I-1-Methyl-3-Pyrrolidinol CAS 13220-33-2 Purity >98.0% (GC)

Incazelo emfushane:

Igama Lekhemikhali: 1-Methyl-3-Pyrrolidinol

Amazwi afanayo: 3-Hydroxy-1-Methylpyrrolidine

I-CAS: 13220-33-2

Ubumsulwa: >98.0% (GC)

Ukubukeka: Uketshezi Oluphuzi Olukhanyayo

Thintana: UDkt. Alvin Huang

Iselula/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

Thumela i-imeyili kithi

Imininingwane Yomkhiqizo

Imikhiqizo Ehlobene

Omaka bomkhiqizo

Incazelo:

I-Ruifu Chemical ingumkhiqizi ohamba phambili we-1-Methyl-3-Pyrrolidinol (3-Hydroxy-1-Methylpyrrolidine) (CAS: 13220-33-2) enekhwalithi ephezulu.I-Ruifu Chemical inganikeza ukulethwa komhlaba wonke, intengo encintisanayo, isevisi enhle kakhulu, amanani amancane kanye nenqwaba etholakalayo.Thenga i-1-Methyl-3-Pyrrolidinol,Please contact: alvin@ruifuchem.com

Chemical Properties:

Igama Lekhemikhali	I-1-Methyl-3-Pyrrolidinol
Omqondofana	I-N-Methyl-3-Pyrrolidinol;I-3-Hydroxy-1-Methylpyrrolidine;N-Methyl-Pyrrolidin-3-ol;I-N-Methyl-Pyrrolidinyl Utshwala;I-1-Methylpyrrolidin-3-ol
Isimo Sesitoko	Ku-Stock, Commercial Production
Inombolo ye-CAS	13220-33-2
I-Molecular Formula	C5H11NO
Isisindo samangqamuzana	101.15 g/mol
Iphuzu elibilayo	75℃/12 mmHg
I-Flash Point	71℃
Ukuminyana	0.921 g/mL ku-25℃ (lit.)
I-Refractive Index n20/D	1.464(lit.)
Kuyazwela	I-Air Sensitive, Hygroscopic
Ukuncibilika	Incibilika Emanzini, Incibilika Otshwaleni, Ether naseBenzene
I-COA ne-MSDS	Iyatholakala
Isampula	Iyatholakala
Umsuka	Shanghai, China
Ibhrendi	I-Ruifu Chemical

Imininingwane:

Izinto	Amazinga Wokuhlola	Imiphumela
Ukubukeka	Uketshezi Oluphuzi Olukhanyayo	Uketshezi Oluphuzi Olukhanyayo
Amanzi nguKarl Fischer	<0.20%	0.15%
Ukuhlanzeka / Indlela Yokuhlaziya	>98.0% (GC)	98.57%
Ukuminyana (20℃)	0.920~0.923	Iyahambisana
I-Refractive Index n20/D	1.463~1.465	Iyahambisana
I-Infrared Spectrum	Ihambisana Nesakhiwo	Iyahambisana
1H NMR Spectrum	Ihambisana Nesakhiwo	Iyahambisana
Isiphetho	Umkhiqizo uhloliwe futhi uthobelana nemibandela enikeziwe

Iphakheji/Isitoreji/Ukuthumela ngomkhumbi:

Iphakheji:Ibhodlela, isikhwama se-Aluminium foil, 25kg/Cardboard Drum, noma ngokwezidingo zekhasimende.

Isimo Sesitoreji:Gcina isiqukathi sivalwe ngokuqinile futhi usigcine endaweni epholile, eyomile (2~8℃) nengena umoya omuhle kude nezinto ezingahambelani.Vikela ekukhanyeni nakumswakama.
Ukuthumela:Zilethe emhlabeni wonke ngendiza, yi-FedEx/DHL Express.Nikeza ukulethwa okusheshayo nokuthembekile.

13220-33-2 - Umzila Wokwenziwa:

13220-33-2 - Indlela Yokulungiselela:

Engeza i-1,2,4-Butanetriol ne-glacial acetic acid embizeni yokusabela, gqugquzela futhi ushise cishe ku-100℃, engeza igesi eyomile ye-hydrogen chloride, bese usabele ku-90~110℃ amahora angu-30, lapho inani elikhulu le-hydrogen chloride liqala avele kugesi lomsila, iphuzu lokugcina lokusabela lihlolwe futhi i-hydrogen chloride yamiswa.Ngemuva kokupholisa, i-material yayikhishwa, igezwe nge-saturated sodium carbonate solution, futhi ifakwe ngaphansi kwe-distillation ngaphansi kwengcindezi encishisiwe, kanye ne-120 kuya ku-135 ℃.(12.6 kuya ku-13. 3kPa) ingxenyenamba, i.e., i-1,4-Dichloro-2-Butanol oily matter, ikhiqiza i-50% ~ 60%.
Ukuhamba ngebhayisikili isixazululo esinamanzi se-1,4-Dichloro-2-Butanol ne-Methylamine singezwe ebhodweni lokuhamba ngebhayisikili, futhi sishisiswe ku-120℃.Ngaphansi kokushisa okuvaliwe, futhi ukusabela kwavuselelwa i-10h.Ngemuva kokupholisa, kwengezwa i-sodium hydroxide eqinile, futhi usawoti we-inorganic onciphile wawuhlungwa.Ungqimba lwamafutha lwahlukaniswa futhi lwafakwa ngaphansi kwe-vacuum distillation, kanye nengxenye engu-76-85℃.(2.1 kPa) yaqoqwa ukuze kube umkhiqizo oqediwe.Ukukhishwa kongqimba olunamanzi nge-benzene nakho kukhiqiza ingxenye ye-1-Methyl-3-Pyrrolidinol.Isivuno sasicishe sibe ngama-60%.
3. Izinqubo ezibalulekile:
3.1 Inqubo yokusabela eshintshiwe: lawula isikhathi sokusabela futhi uthole indawo yokugcina yokusabela
3.2 Inqubo ye-vacuum distillation ye-1,4-Dichloro-2-Butanol: lawula i-vacuum degree ye-vacuum distillation kanye nokushisa kwengxenye
3.3 Inqubo yokusabela ngomjikelezo: lawula izinga lokushisa lokusabela nesikhathi
3.4 1-Methyl-3-Pyrrolidinol vacuum distillation inqubo: lawula vacuum degree of vacuum distillation kanye lokushisa ingxenyenamba
4. Amaphuzu okulawula ikhwalithi:
Iphoyinti lokulawula ikhwalithi 1: 1,2,4-Butanetriol izinga lekhwalithi yezinto ezingavuthiwe
Iphoyinti lokulawula ikhwalithi 2: Izinga lekhwalithi yokulawula okumaphakathi kokusabela kokuhamba ngebhayisikili
Iphoyinti lokulawula ikhwalithi 3: 1,4-Dichloro-2-Butanol izinga elimaphakathi lekhwalithi
Iphoyinti lokulawula ikhwalithi 4: I-1-Methyl-3-Pyrrolidinol iqedile izinga lekhwalithi yomkhiqizo

13220-33-2 - Indlela Yokuhlola:

Okuqukethwe Umswakama: Thatha lo mkhiqizo futhi uwuhlole ngokwendlela yokunquma umswakama (Indlela Yokuqala A Yesithasiselo Ⅷ M, Uhlelo lwango-2010 lwe-People's Republic of China Pharmacopoeia).Umswakama akufanele udlule u-0.2%.
Ukuminyana Okuhlobene: Ukuminyana okuhlobene kwalo mkhiqizo (Isithasiselo VI A Sengxenye II, uhlelo lwango-2010) ngu-0.920~0.923
I-Refractive Index: Inkomba ye-refractive yalo mkhiqizo (Isithasiselo VI F sengxenye II yohlelo lwango-2010) ngu-1.463~1.465
Ukunqunywa kokuqukethwe: Okuqukethwe kwe-1-Methyl-3-Pyrrolidinol akufanele kube ngaphansi kuka-98.0% nge-chromatography yegesi (Isithasiselo Ⅴ E, Ingxenye II, uhlelo luka-2010).
Ikholomu: I-Capillary in silica encibilikisiwe SPB-5, ububanzi bangaphakathi 0.32mm, ubude 30m
T Injector: 300 ℃
I-FID: 320 ℃
Ikholomu T: 80℃ imizuzu emi-5, kuye ku-200℃ ku-5℃/min, bese ku-200℃ imizuzu engu-7
Isithwali: I-Helium ku-1 ml/min
Isilinganiso Sokuhlukanisa: 100:1
Umjovo: 1 microliter
Isixazululo sokuhlola: chitha u-200mg wesampula ngaphansi kokuhlaziywa ku-10ml ye-methanol.Jova i-microliter engu-1.I-1μl yafakwa ku-chromatograph yegesi ukuze kuqoshwe i-chromatogram.Okuqukethwe kwe-1-Methyl-3-Pyrrolidinol kubalwe ngendlela evamile yendawo ephakeme kakhulu.

Izinzuzo:

Amandla Anele: Izinsiza ezanele kanye nochwepheshe

Isevisi Yobuchwepheshe: Isevisi yokuthenga yokuma eyodwa

Iphakheji le-OEM: Iphakheji yangokwezifiso kanye nelebula iyatholakala

Ukulethwa Okusheshayo: Uma kungaphakathi kwesitoko, ukulethwa kwezinsuku ezintathu kuqinisekisiwe

Impahla Ezinzile: Gcina isitoko esinengqondo

Ukusekelwa Kwezobuchwepheshe: Isixazululo sezobuchwepheshe siyatholakala

Isevisi Yokuhlanganisa Ngokwezifiso: Isukela kumagremu kuye kumakhilo

Ikhwalithi Ephezulu: Kusungulwe uhlelo oluphelele lokuqinisekisa ikhwalithi

I-FAQ:

Indlela Yokuthenga?Sicela uxhumaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

Iminyaka engu-15 Yokuhlangenwe nakho?Sinesipiliyoni seminyaka engaphezu kwe-15 ekwakhiweni nasekuthumeleni kwamanye amazwe uhla olubanzi lwezinga eliphezulu lokuxhumanisa imithi noma amakhemikhali amahle.

Izimakethe Eziyinhloko?Thengisa emakethe yasekhaya, eNyakatho Melika, eYurophu, eNdiya, eKorea, eJapane, e-Australia, njll.

Izinzuzo?Ikhwalithi ephezulu, intengo ethengekayo, izinsizakalo ezichwepheshile nokusekelwa kobuchwepheshe, ukulethwa okusheshayo.

IkhwalithiIsiqiniseko?Isistimu yokulawula ikhwalithi eqinile.Imishini yobuchwepheshe yokuhlaziya ifaka i-NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, NOMA, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, njll.

Amasampula?Imikhiqizo eminingi inikeza amasampula wamahhala wokuhlolwa kwekhwalithi, izindleko zokuthumela kufanele zikhokhelwe amakhasimende.

Ukuhlolwa Kwemboni?Wamukelekile ekucwaningweni kwemboni.Sicela wenze i-aphoyintimenti kusengaphambili.

I-MOQ?Ayikho i-MOQ.I-oda elincane liyamukeleka.

Isikhathi sokuthumela? Uma kungaphakathi kwesitoko, ukulethwa kwezinsuku ezintathu kuqinisekisiwe.

Ezokuthutha?By Express (FedEx, DHL), by Air, by Sea.

Amadokhumenti?Ngemuva kwenkonzo yokuthengisa: I-COA, i-MOA, i-ROS, i-MSDS, njll.

Custom Synthesis?Ingahlinzeka ngezinsizakalo zokwenziwa ngokwezifiso ukuze zilingane kangcono nezidingo zakho zocwaningo.

Imigomo Yokukhokha?I-invoyisi ye-Proforma izothunyelwa kuqala ngemva kokuqinisekiswa kwe-oda, kufakwe nemininingwane yethu yasebhange.Inkokhelo nge-T/T (Telex Transfer), PayPal, Western Union, njll.

13220-33-2 - Ubungozi Nokuphepha:

Izimpawu Zengozi Xi - Iyacasula
Amakhodi Engozi
36/37/38 - Ukucasula amehlo, uhlelo lokuphefumula kanye nesikhumba.
Incazelo Yokuphepha
S26 - Uma uthintana namehlo, geza ngokushesha ngamanzi amaningi futhi ufune iseluleko sezokwelapha.
I-S36/37/39 - Gqoka izingubo zokuzivikela ezifanele, amagilavu nokuvikela iso/ubuso.
I-WGK Germany 3
I-HS Code 2933990099

13220-33-2 - Isicelo:

I-1-Methyl-3-Pyrrolidinol (3-Hydroxy-1-Methylpyrrolidine) (i-CAS: 13220-33-2) isetshenziswa njenge-organic synthesis intermediate, esetshenziswa njengendawo ephakathi kwemithi embonini yezemithi.