyo, xa ligcinwe malunga ne-0°C
– Ukusebenzisa izongezelelo zokudibanisa ezikhoyo ngokubanzi ikhemisti inokufumana umlinganiselo ofanelekileyo wereagent ukulinganisa phakathi kwemveliso yemveliso kunye neempendulo zecala kubandakanya i-epimerization.
Ngethuba lemizuzu emi-2, ukuya kwi-1,1,3,3-Tetramethylurea (2.5 mL, 21 mmol) / 10 mL isisombululo se-toluene inxalenye encinci ye-oxalyl chloride (2.0 mL, 23 mmol) yongezwa ngelixa umxube wokuphendula uvuselelwe. kwiqondo lobushushu lokuhlambela lamanzi omkhenkce.Emva kokuvuselela kwiqondo lokushisa kweeyure ze-18, umxube wokuphendula wawugxininiswe phantsi koxinzelelo oluncitshisiweyo ukuya kumthamo omalunga ne-5 mL kunye ne-precipitate efunyenweyo iqokelelwe ngokuhluzwa.Isiqina esiqokelelweyo sanyibilikiswa malunga ne-20 mL yamanzi kwaye emva koko sanyangwa nge-potassium hexafluorophosphate (3.8g, 21 mmol)/50 mL yesisombululo esinamanzi ngelixa umxube ushukunyiswa ngamandla kwiqondo lobushushu begumbi, ukufumana imvula emhlophe.Imvula yaqokelelwa ngokuhluzwa kwaye yomiswa phantsi kwevacuum.Isiqina saye sanyangwa malunga ne-8 mL ye-acetone kwaye yahluzwa ukususa izinto ezinganyibilikiyo.I-filtrate ebangelwayo yongezwa kwiingxenye ezincinci kwi-60 mL ye-diethyl ether kunye nokuvuselela ngamandla kwiqondo lokushisa.Imveliso efunwayo yaqokelelwa ngokuhluzwa kwaye yomiswa phantsi kwevacuum ukunika i-4.5g (76%).