I-TCFH CAS 94790-35-9 Purity >99.0% (HPLC) Factory Coupling Reagents
I-Shanghai Ruifu Chemical Co., Ltd. ingumkhiqizi ohamba phambili we-TCFH (CAS: 94790-35-9) enekhwalithi ephezulu.I-Ruifu Chemical ihlinzeka ngochungechunge lwama-reagents avikelayo kanye nama-reagents ahlanganisayo.I-Ruifu inganikeza ukulethwa komhlaba wonke, intengo encintisanayo, amanani amancane nayinqwaba atholakalayo.Thenga i-TCFH,Please contact: alvin@ruifuchem.com
Igama Lekhemikhali | N,N,N',N'-Tetramethylchloroformamidinium Hexafluorophosphate |
Omqondofana | TCFH;I-Chloro-N,N,N',N'-Tetramethylformamidinium Hexafluorophosphate;N--[Chloro(dimethylamino)methylene]-N-Methyl-Methanaminium Hexafluorophosphate;I-Tetramethylchloroformamidinium Hexafluorophosphate |
Isimo Sesitoko | In Stock, Mass Production |
Inombolo ye-CAS | 94790-35-9 |
I-Molecular Formula | I-C5H12ClF6N2P |
Isisindo samangqamuzana | 280.58 g/mol |
I-Melting Point | 99.0~108.0℃ |
Ukuminyana | 1.58 |
Kuyazwela | Kuyazwela Umswakama, Kuyazwela Ukushisa |
Isikhathi Sokugcina. | Indawo epholile neyomile (2~8℃) |
I-COA ne-MSDS | Iyatholakala |
Isigaba | Ama-Reagents wokuhlanganisa |
Ibhrendi | I-Ruifu Chemical |
Izinto | Amazinga Wokuhlola | Imiphumela |
Ukubukeka | I-Crystalline Powder emhlophe ukuya kokumhlophe | Iyahambisana |
I-Melting Point | 99.0~108.0℃ | 102.4 ~ 103.6℃ |
Ukulahlekelwa Ekumisweni | <0.50% | 0.15% |
Ukuhlanzeka / Indlela Yokuhlaziya | >99.0% (HPLC) | 99.9% |
I-Infrared Spectrum | Ivumelana Nesakhiwo | Iyahambisana |
I-Proton NMR Spectrum | Ivumelana Nesakhiwo | Iyahambisana |
Isiphetho | Umkhiqizo uhloliwe futhi uthobelana nemibandela enikeziwe |
Iphakheji:Ibhodlela, isikhwama se-Aluminium foil, 25kg/Cardboard Drum, noma ngokwezidingo zekhasimende.
Isimo Sesitoreji:Gcina ezitsheni ezivaliwe endaweni epholile neyomile (2~8℃) kude nezinto ezingahambelani.Vikela ekukhanyeni nakumswakama.
Ukuthumela:Thumela emhlabeni wonke nge-FedEx / DHL Express.Nikeza ukulethwa okusheshayo nokuthembekile.
Indlela Yokuthenga?Sicela uxhumaneDr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com
Iminyaka engu-15 Yokuhlangenwe nakho?Sinesipiliyoni seminyaka engaphezu kwe-15 ekwakhiweni nasekuthumeleni kwamanye amazwe uhla olubanzi lwezinga eliphezulu lokuxhumanisa imithi noma amakhemikhali amahle.
Izimakethe Eziyinhloko?Thengisa emakethe yasekhaya, eNyakatho Melika, eYurophu, eNdiya, eKorea, eJapane, e-Australia, njll.
Izinzuzo?Ikhwalithi ephezulu, intengo ethengekayo, izinsizakalo ezichwepheshile nokusekelwa kobuchwepheshe, ukulethwa okusheshayo.
IkhwalithiIsiqiniseko?Isistimu yokulawula ikhwalithi eqinile.Imishini yobuchwepheshe yokuhlaziya ifaka i-NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, NOMA, KF, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, njll.
Amasampula?Imikhiqizo eminingi inikeza amasampula wamahhala wokuhlolwa kwekhwalithi, izindleko zokuthumela kufanele zikhokhelwe amakhasimende.
Ukuhlolwa Kwemboni?Wamukelekile ekucwaningweni kwemboni.Sicela wenze i-aphoyintimenti kusengaphambili.
I-MOQ?Ayikho i-MOQ.I-oda elincane liyamukeleka.
Isikhathi sokuthumela? Uma kungaphakathi kwesitoko, ukulethwa kwezinsuku ezintathu kuqinisekisiwe.
Ezokuthutha?By Express (FedEx, DHL), by Air, by Sea.
Amadokhumenti?Ngemuva kwenkonzo yokuthengisa: I-COA, i-MOA, i-ROS, i-MSDS, njll.
Custom Synthesis?Ingahlinzeka ngezinsizakalo zokwenziwa ngokwezifiso ukuze zilingane kangcono nezidingo zakho zocwaningo.
Imigomo Yokukhokha?I-invoyisi ye-Proforma izothunyelwa kuqala ngemva kokuqinisekiswa kwe-oda, kufakwe nemininingwane yethu yasebhange.Inkokhelo nge-T/T (Telex Transfer), PayPal, Western Union, njll.
Amakhodi Engozi
R36/37/38 - Ukucasula amehlo, uhlelo lokuphefumula kanye nesikhumba.
R40 - Ubufakazi obulinganiselwe bomphumela we-carcinogenic
Incazelo Yokuphepha
S26 - Uma uthintana namehlo, geza ngokushesha ngamanzi amaningi futhi ufune iseluleko sezokwelapha.
I-S36 - Gqoka izingubo ezifanele zokuzivikela.
S22 - Ungaphefumuli uthuli.
I-WGK Germany 3
I-FLUKA BRAND F AMAKHODI 3-10-21
N,N,N',N'-Tetramethylchloroformamidinium Hexafluorophosphate (TCFH) (CAS: 94790-35-9), i-coupling reagent ye-peptide synthesis kanye nezinto zokuqala zokulungiselela amanye ama-reagents ahlanganisayo.I-TCFH iyi-reagent enhle yokuhlanganisa i-peptide synthesis synthesis.Njengesisebenzi esivamile sokwenza kusebenze samakhemikhali esigaba esiqinile, i-TCFH ikhuthaza ngokuyinhloko ukwakheka kokuphuma kokuphuma kwe-amine ye-carboxylic acid kune-amide enqubweni yokuhlanganisa ama-amino acid.Iwusizo kakhulu ekuhlanganisweni kwama-amino acid avinjwe kakhulu, futhi inezici zenqubo elula nelula yokuhlanganisa nempilo ende yeshalofu.
I-TCFH iyi-reagent ephephile, ethengekayo ye-ester kanye ne-amide synthesis enzima.
I-TCFH njenge-reagent inezinzuzo ezimbalwa ngaphandle kokuthi iyonga:
- Ngenxa yamandla aphezulu okuhlangana, ingasetshenziswa ekuphenduleni okwenziwe ngaphambilini kuphela ngokusebenzisa ama-couplings e-carbodiimide-mediated, enwebeka ngale ndlela ukusetshenziswa kwayo kokwakhiwa kwama-esters, ama-diacyl amide kanye ne-acylation yama-amine angasebenzi.
- Iqinile, inhlanganisela ezinzile, lapho igcinwe cishe ku-0°C
- Ngokusebenzisa izithasiselo zokuhlanganisa ezitholakala kabanzi usokhemisi angathola isilinganiso esilungile se-reagent ukuze alinganisele phakathi kwesivuno somkhiqizo kanye nokusabela okuseceleni okuhlanganisa ukucwiliswa kwe-epimerization.
Esikhathini esiyimizuzu emi-2, ku-1,1,3,3-Tetramethylurea (2.5 mL, 21 mmol)/10 mL isixazululo se-toluene ingxenye encane ye-oxalyl chloride (2.0 mL, 23 mmol) yengezwe ngenkathi ingxube yokusabela inyakaziswa. at lokushisa okugeza ice-amanzi.Ngemva kokunyakazisa ekamelweni lokushisa amahora angu-18, ingxube yokusabela yagxiliswa ngaphansi kwengcindezi encishisiwe ibe umthamo ongaba ngu-5 mL futhi imvula ewumphumela yaqoqwa ngokuhlunga.Okuqinile okuqoqiwe kwancibilika cishe ku-20 mL wamanzi kwase kuxutshwa nge-potassium hexafluorophosphate (3.8g, 21 mmol)/50 mL yesisombululo esinamanzi kuyilapho ingxube inyakaziswa ngamandla ekamelweni lokushisa, ukuze kutholwe imvula emhlophe.Imvula iqoqwe ngokuhlunga futhi yomiswa ngaphansi kwe-vacuum.Okuqinile kwabe sekuphathwa cishe ngo-8 mL we-acetone futhi kuhlungwa ukuze kukhishwe izinto ezingancibiliki.I-filtrate ewumphumela yengezwa ngezingxenye ezincane ku-60 mL we-diethyl ether ngokunyakaziswa okunamandla ekamelweni lokushisa.Umkhiqizo ofisa uqoqwe ngokuhlunga futhi womiswa ngaphansi kwe-vacuum ukunikeza u-4.5g (76%).