(Boc)2NH CAS 51779-32-9 Di-tert-Butyl Iminodicarboxylate Purity >99.0% (HPLC) Factory Protecting Reagent

Incazelo emfushane:

Igama Lekhemikhali: Di-tert-Butyl Iminodicarboxylate

Omqondofana: (Boc)2NH;I-N-Boc-tert-Butylcarbamate

CAS: 51779-32-9

Ubumsulwa: >99.0% (HPLC)

Ukubukeka: I-Crystalline Powder Emhlophe

Ukuvikela ama-reagents, Ikhwalithi ephezulu

Thintana: UDkt. Alvin Huang

Iselula/Wechat/WhatsApp: +86-15026746401

E-Mail: alvin@ruifuchem.com

Thumela i-imeyili kithi

Imininingwane Yomkhiqizo

Imikhiqizo Ehlobene

Omaka bomkhiqizo

Incazelo:

I-Shanghai Ruifu Chemical Co., Ltd. ingumkhiqizi ohamba phambili we-Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9) enekhwalithi ephezulu.I-Ruifu Chemical ihlinzeka ngochungechunge lwama-reagents avikelayo kanye nama-reagents ahlanganisayo.Singahlinzeka ngezidingo zomhlaba wonke, amanani ancintisanayo, amanani amancane kanye nenqwaba etholakalayo.Thenga i-Di-tert-Butyl Iminodicarboxylate,Please contact: alvin@ruifuchem.com

Chemical Properties:

Igama Lekhemikhali	I-Di-tert-Butyl Iminodicarboxylate
Omqondofana	(Boc)2NH;tert-Butyl Iminodicarboxylate;I-N-Boc-tert-Butylcarbamate;Iminodicarboxylic Acid Di-tert-Butyl Ester;I-Bis(tert-Butoxycarbonyl)ammonia
Isimo Sesitoko	Kukhona kusitoki
Inombolo ye-CAS	51779-32-9
I-Molecular Formula	I-C10H19NO4
Isisindo samangqamuzana	217.27 g/mol
I-Melting Point	114.0 ~ 120.0℃
Ukuminyana	1.037±0.06 g/cm3
Kuyazwela	Izwela Umoya, Izwela Ukukhanya
Ukuncibilika kwamanzi	Ayincibiliki Emanzini
Ukuncibilika	I-Chloroform, iMethanol
Isikhathi Sokugcina.	Indawo epholile neyomile (2~8℃)
I-COA ne-MSDS	Iyatholakala
Isigaba	Ukuvikela ama-reagents
Ibhrendi	I-Ruifu Chemical

Imininingwane:

Izinto	Amazinga Wokuhlola	Imiphumela
Ukubukeka	I-Crystalline Powder Emhlophe	Iyahambisana
I-Melting Point	114.0 ~ 120.0℃	118.8 ~ 119.3 ℃
Ukulahlekelwa Ekumisweni	<0.50%	0.10%
Ukuhlanzeka / Indlela Yokuhlaziya	>99.0% (HPLC)	99.6%
I-Infrared Spectrum	Ivumelana Nesakhiwo	Iyahambisana
I-NMR Spectrum	Ivumelana Nesakhiwo	Iyahambisana
Isiphetho	Umkhiqizo uhloliwe futhi uthobelana nemibandela enikeziwe

Ukuhlolwa Kobumsulwa:

Ikholomu ye-Chromatographic: SE-54 30m×0.25mm×0.5μm;
Umtshina: FID
Izinga lokushisa lokuqala: 100 ℃
Isikhathi sokuqala: 1min
Izinga lokushisa: 20 ℃/min
Izinga lokushisa lokugcina: 190 ℃
Ekugcineni: 10min
Izinga lokushisa lomjovo: 160 ℃
Izinga lokushisa lomtshina: 200 ℃
Isilinganiso sokuhlukaniswa: 50:1;
Usayizi wesampula: 0.2μl;
I-Diluent: i-methanol
Umphumela: Ubumsulwa bebungaphezu kwama-99.0% ngendlela yokujwayela kwendawo.

Iphakheji/Isitoreji/Ukuthumela ngomkhumbi:

Iphakheji:Ibhodlela, isikhwama se-Aluminium foil, 25kg/Cardboard Drum, noma ngokwezidingo zekhasimende.
Isimo Sesitoreji:Gcina ezitsheni ezivaliwe endaweni epholile neyomile (2~8℃) kude nezinto ezingahambelani.Vikela ekukhanyeni nakumswakama.
Ukuthumela:Thumela emhlabeni wonke nge-FedEx / DHL Express.Nikeza ukulethwa okusheshayo nokuthembekile.

Izinzuzo:

Amandla Anele: Izinsiza ezanele kanye nochwepheshe

Isevisi Yobuchwepheshe: Isevisi yokuthenga yokuma eyodwa

Iphakheji le-OEM: Iphakheji yangokwezifiso kanye nelebula iyatholakala

Ukulethwa Okusheshayo: Uma kungaphakathi kwesitoko, ukulethwa kwezinsuku ezintathu kuqinisekisiwe

Impahla Ezinzile: Gcina isitoko esinengqondo

Ukusekelwa Kwezobuchwepheshe: Isixazululo sezobuchwepheshe siyatholakala

Isevisi Yokuhlanganisa Ngokwezifiso: Isukela kumagremu kuye kumakhilo

Ikhwalithi Ephezulu: Kusungulwe uhlelo oluphelele lokuqinisekisa ikhwalithi

I-FAQ:

Indlela Yokuthenga?Sicela uxhumaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com

Iminyaka engu-15 Yokuhlangenwe nakho?Sinesipiliyoni seminyaka engaphezu kwe-15 ekwakhiweni nasekuthumeleni kwamanye amazwe uhla olubanzi lwezinga eliphezulu lokuxhumanisa imithi noma amakhemikhali amahle.

Izimakethe Eziyinhloko?Thengisa emakethe yasekhaya, eNyakatho Melika, eYurophu, eNdiya, eKorea, eJapane, e-Australia, njll.

Izinzuzo?Ikhwalithi ephezulu, intengo ethengekayo, izinsizakalo ezichwepheshile nokusekelwa kobuchwepheshe, ukulethwa okusheshayo.

IkhwalithiIsiqiniseko?Isistimu yokulawula ikhwalithi eqinile.Imishini yobuchwepheshe yokuhlaziya ifaka i-NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, NOMA, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, njll.

Amasampula?Imikhiqizo eminingi inikeza amasampula wamahhala wokuhlolwa kwekhwalithi, izindleko zokuthumela kufanele zikhokhelwe amakhasimende.

Ukuhlolwa Kwemboni?Wamukelekile ekucwaningweni kwemboni.Sicela wenze i-aphoyintimenti kusengaphambili.

I-MOQ?Ayikho i-MOQ.I-oda elincane liyamukeleka.

Isikhathi sokuthumela? Uma kungaphakathi kwesitoko, ukulethwa kwezinsuku ezintathu kuqinisekisiwe.

Ezokuthutha?By Express (FedEx, DHL), by Air, by Sea.

Amadokhumenti?Ngemuva kwenkonzo yokuthengisa: I-COA, i-MOA, i-ROS, i-MSDS, njll.

Custom Synthesis?Ingahlinzeka ngezinsizakalo zokwenziwa ngokwezifiso ukuze zilingane kangcono nezidingo zakho zocwaningo.

Imigomo Yokukhokha?I-invoyisi ye-Proforma izothunyelwa kuqala ngemva kokuqinisekiswa kwe-oda, kufakwe nemininingwane yethu yasebhange.Inkokhelo nge-T/T (Telex Transfer), PayPal, Western Union, njll.

51779-32-9 - Ubungozi Nokuphepha:

Izimpawu Zengozi Xi - Iyacasula
Amakhodi Engozi 36/37/38 - Ukucasula amehlo, uhlelo lokuphefumula kanye nesikhumba.
Incazelo Yezokuphepha S26 - Uma uthintana namehlo, geza ngokushesha ngamanzi amaningi futhi ufune iseluleko sezokwelapha.
I-S37/39 - Gqoka amagilavu afanelekile kanye nokuvikela iso/ubuso
I-WGK Germany 3
I-HS Code 29241990
I-Hazard Note Irritant

Isicelo:

I-Di-tert-Butyl Iminodicarboxylate ((Boc)2NH) (CAS: 51779-32-9)
I-Di-tert-Butyl Iminodicarboxylate iyisisetshenziswa esimaphakathi semithi, esingalungiswa ngokusabela kwesinyathelo esisodwa se-formamide ne-Boc2O.
I-compound isetshenziswa njenge-reagent yokulungiswa kwama-amine ayinhloko avela ku-alkyl halides.Yaduma njengenye indlela ye-Gabriel synthesis yokuguqulwa okufanayo.Ama-amine angabuye alungiswe kusuka otshwaleni ngokuphelelwa amanzi emzimbeni kusetshenziswa ukusabela kwe-Mitsunobu.Ekusetshenzisweni okujwayelekile i-reagent ikhishwa ukuze inikeze usawoti we-potassium, okuyi-N-alkylated.Amaqembu okuvikela ama-Boc abe esesuswa ngaphansi kwezimo ezine-asidi.
I-Di-tert-Butyl Iminodicarboxylate iyiqembu le-amine elivikelwe elisetshenziselwa ukulungisa ama-spirocycle avinjiwe njengabaphikisi be-CCR1.
Ukulungiswa kwesisombululo se-DMAP (0.61g, 5.0mmol) ku-MeCN (15ml) yengezwa kancane kancane kusixazululo se-formamide (2.5g,56mmol) ne-Boc2O (24).g, 110mol) ku-MeCN (15ml).Ngemva kokunyakazisa ekamelweni lokushisa amahora angu-4, isixazululo esiphuzi sapholiswa sibe ngu-0°C, futhi i-N,N-diethylenediamine (6.97g, 60mmol) yengezwa kancane kancane ku-0℃.Ingxube ewumphumela yashukunyiswa ekamelweni lokushisa i-12h futhi ihlungwe nge-silica pad encane;ingxube ewumphumela yahlungwa ekamelweni lokushisa.I-solvent ibe ihwamuka ngaphansi kwengcindezi encishisiwe.Umkhiqizo ongahluziwe wahlanzwa nge-silica gel chromatography futhi wafakwa nge-EtOAc/hexane (1:5) ukuze uthole umkhiqizo wesihloko, oqinile omhlophe (10.99g, 92%).