(Boc) 2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity>99.0% (HPLC) Ile-iṣẹ Idabobo Reagent Ifihan Aworan

(Boc) 2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity>99.0% (HPLC) Reagent Idaabobo Ile-iṣẹ

Apejuwe kukuru:

Orukọ Kemikali: Di-tert-Butyl Iminodicarboxylate

Awọn itumọ ọrọ: (Boc) 2NH;N-Boc-tert-Butylcarbamate

CAS: 51779-32-9

Mimọ:> 99.0% (HPLC)

Irisi: White Crystalline Powder

Idaabobo Reagents, Didara to gaju

Olubasọrọ: Dokita Alvin Huang

Mobile/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

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Apejuwe:

Shanghai Ruifu Chemical Co., Ltd jẹ olupilẹṣẹ asiwaju ti Di-tert-Butyl Iminodicarboxylate ((Boc) 2NH) (CAS: 51779-32-9) pẹlu didara to gaju.Kemikali Ruifu n pese lẹsẹsẹ ti awọn reagents aabo ati awọn isọdọkan.A le pese ifijiṣẹ agbaye, idiyele ifigagbaga, kekere ati awọn iwọn olopobobo ti o wa.Ra Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com

Kemikali Properties:

Orukọ Kemikali	Di-tert-Butyl Iminodicarboxylate
Awọn itumọ ọrọ sisọ	(Boc)2NH;tert-Butyl Iminodicarboxylate;N-Boc-tert-Butylcarbamate;Iminodicarboxylic Acid Di-tert-Butyl Ester;Bis (tert-Butoxycarbonyl) amonia
Iṣura Ipo	O wa
Nọmba CAS	51779-32-9
Ilana molikula	C10H19NO4
Òṣuwọn Molikula	217,27 g / mol
Ojuami Iyo	114.0 ~ 120.0 ℃
iwuwo	1,037 ± 0,06 g / cm3
Ni imọlara	Air Sensitive, Light kókó
Omi Solubility	Ailopin ninu Omi
Solubility	Chloroform, kẹmika
Ibi ipamọ otutu.	Itura & Ibi Gbẹ (2 ~ 8℃)
COA & MSDS	Wa
Ẹka	Idaabobo Reagents
Brand	Ruifu Kemikali

Awọn pato:

Awọn nkan	Ayewo Standards	Awọn abajade
Ifarahan	Funfun Crystalline Powder	Ibamu
Ojuami Iyo	114.0 ~ 120.0 ℃	118.8 ~ 119.3℃
Pipadanu lori Gbigbe	<0.50%	0.10%
Mimọ / Analysis Ọna	> 99.0% (HPLC)	99.6%
Infurarẹẹdi julọ.Oniranran	Ni ibamu si Eto	Ibamu
NMR julọ.Oniranran	Ni ibamu si Eto	Ibamu
Ipari	Ọja naa ti ni idanwo & ni ibamu pẹlu awọn pato ti a fun

Idanwo Mimo:

Ọwọn Chromatographic: SE-54 30m×0.25mm×0.5μm;
Oluwadi: FID
Iwọn otutu akọkọ: 100 ℃
Akoko ibẹrẹ: 1min
Iwọn alapapo: 20 ℃ / min
Ipari otutu: 190 ℃
Ni ipari: 10 min
Iwọn otutu abẹrẹ: 160 ℃
Iwọn otutu ti aṣawari: 200 ℃
Pipin ipin: 50:1;
Iwọn apẹẹrẹ: 0.2μl;
Diluent: kẹmika
Esi: Mimo naa tobi ju 99.0% nipasẹ ọna isọdọtun agbegbe.

Package/Ipamọ/Gbigbe:

Apo:Igo, apo apamọwọ Aluminiomu, 25kg / Paali Drum, tabi gẹgẹbi ibeere alabara.
Ipò Ìpamọ́:Fipamọ sinu awọn apoti edidi ni itura ati ki o gbẹ (2 ~ 8℃) ile itaja kuro lati awọn nkan ti ko ni ibamu.Dabobo lati ina ati ọrinrin.
Gbigbe:Firanṣẹ si agbaye nipasẹ FedEx / DHL Express.Pese ifijiṣẹ yarayara ati igbẹkẹle.

Awọn anfani:

Agbara to to: Awọn ohun elo to ati awọn onimọ-ẹrọ

Iṣẹ Ọjọgbọn: Iṣẹ rira iduro kan

OEM Package: Aṣa package ati aami wa

Ifijiṣẹ Yara: Ti o ba wa laarin ọja iṣura, iṣeduro ifijiṣẹ ọjọ mẹta

Ipese Idurosinsin: Ṣetọju ọja iṣura ti o tọ

Atilẹyin imọ-ẹrọ: Ojutu imọ-ẹrọ wa

Iṣẹ Iṣọkan Aṣa: Larin lati giramu si kilos

Didara to gaju: Ṣeto eto idaniloju didara pipe

FAQ:

Bawo ni lati Ra?Jọwọ kan siDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

15 Ọdun Iriri?A ni diẹ sii ju ọdun 15 ti iriri ni iṣelọpọ ati okeere ti ọpọlọpọ awọn agbedemeji elegbogi didara tabi awọn kemikali to dara.

Awọn ọja akọkọ?Ta si ọja ile, North America, Europe, India, Korea, Japanese, Australia, ati be be lo.

Awọn anfani?Didara to gaju, idiyele ifarada, awọn iṣẹ alamọdaju ati atilẹyin imọ-ẹrọ, ifijiṣẹ yarayara.

DidaraIdaniloju?Eto iṣakoso didara to muna.Awọn ohun elo ọjọgbọn fun itupalẹ pẹlu NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, bbl

Awọn apẹẹrẹ?Pupọ awọn ọja pese awọn apẹẹrẹ ọfẹ fun igbelewọn didara, idiyele gbigbe yẹ ki o san nipasẹ awọn alabara.

Ayẹwo ile-iṣẹ?Ayẹwo ile-iṣẹ kaabo.Jọwọ ṣe ipinnu lati pade ni ilosiwaju.

MOQ?Ko si MOQ.Ibere kekere jẹ itẹwọgba.

Akoko Ifijiṣẹ? Ti o ba wa laarin ọja iṣura, iṣeduro ifijiṣẹ ọjọ mẹta.

Gbigbe?Nipa Express (FedEx, DHL), nipasẹ Air, nipasẹ Okun.

Awọn iwe aṣẹ?Lẹhin iṣẹ tita: COA, MOA, ROS, MSDS, ati bẹbẹ lọ ni a le pese.

Aṣa Synthesis?Le pese awọn iṣẹ iṣelọpọ aṣa lati baamu awọn iwulo iwadii rẹ dara julọ.

Awọn ofin sisan?Iwe risiti Proforma yoo firanṣẹ ni akọkọ lẹhin ijẹrisi aṣẹ, ti ifi alaye banki wa sinu.Isanwo nipasẹ T/T (Telex Gbigbe), PayPal, Western Union, ati bẹbẹ lọ.

51779-32-9 - Ewu ati Aabo:

Awọn aami ewu Xi - Irritant
Awọn koodu Ewu 36/37/38 - Irritating si oju, eto atẹgun ati awọ ara.
Apejuwe Aabo S26 - Ni ọran ti olubasọrọ pẹlu awọn oju, fi omi ṣan lẹsẹkẹsẹ pẹlu ọpọlọpọ omi ki o wa imọran iṣoogun.
S37/39 - Wọ awọn ibọwọ ti o dara ati aabo oju / oju
WGK Germany 3
HS koodu 29241990
Akọsilẹ ewu Irritant

Ohun elo:

Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
Ohun elo Di-tert-Butyl Iminodicarboxylate jẹ agbedemeji elegbogi, eyiti o le ṣetan nipasẹ iṣesi-igbesẹ kan ti formamide ati Boc2O.
A ti lo agbo naa bi reagent fun igbaradi ti amines akọkọ lati awọn halides alkyl.O jẹ olokiki bi yiyan si iṣelọpọ Gabrieli fun iyipada kanna.Amines le tun ti wa ni pese sile lati alcohols nipa gbígbẹ nipa lilo awọn Mitsunobu lenu.Ninu imuse deede, reagent ti yọkuro lati fun iyọ potasiomu, eyiti o jẹ N-alkylated.Awọn ẹgbẹ aabo Boc ti wa ni atẹle kuro labẹ awọn ipo ekikan.
Di-tert-Butyl Iminodicarboxylate jẹ ẹgbẹ amine ti o ni aabo ti a lo lati mura awọn spirocycles ti o ni idinamọ gẹgẹbi awọn alatako CCR1.
Igbaradi ojutu ti DMAP (0.61g, 5.0mmol) ni MeCN (15ml) ti wa ni afikun laiyara si ojutu ti formamide (2.5g,56mmol) ati Boc2O (24)g, 110mol) ni MeCN (15ml).Lẹhin igbiyanju ni iwọn otutu yara fun wakati 4, ojutu ofeefee naa ti tutu si 0 ° C, ati N, N-diethylenediamine (6.97g, 60mmol) ti wa ni afikun laiyara ni 0℃.Abajade adalu ti a rú ni yara otutu fun 12h ati filtered nipasẹ kan tinrin silica paadi;Abajade adalu ti a filtered ni yara otutu.Awọn epo ti wa ni ki o evaporated labẹ dinku titẹ.Ọja robi naa jẹ mimọ nipasẹ kiromatogirafi jeli silica ati pe o pọ pẹlu EtOAc/ hexane (1: 5) lati gba ọja akọle, ti o jẹ funfun ti o lagbara (10.99g, 92%).